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Entry  Monday, February 05, 2018, 17:26, Marla Cervantes, UO2/C, 40282-1, TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#9 Carbonization-Batch9-060218.docx

Monday, February 05, 2018, 17:24

35 circles from cast#2 of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 4.59 g

Graphite container = 5.3 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 Tuesday, February 06, 2018, 10:59

Initial IGP1 = 4.79e-7 Torr

Tapped up entire process manually to 520A in 30 min

TGHT = 520 A, 5.32 V

Vacuum coming down indicating carbonization process complete.  

Will remain at max setpoint for 4 hrs to ensure full carbonization before cooling down.


 Tuesday, February 06, 2018, 14:44

Initiating auto-cool at 2.0 A/min 


 Thursday, February 08, 2018, 10:43

Vented with Ar and removed from EVAP1


 

Entry  Thursday, February 01, 2018, 13:15, Marla Cervantes, UO2/C, 40282-1, TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#8 Carbonization-Batch8-020218.docx

 Thursday, February 01, 2018, 12:59

35 circles of 14 mm diameter were packed into a graphite sample container.

28 discs corresponded to cats#1 and 7 discs to cast#2

35 x UO2/C circles = 3.42 g

Graphite container = 6.96 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 Friday, February 02, 2018, 13:18

Initial IGP1 = 4.82x10e-7 Torr

Tapped up entire process manually to 520A in 30 min

TGHT = 520 A, 5.63 V

Vacuum coming down nicely indicating carbonization process complete 

Will remain at max setpoint for 4 hrs to ensure full carbonization before cooling down.


 Friday, February 02, 2018, 16:57

Initiating auto-cool at 2.0 A/min 


Monday, February 05, 2018, 17:23 

Vented with Argon and removed form evaporator 1

Entry  Monday, January 29, 2018, 09:28, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, In progress, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#7 

 Monday, January 29, 2018, 09:26

35 circles of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 4.94 g

Graphite container = 5.03 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 

    Reply  Monday, January 29, 2018, 11:07, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Problems, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#7 

Marla Cervantes wrote:

 Monday, January 29, 2018, 09:26

35 circles of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 4.94 g

Graphite container = 5.03 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 29, 2018, 11:06

A power outage around 10 am tripped off EVAP1.

       Reply  Monday, January 29, 2018, 14:25, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Problems resolved, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#7 

Marla Cervantes wrote:

Marla Cervantes wrote:

 Monday, January 29, 2018, 09:26

35 circles of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 4.94 g

Graphite container = 5.03 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 29, 2018, 11:06

A power outage around 10 am tripped off EVAP1.

 Monday, January 29, 2018, 14:22

Water flow turned on.

Chamber set to pumping down. 


 

          Reply  Tuesday, January 30, 2018, 16:07, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#7 Carbonization-Batch7-300118.docx

Marla Cervantes wrote:

Marla Cervantes wrote:

Marla Cervantes wrote:

 Monday, January 29, 2018, 09:26

35 circles of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 4.94 g

Graphite container = 5.03 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 29, 2018, 11:06

A power outage around 10 am tripped off EVAP1.

 Monday, January 29, 2018, 14:22

Water flow turned on.

Chamber set to pumping down. 


 

 Tuesday, January 30, 2018, 16:06

Initial IGP1 = 9.4x10e-7 Torr

Tapped up entire process manually to 520A in 32 min

TGHT = 520 A, 5.45 V

Vacuum coming down indicating carbonization process complete 

Will remain at max setpoint for 4 hrs to ensure full carbonization before cooling down.


 Tuesday, January 30, 2018, 18:40

 Initiating auto-cool at 2.0 A/min 


 Wednesday, January 31, 2018, 14:00

Ar tank was changed.


Thursday, February 01, 2018, 12:58 

EVAP1 was vented with Argon and UCx was removed form evaporator 1.

 

Entry  Friday, January 19, 2018, 12:32, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, In progress, Carbonizing UO2/C discs for 1stepUCx in graphite sample container_#6 

 Friday, January 19, 2018, 12:29

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.69 g

Graphite container = 6.84 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 

    Reply  Monday, January 22, 2018, 15:51, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Problems, Carbonizing UO2/C discs for 1stepUCx in graphite sample container_#6 

Marla Cervantes wrote:

 Friday, January 19, 2018, 12:29

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.69 g

Graphite container = 6.84 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 22, 2018, 15:48

A power outage on Sunday tripped off EVAP1.

       Reply  Monday, January 22, 2018, 16:20, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Problems resolved, Carbonizing UO2/C discs for 1stepUCx in graphite sample container_#6 180122-1e-1.jpg

Marla Cervantes wrote:

Marla Cervantes wrote:

 Friday, January 19, 2018, 12:29

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.69 g

Graphite container = 6.84 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 22, 2018, 9:00

A power outage on Sunday tripped off EVAP1.

 Monday, January 22, 2018, 10:00

Chamber pumping down.

Water flow turned on.


Monday, January 22, 2018, 13:30

IGP1 = 8e-6 Torr

Tapped up entire process manually to 520A in 45 min

TGHT = 520 A, 6.08 V 

Vacuum coming down indicating carbonization process complete

Will remain at max setpoint overnight.


 

          Reply  Tuesday, January 23, 2018, 12:49, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container_#6 Carbonization-Batch6-220118.docx

Marla Cervantes wrote:

Marla Cervantes wrote:

Marla Cervantes wrote:

 Friday, January 19, 2018, 12:29

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.69 g

Graphite container = 6.84 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 

 Monday, January 22, 2018, 9:00

A power outage on Sunday tripped off EVAP1.

 Monday, January 22, 2018, 10:00

Chamber pumping down.

Water flow turned on.


Monday, January 22, 2018, 13:30

IGP1 = 8e-6 Torr

Tapped up entire process manually to 520A in 45 min

TGHT = 520 A, 6.08 V 

Vacuum coming down indicating carbonization process complete

Will remain at max setpoint overnight.


 

 Tuesday, January 23, 2018, 9:30

Initiating auto-cool at 2 A/min


 Tuesday, January 23, 2018, 16:00

 EVAP1 was not vented, Ar tank has low level, Ar tank will be replaced.


Wednesday, January 24, 2018, 11:37

 EVAP1 was vented very carefully using the Ar remaining in the Ar tank.

Ar tank remaining gas: ~8 psi.


Wednesday, January 24, 2018, 15:42 

UCx was transferred to glove box.

Final mass 4.501 g

Entry  Wednesday, January 10, 2018, 14:44, Marla Cervantes, UO2/C, 40282-1, TARGET BOAT, In progress, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#4 

 Wednesday, January 10, 2018, 14:44

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.75 g

Graphite container = 5.38 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.

    Reply  Friday, January 12, 2018, 07:46, Laura Lambert, UO2/C, , TARGET BOAT, In progress, Carbonizing UO2/C discs for 1stepUCx in graphite sample container_#4 

Marla Cervantes wrote:

 Wednesday, January 10, 2018, 14:44

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.75 g

Graphite container = 5.38 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.

 Friday, January 12, 2018, 07:43

IGP1 = 0.0266 Torr

TGHT = 520A, 5.92V

Voltage has been climbing consistently since it has reached it's max setpoint, gone up ~0.8V in ~18hrs

Carbonization complete.

Initiating auto-cool at 2.0A/min

Will update later with more information on this process.


 Friday, January 12, 2018, 09:47

Turned the turbo pump back on, to ensure safe cooling.


 

       Reply  Thursday, January 18, 2018, 11:56, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container TP1-off_#4 Carbonization-Batch4-110118-TP_off.docx

Laura Lambert wrote:

Marla Cervantes wrote:

 Wednesday, January 10, 2018, 14:44

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.75 g

Graphite container = 5.38 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.

 Friday, January 12, 2018, 07:43

IGP1 = 0.0266 Torr

TGHT = 520A, 5.92V

Voltage has been climbing consistently since it has reached it's max setpoint, gone up ~0.8V in ~18hrs

Carbonization complete.

Initiating auto-cool at 2.0A/min

Will update later with more information on this process.


 Friday, January 12, 2018, 09:47

Turned the turbo pump back on, to ensure safe cooling.


 

 Monday, January 15, 2018, 10:00

Vented with Argon and removed from evap1


NB: The initial mass of the UO2/C discs was 5.9 g

 

 

       The final mass of the UCx discs was 4.614 g

Entry  Wednesday, January 17, 2018, 13:47, Marla Cervantes, UO2/C, 40282-1, TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#5 Carbonization-Batch5-180118.docx

 Monday, January 15, 2018, 13:37

35 circles of 14 mm diameter were packed into a graphite sample container.

35 x UO2/C circles = 5.58 g

Graphite container = 5.22 g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3 new Ta foils for heat shielding and the boat was installed in Evap1.

Chamber currently pumping down.


Tuesday, January 16, 2018, 13:41 

Initial IGP1 = 9x10e-7 Torr

Tapped up entire process manually to 520A in 1.5 hrs

TGHT = 525 A, 5.64 V

Vacuum coming down nicely indicating carbonization process complete 

Will remain at max setpoint overnight to ensure full carbonization before cooling down.


Wednesday, January 17, 2018, 10:30

Initiating auto-cool at 2.0A/min 


Wednesday, January 17, 2018, 4:30

Vented with Argon and removed form evaporator 1

Entry  Thursday, November 23, 2017, 13:39, Marla Cervantes, UO2/C, 40282-2 , TARGET BOAT, Done, Carbonizing UO2/C discs for 1stepUCx in graphite sample container _#3 171124_1e-1.jpg

 Thursday, November 23, 2017, 13:34

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.75 g

Graphite container = 5.38 g

Graphite container is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 Friday, November 24, 2017, 12:48

IGP1=1.3e-6 Torr

TGHT = 520A, 4.98V 

Vacuum went down indicating carbonization.

Will remain at max setpoint for the weekend.


 Monday, November 27, 2017, 09:58

IG1 = 2.6e-6 Torr

TGHT = 520A, 5.1V

Carbonization complete in 3 hrs and 30 min.

Initiating auto-cool at 2.0A/min


 Wednesday, November 27, 2017, 13:10

 IEVAP was vented in argon and sample removed/transferred to glove box on Friday.

Entry  Wednesday, November 22, 2017, 14:20, Laura Lambert, , , , Maintenance, New eye wash for hot lab! 

 Wednesday, November 22, 2017, 11:05

Eye wash installed yesterday, simple attachment on sink spout.

Easy to use, simply twist attachment 180 degrees.

Water for tap can be turned on before or after twist.

Adjust pressure/ temperature accordingly.

Auto shut-off for eye-wash at ~38C [100F] - no accidental eye-burning when trying to wash eyes!


 

Entry  Tuesday, November 14, 2017, 16:16, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, Done, Carbonizing UC2 discs for 1stepUCx in graphite sample container _#2 striptool.JPG

 Tuesday, November 14, 2017, 16:12

Circles from cast 1 were used, the same as the last round of 1stepUCx [see elog i.d. 164]

A 14mm punch was used to punch out circles from the cast.

35 circles were packed into a graphite sample container.

35 x UO2/C circles = 5.43g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 Wednesday, November 15, 2017, 08:53

IGP1 = 1.6e-6 Torr

Tapping up manually...


 Wednesday, November 15, 2017, 11:59

IGP1 = 5.0e-5 Torr

Tapped up entire process manually to 520A in 3hrs!!!

TGHT = 520A, 4.98V

Vacuum coming down nicely indicating carbonization process complete 

Will remain at max setpoint for 4hrs to ensure full carbonization before cooling down later this afternoon.


 Wednesday, November 15, 2017, 15:16

IG1 = 8.65e-6 Torr

TGHT = 520A, 4.92V

Carbonization complete.

Initiating auto-cool at 2.0A/min


 Monday, November 20, 2017, 13:28

Evap1 was vented in argon and sample removed/ transfered to glove box on friday.

Discs look good, slightly lighter grayer compared to production UCx discs after second cast but before final carbonization.

Material seems to adhere to graphite backing foil well, no flakes coming off from just moving discs around.

Weight of 35 carbonized discs = 4.387g

Weight loss = 5.43g - 4.387g = 1.043g


 

Entry  Tuesday, November 07, 2017, 14:38, Laura Lambert, Empty, , LP-FEBIAD, Done, TBHT test with LP-FEBIAD evap1_data.xlsx

 Tuesday, November 07, 2017, 14:34

LP-FEBIAD used several years ago for temperature measurements is used for this test.

3xTa heat shields on container, incl center block - these heat shields have remained on there since the last round of tests in 2014?

Old version of LP container with larger center block.

Will heat TBHT to 290A and report data.

Loaded into evap1 and pumped down this a.m

IGP1 = 7.73e-6 Torr


Wednesday, November 08, 2017, 13:20

Tapped up to 290A manually.

TBHT epics controls = 287.7A, 2.45V

TBHT power supply = 290.4A, 2.46V

IGP1 epics = 2.51e-6 Toor

IGP1 direct readout = 3.18e-6 Torr

TP = 26.1C

Initiating auto-cool at 2.0A/min


 Thursday, November 09, 2017, 11:41

Vented in air.

TBHT test went well. 

See attachment for data collected.


 

Entry  Tuesday, November 07, 2017, 12:04, Laura Lambert, , , , Maintenance, Noise levels checked - ear protection not required. 

 Tuesday, November 07, 2017, 11:58

Noise levels were checked with monitor by Terry.

Max readings in lab reached ~83dB but sat between 70-78dB in most areas.

This is under limit for requirement to wear ear protection [85dB].

To reach limit - noise levels would need to increase drastically.

Conclusion: ear protection not required in lab.

Recommended if working in there for long periods of time for personal preference, but not a requirement.


 

Entry  Tuesday, November 07, 2017, 11:57, Laura Lambert, , , , Maintenance, Interlocks limits changed to 100mTorr 

 Tuesday, November 07, 2017, 11:55

Interlocks limits updated/ changed to 100mTorr for both TGHT and TBHT by Ray


 

Entry  Tuesday, October 10, 2017, 14:16, Laura Lambert, UO2/C, 40282-1, TARGET BOAT, Done, Processing UC2Flk_19 

 Tuesday, October 10, 2017, 14:11

UO2/C green was prepared Oct 4th, 2017

The cast peeled off the glass nicely Oct 6th, 2017

Initial UO2 powder used = 50.26g (Inventory R-01032A, UO2 + bottle = 676.34g before use)

Graphite powder used = 10.12g

Green cast dried UO2/C + organic mass = 61.30g 

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat was wrapped with 3-layers of heat shield [reused] and installed in evap1 this morning.

Chamber currently pumping down.

Target boat will be ramped up to 520A.

Vacuum limit stop at 3.0e-4 Torr, backing off at 6.0e-4 Torr.


 Wednesday, October 11, 2017, 09:06

IGP1 = 1.74e-6 Torr

Tapped up to 35A, 0.29V

Waited ~70min, vacuum stable.

IGP1 = 6.9e-6 Torr

Initiating auto-ramp at 0.2A/min


 Wednesday, October 11, 2017, 13:06

IGP1 = 3.1e-4 Torr

TGHT = 61A, 0.49V

Vacuum stable.

Changing vacuum limits.

Vacuum limit stop at 5.0e-4 Torr, backing off at 8.0e-4 Torr.


 Thursday, October 12, 2017, 08:31

IGP1 = 1.06e-5 Torr

TGHT = 275A, 2.55V

Vacuum stable.

Increasing ramping rate to 0.5A/min.


 Thursday, October 12, 2017, 09:03

IGP1 = 1.47e-5 Torr

TGHT = 290A, 2.70V

Vacuum stable.

Increasing ramping rate to 1.0A/ 30sec.


 Friday, October 13, 2017, 08:30

IGP1 = 5.8e-6 Torr

TGHT = 520A, 4.98V

Vacuum stable.

Carbonization process complete!

Evap1 has remained at max setpoints for ~17hrs

Initiating auto-cool at 1.0A/min


 Tuesday, October 17, 2017, 15:01

TGHT had sat at 0A for at least 24hrs.

At ~3:30-4am this morning everything tripped off. The only thing remained on was the roughing pump.

Power bump? Did someone accidentally turn it off? Will follow up on this...

Vacuum was sitting at ~3.5e-2Torr when I noticed today.

Most vacuum had been lost, but there was still a small vacuum - materials should be okay.

Purged and vented in Ar.

Transferred materials to glove box.


 

Entry  Wednesday, September 27, 2017, 12:05, Laura Lambert, UO2/C, 40282-1, TARGET BOAT, Done, Processing UC2Flk_18 

 Wednesday, September 27, 2017, 09:25

UO2/C green was prepared Sept 20th, 2017.

The cast peeled off the glass Sept 22nd, 2017 - not quite enough 'special' ingredient.

UO2 stuck to glass around edges of cast - a lot of flakes produced while peeling off.

Initial UO2 powder used = 50.00g (Inventory R-01032A, UO2 + bottle = 726.38g before use)

Graphite powder used = 10.03g

Green cast dried UO2/C + organic mass = 60.38g 

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat was wrapped with 3-layers of heat shield [reused from last 1stepUCx] and installed in evap1 yesterday afternoon.

Chamber pumped down overnight.

Target boat will be ramped up to 520A.

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.

IG1 = 3.5e-6 Torr

Tapped up to 30A, 0.43V

Waited ~50min, vacuum stable.

IGP1 = 8.6e-6 Torr

Initiating auto-ramp at 0.1A/min


 Wednesday, September 27, 2017, 13:28

IGP1 = 1.4e-5 Torr

TGHT = 38.5A, 0.48V

Vacuum stable.

Changing vacuum limits and ramping rate.

Vacuum limit stop at 2.0e-4 Torr, backing off at 5.0e-4 Torr.

Increasing ramping rate to 0.2A/min.


 Thursday, September 28, 2017, 08:41

IGP1 = 3.26e-5 Torr

TGHT = 174A, 1.71V

Vacuum stable.

Increasing ramping rate to 0.5A/min.


 Thursday, September 28, 2017, 09:56

IGP1 = 4.85e-5 Torr

TGHT = 195A, 1.92V

Vacuum initially climbed a small amount with last increase, has started to decrease - vacuum stable.

Increasing ramping rate to 1.0A/min.


Thursday, September 28, 2017, 10:30  

IGP1 = 5.3e-5 Torr

TGHT = 220A, 2.18V

Vacuum increased slightly again with faster ramping rate.

Vacuum now dropping - stable.

Increasing ramping rate to 2.0A/min.


 Thursday, September 28, 2017, 11:07

IGP1 = 6.35e-5 Torr

TGHT = 302A, 3.09V

Vacuum increased slightly again with faster ramping rate.

Vacuum now dropping - stable.

Increasing ramping rate to 2.5A/min.


Thursday, September 28, 2017, 11:45

IGP1 = 1.67e-4 Torr

TGHT = 380A, 4.04V

Vacuum increased normally at slow rate for first half hour.

~30min into the 2.5A/min rate increase, vacuum started to climb much faster.

Paused auto-ramp for few min to allow vacuum to stabilize.

Vacuum decreasing - stable.

IGP1 = 1.4e-4 Torr

Decreasing ramping rate to 0.5A/min for next hour while unable to watch.


 Thursday, September 28, 2017, 13:20

IGP1 = 1.93e-4 Torr

TGHT = 425A, 4.58V

Vacuum stable.

Changing vacuum limits and ramping rate.

Increasing ramping rate 1.0A/min.

Vacuum limit stop at 3.0e-4 Torr, backing off at 6.0e-4 Torr.


 Thursday, September 28, 2017, 14:06

IGP1 = 3.1e-4 Torr

TGHT = 456A, 4.93V

Vacuum stable.

Changing vacuum limits and ramping rate.

Changing ramping rate to 0.5A/ 30sec.

Vacuum limit stop at 4.0e-4 Torr, backing off at 7.0e-4 Torr.


 Thursday, September 28, 2017, 14:44

IGP1 = 4.0e-4 Torr

TGHT = 468A, 5.07V

Vacuum stable.

Changing vacuum limits.

Vacuum limit stop at 5.0e-4 Torr, backing off at 8.0e-4 Torr.


 Thursday, September 28, 2017, 15:49

TP thermocouple = 28.1C

IGP1 = 5.0e-4 Torr

TGHT = 485A, 5.25V

Vacuum stable.

Changing ramping rate for overnight heating.

Decreasing ramping rate to 0.5A/min.


 Friday, September 29, 2017, 09:11

TP thermocouple = 26.1C

IGP1 = 5.0e-6 Torr

TGHT = 520A, 5.60V

Vacuum stable.

Carbonization process complete!

Evap1 has remained at max setpoints for ~13hrs

Initiating auto-cool at 1.0A/min


 Tuesday, October 03, 2017, 10:09

Vented in Ar and transferred from evap1 to glove box yesterday.


 

Entry  Thursday, September 21, 2017, 11:35, Laura Lambert, Empty, , , Done, Testing TBHT [1st run!], RP [new oil] and IG [new gauge] 

 Thursday, September 21, 2017, 11:32

Copper plate attached to TBHT to allow current to be applied.

Started pumping down this a.m.

Roughing pump sounds normal.

Currently Ion Gauge times out before turning on, will attempt again later when lower vacuum achieved...


 Monday, September 25, 2017, 13:30

Ion Gauge hadn't been fully hooked up via eipcs yet.

Ramped down last week/ vented/ hooked up ion gauge in epics/ restarted IOC - now updated and good to go.

Started pumping down again this a.m.

Roughing pump sounds normal.

Ion gauge working well!

IGP1 = 2.7e-5 Torr


 Wednesday, September 27, 2017, 09:20

Cooled down, vented in air and opened up yesterday.

TBHT ran well -  readout on power supply and readout on striptool were very close.

Roughing pump ran smoothly - nothing other than usual problems.

Sometimes when roughing pump is 1st turned on it chokes up and sounds TERRIBLE. At this point if you turn it off and leave it for a few seconds then try turning it on again it usually works fine.

Ion gauge ran well - direct readout vs striptool readout are slightly off because the direct readout is in mBar and the striptool in Torr.

One minor thing noticed with the new ion gauge - when water is turned on the vacuum increases very minorly by ~5e-8 Torr.

This wouldn't show up with the old Ion Gauge - maybe the new one is slightly more sensitive?

Otherwise everything ran great 


 

Entry  Wednesday, September 20, 2017, 08:07, Aaron Schmidt, , , , Maintenance, Ion gauge & RP status 

Wednesday, September 20, 2017, 08:00: 

-A new ion gauge was installed yesterday afternoon and the old one removed. The old IG was found to be contaminated (300 cpm) and as of 20/09/2017, it is double bagged and stashed underneath the evaporator for the time being. 

Completed under work permit: I2017-09-19-9

-The roughing pump was reconnected this morning without issue.

Entry  Thursday, September 07, 2017, 14:26, Aaron Schmidt, , , , Maintenance, roughing pump oil replaced 

 Thursday, September 07, 2017, 11:00 -12:00

The roughing pump was disconnected from Evaporator 1, along with the exhaust/ventilation. No contamination was found on swipes.

The oil was refilled.

The roughing pump was then moved away from the PLC to allow access for Dave Morris. The RP can be reconnected and tested after the PLC work is complete.

Work permit # I2017-09-07-1

 

Entry  Wednesday, August 23, 2017, 15:54, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, Done, Carbonizing UC2 discs for 1stepUCx in graphite sample container _#1 IMG_1768.JPGIMG_1774.JPG

 Wednesday, August 23, 2017, 15:41

2 rounds of UO2/C were cast onto a graphite sheet in the fume hood and let dry.

For this round of samples, circles from cast 1 were used

Graphite powder used = 5.16g

A 14mm punch was used to punch out circles from a 16mm wide strip.

35 circles were packed into a graphite sample container.

graphite container [no endcap] = 3.37g

35 x UO2/C circles = 4.76g

graphite container+smpls = 8.13g

container+smpls+endcap = 10.08g

Graphite tube is placed inside a target boat.

Boat previously coated with TaC and sintered - 1st use of newly sintered boat.

Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber currently pumping down.


 Friday, August 25, 2017, 09:59

IG1 = 3.45e-6 Torr.

Stepped up manually to 80A.

Vacuum stable.

IG1 = 3.0e-5 Torr.

Initiating auto-ramp.

Target boat will be ramped up to 520A at the rate of 0.1A/min.

Vacuum limit stop at 1.0e-4 Torr, backing off at 5.0e-4 Torr.


 Monday, August 28, 2017, 08:09

IG1 = 6.3e-6 Torr

TGHT = 455A, 4.65V

Vacuum stable.

Increasing ramping rate to 0.2A/min.


 Monday, August 28, 2017, 08:53

IG1 = 7.3e-6 Torr

TGHT = 465A, 4.75V

Vacuum stable.

Increasing ramping rate to 0.5A/min.


 Monday, August 28, 2017, 13:17

IG1 = 1.32e-5 Torr

TGHT = 520A, 5.44V

Vacuum still fairly high and not dropping very fast indicating carbonization incomplete.

Increasing max setpoint to 530A and restarting auto-ramp.


 Monday, August 28, 2017, 15:13

IG1 = 1.32e-5 Torr

TGHT = 530A, 5.58V

Vacuum still high, wavering up and down/ not dropping - carbonization remains incomplete.

Increasing max setpoint to 540A and restarting auto-ramp.


 Tuesday, August 29, 2017, 09:28

IG1 = 3.72e-6 Torr

TGHT = 540A, 5.66V

Carbonization complete.

Initiating auto-cool at 2.0A/min


 

Entry  Thursday, July 13, 2017, 12:49, Laura Lambert, , , , Problems, *hot lab is HOT* Capture.JPG

Thursday, July 13, 2017, 12:48

NOTE: hot lab reached 27degrees every day this week and went up to 28C today! 

This is with the small portable fan running.

27C was reached even with both evaporators off.

When at 28C: evap2 = ~1500C and evap1 = 35A


 Thursday, July 20, 2017, 15:58

Hot lab reached 30C today.

Small fan off - unsure if able to run due to contamination spread...

Both evap1 and evap2 were under vacuum but had not initiated ramping up yet.


 

    Reply  Thursday, July 27, 2017, 09:08, Laura Lambert, , , , Problems resolved, *hot lab is HOT* 

Laura Lambert wrote:

Thursday, July 13, 2017, 12:48

NOTE: hot lab reached 27degrees every day this week and went up to 28C today! 

This is with the small portable fan running.

27C was reached even with both evaporators off.

When at 28C: evap2 = ~1500C and evap1 = 35A


 Thursday, July 20, 2017, 15:58

Hot lab reached 30C today.

Small fan off - unsure if able to run due to contamination spread...

Both evap1 and evap2 were under vacuum but had not initiated ramping up yet.


 

 Thursday, July 27, 2017, 09:06

There was a broken valve motor affecting all ISAC rooms - temporary fix in place.

Ventilation in ISAC hot lab has been increased.

Temperature back to a reasonable level - currently sitting at 22C!


 

Entry  Wednesday, July 12, 2017, 17:07, Laura Lambert, UC2, 42218-15, LP-SIS, In progress, Conditioning UCx#21 

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

    Reply  Thursday, July 13, 2017, 14:50, Laura Lambert, UC2, 42218-15, LP-SIS, Problems, Conditioning UCx#21 

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

       Reply  Wednesday, July 19, 2017, 14:15, Laura Lambert, UC2, 42218-15, LP-SIS, Problems resolved, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

          Reply  Wednesday, July 19, 2017, 14:17, Laura Lambert, UC2, 42218-15, LP-SIS, In progress, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

             Reply  Thursday, July 20, 2017, 15:00, Laura Lambert, UC2, 42218-15, LP-SIS, Problems, Conditioning UCx#21 Capture.JPGCapture3.JPG

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

                Reply  Thursday, July 20, 2017, 15:35, Laura Lambert, UC2, 42218-15, LP-SIS, Problems resolved, Conditioning UCx#21 

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

 Thursday, July 20, 2017, 15:14

Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2

AKA attempting to take a vacuum reading from one that doesn't exist for evap1

This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.

Changed a few things in the auto-ramp system:

-Updated messages.

-Auto-ramp aborts when TGHT/TBHT trips off.

-Displays setpoint it is ramping up to for next step

-Confirms which ion gauge it is reading

-Displays final setpoint and increment on message board

-No longer displays TBHT as 'tripped off' when not running.

System updated.


 

                   Reply  Thursday, July 20, 2017, 15:57, Laura Lambert, UC2, 42218-15, LP-SIS, Done, Conditioning UCx#21 IMG_3249.JPGIMG_3251.JPGIMG_3257.JPGIMG_3258.JPGIMG_3260.JPG

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

Laura Lambert wrote:

 Wednesday, July 12, 2017, 17:06

Target container was previously coated with TaC and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 400 discs of UCx with 13.60cm in length [8 packs of 5 + 360 single discs/ 2.6cm on left side, 2.8cm on right side wrt ionizer into page].

Discs in target are arranged as follows: 1pack / 60singles / 1pack / 60singles / 1pack / 60singles / 2packs / 60singles / 1pack / 60singles / 1pack / 60singles / 1pack

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 450A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog373 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, July 13, 2017, 12:49

Tapped up manually to 35A.

Waited ~2hrs, vacuum stable: IG1 = 2.64e-6 Torr

Initiating auto-ramp.


 

 Thursday, July 13, 2017, 14:48

Update: auto-ramp not started.

With recent updates to evap1 epics, not everything was uploaded correctly.

TGHT auto-ramp system not working: parameter boxes have white outline indicating locked.

No parameters can be inputed and therefore unable to start auto-ramp.


 Friday, July 14, 2017, 15:56

Problems still not fixed.

Have tapped up manually to 50A, 0.59V

Vacuum stable; IG1 = 5.26e-6 Torr.

Will remain at setpoints over weekend before continuing to ramp up manually...


 Monday, July 17, 2017, 15:10

New problems:

Paddle wheels for evap2 need replacing asap [see elog evap2 i.d.378]

In order to replace, supply/ return need to be turned off and a full purge; therefore, evap1 must be off otherwise it will trip off from no water.

Evap2 needs to be fixed asap and cannot wait for this process to be complete.

Evap1 had been tapped up manually to 60A.

Tapping down manually to 0A so one can start the paddle wheel replacement work tomorrow.


 Tuesday, July 18, 2017, 15:31

Paddle wheels for evap2 replaced and up and running again.

IG1 = 1.2e-6 Torr.

Starting to tap back-up manually...


 

 Wednesday, July 19, 2017, 14:12

TGHT auto-ramp fixed.

Since TBHT isn't hooked up yet, epics thinks TBHT has tripped off.

Currently during auto-ramp, every time steps up: states TBHT tripped off.

This is not the case but not a big deal as we will soon have TBHT hooked up and this won't be an issue.

Also it only states it, doesn't stop auto-ramp and therefore technically works fine/ will go with this for now...

Note: Might be a few spikes on striptool from past hour when IOC was rebooted.


 

 Wednesday, July 19, 2017, 14:16

Tapped up manually to 30A yesterday.

Continued manual tap up today and reached 60A.

Initiated auto-ramp.

IG1 = 4.4e-6 Torr


 

 Thursday, July 20, 2017, 14:48

TGHT tripped off yesterday evening 

Auto-ramping was fixed but a few more glitches in the system caused the TGHT to trip.

Please refer to photos.

When auto-ramp is running and vacuum reaches the parameter set for 'Good Vacuum', the auto-ramp should stop until the vacuum drops below the good vacuum at which point it can then continue to auto-ramp.

When auto-ramp is running and vacuum reaches the parameter set for 'Bad Vacuum', the auto-ramp should initiate auto-cool/ramp-down until the vacuum drops to the good vacuum parameter at which point it can then proceed with the 'Good Vacuum' requirement.

With this scenario, the auto-ramp system ignored the parameters set for good and bad vacuum, proceeded past both points and continued to ramp until the vacuum eventually reached it's trip off vacuum causing the TGHT to trip.

The TGHT current was at ~90A when it tripped off, so the target should be OK.


 

 Thursday, July 20, 2017, 15:14

Turns out the auto-ramp was reading the vacuum of 'IGP1' which is what the old ion gauge used to be called for evap1 and is currently one on evap2

AKA attempting to take a vacuum reading from one that doesn't exist for evap1

This ion gauge is now labelled 'IGP' and the auto-ramp system now uses 'IGP' for the vacuum parameter confirmations.

Changed a few things in the auto-ramp system:

-Updated messages.

-Auto-ramp aborts when TGHT/TBHT trips off.

-Displays setpoint it is ramping up to for next step

-Confirms which ion gauge it is reading

-Displays final setpoint and increment on message board

-No longer displays TBHT as 'tripped off' when not running.

System updated.


 

Thursday, July 20, 2017, 15:57

Tapped up manually to 35A, 0.45V

IG1 = 5.26e-6 Torr

Re-initiated auto-ramp at 0.1A/min.


 Friday, July 21, 2017, 13:50

TGHT = 81A, 0.92V

IG1 = 5.2e-5 Torr

Vacuum currently yo-yo-ing, but stable.

Changing vacuum limits.

Vacuum limit stop at 1.0e-4 Torr, backing off at 5.0e-4 Torr.

TP = 28.4C, RT = 27.3C


 Thursday, July 27, 2017, 09:02

TGHT = 431A, 4.37V

IG1 = 1.32e-5 Torr

Vacuum stable.

Increasing ramping rate to 0.2A/min

TP = 26.7C, RT = 22.0C


 Friday, July 28, 2017, 09:35

TGHT = 450A, 4.59V

IG1 = 5.4e-6 Torr

Target has remained at max setpoint for 23hrs.

TP = 25.9C, RT = 19.5C

Initiating auto-cool at 1.0A/min


 Friday, August 04, 2017, 13:59

Evap1 was vented in Ar and transferred to the glove box on monday.

A few discs on opened end had slightly shifted [see photo], discs moved back in place - can see down into target.

Discoloration of Ta container to gold in some spots - this is normal as seen with most UCx targets

Target looks good.

Still requires 2nd endcap to be inserted.


 Monday, August 21, 2017, 11:13

Both endcaps in.

No Rh foil inserted.

Endcaps require expanding.


 

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