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  Evaporator_2, Page 6 of 35  Not logged in ELOG logo
IDdown Date Author Target Material Target Oven W.O# Source Status Subject
  590   Thursday, September 01, 2022, 12:32 Darwin Ortiz RosalesTaC44691-13LP-SISDoneTaC coating sintering

Thursday, September 01, 2022, 10:34

The coated container was wrapped in three Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp starged at 2A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-05 Torr

Bad vacuum = 5.0E-04 Torr


Thursday, September 01, 2022, 12:39

Has been stabilizing at 40A on both heaters.

Starting 1A/min autoramp to 80A

 

A discrepancy between setpoint and readback currents was observed for both TGHT and TBHT.  The difference is substancial and warrants investigation.  This process will be paused until further notice


Tuesday, September 06, 2022, 14:45

Controls has been troubleshooting EVAP2.  In the process TBHT has been damaged. Arthur will take a look at it ASAP and his group will try and fix it tomorrow. 

Regarding our initial problem, it appears that when an electrical safety box was installed, the copper water lines connected to output terminals of the power supply, were moved so that they were in contact with the evaporator cage.  See the figure below.


Thursday, September 08, 2022, 12:47

 Target has been removed and a new test target (HP-FEBIAD) has been placed inside.  System left to generate enough vacuum and then testing will be performed.


Friday, September 09, 2022, 15:58

System was tested and all seems good.  This coat/sintering will continue after conditioning of graphite material

 


Saturday, September 24, 2022, 09:13

Continuation of process. 

IGP1= 4.3e-07 Torr

ramping @ 1A/min to 230 A on both TGHt and TBHT


Saturday, September 24, 2022, 16:28

ramped to 430A, 7.2V on TGHT and 233A, 4.2V on TBHT.  Will leave until 7 pm.

 


Saturday, September 24, 2022, 19:44

Starting rampdown @-2A/min TGHT -1A/min TBHT

camera offline

IGP1= 1.2e-6 Torr

 


Monday, September 26, 2022, 09:41

IGP1=2.2e-07 Torr.  Shutting off TBHT and TGHT.


Thursday, September 29, 2022, 09:53

Final notes: coating looks good .  Probably 3 hours at final temperature is better to prevent material degradation.

  589   Thursday, August 25, 2022, 10:16 Darwin Ortiz RosalesTiC44692-10HP-FEBIADDoneTiC 220818 Sintering (TiC #6)

Thursday, August 25, 2022, 10:06

 

Target container is loaded with 379 Discs of TiC for Target and 5 extra discs for analysis on left end

Target length = 12.5

3 Ta foil heatshields and on TaC coated Ta spring on right side

Total weight including heatshields and spring = 1551.4 g   Final total weight = 1545.5 g

Final power should be ~10988 Watt

TGHT ramp up to 820A, and TGHT to 300A at 0.1A/min.

IGP1= 7.7e-7 Torr

Good vacuum =3.0e-05 Torr

Bad vacuum = 5e-04 Torr

Initial TGHT and TBHT autoramped @1A/min to 50A

TBHT mas 230A

TGHT max depends on final power

 


Thursday, August 25, 2022, 11:17 

Start autoramp at 1A/min to 80A on both TGHT and TBHT


Thursday, August 25, 2022, 11:54 

leaving at 80A until pressure stops rising

 


Thursday, August 25, 2022, 22:29

left to autoramp to 230A TBHT and 750 A TGHT since approximately 2:00 pm

Will leave ramping @1A/min to 750 A on TGHT

TBHT currently at 230A


 Friday, August 26, 2022, 07:27

TGHT = 850A, 9.3V

Started autoramp to 850A at 1A/min for TGHT

TBHT held at 230A

OMEGA = 1584C

 


Friday, August 26, 2022, 09:34

Target running at ~820A, 13.1 V since 9

Cooling to start between 1:15 to 1:30 pm

OMEGA reads 1668 C at top current

current reading oscillates between 812A and 828A and 13.1V  to 13.2V.

 


Monday, August 29, 2022, 12:21

Cooling at -2A/min for TGHT and -1A/min TBHT started on time on Friday August 26th.

Target remained under vacuum after cooling, over the weekend.

Target removed this morning and looks good. 5 discs removed for analysis

 

  588   Wednesday, August 10, 2022, 09:31 Ivan BaoEmpty TARGET BOATIn progressTC tests

1st test polarity 1

10:12 am Begin pumping down to rough vacuum
12:50 pm begin ramping up towards 2000C. Ta tube only, welded thermocouple mount
3:08 Ta tube reached 2000C, began ramping down. The ramping up process was smooth and no hiccups happened
4:57 ramp down complete, began shutting down the evap2, will let the turbopump to slow down spin overnight.

2nd test polarity 2(swapped)

Tuesday, Aug 09 2022, 4pm begin pumping to vacuum after switching the polarity of the power supply

Wednesday, August 10, 2022, 13:09 begin ramping up

3:18 ramped to 671A. 2000C, no hiccups, everything is nominal. The thermocouple reads higher than before, about 20-30 deg C colder than pyro at high temperatures (1400C and above)

No bad connections, short circuits or unexpected overheating.

begin ramping down

ramping down was smooth, with error being the TC about 40 deg C colder than pyro at temp above 1500C

ramping done completed at Wednesday, August 10, 2022, 16:46 , shutting down evap 2 roughing and turbopump

  587   Thursday, August 04, 2022, 09:31 Ferran Boix PamiesEmpty TARGET BOATIn progressTC on Ta boat test.

 11am: Setting up new target tube thermocouple test

Thursday, August 04, 2022, 09:31 Test finished August 3rd afternoon. Venting now.  

 

 

  586   Wednesday, June 29, 2022, 10:12 Darwin Ortiz RosalesTaC44692-10HP-FEBIADDoneTaC coating sintering

Wednesday, June 29, 2022, 10:07

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

OMEGA slope= 0.990

Good vacuum = 3.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 1.2 e-06 Torr

Start autoramp @2A/min to 80 A then autoramp heat @1A/min to 150 A.  Then autoramp TGHT to 675A and TBHT to 230A.1


Wednesday, June 29, 2022, 10:13

Chamber isolation performed and no change of pressure observed.

Water leak test performed and no pressure change detected.

Starting ramp up


Wednesday, June 29, 2022, 13:23

Ramping to 675A on TGHT and 230A on TBHT @ 2A/min

Ramped TGHT to 680A, 10.6V  and held for 4 hours


Wednesday, June 29, 2022, 21:52

Started rampdown @-2A/min TGHT and -1A/min TBHT

  585   Tuesday, June 28, 2022, 09:31 Ferran Boix PamiesEmpty41882-2TARGET BOATIn progressTC test on Ta tube

Tuesday, June 27, 2022, early afternoon: We assembled the setup in evap2 and started the pumps leaving it running over night.

Tuesday, June 28, 2022, 09:31 Turbo pump stopped for unknown reasons a few hours after we left. Restarting the pump.

Tuesday, June 28, 2022, 10:23 Vacuum down to 1e-5T start to ramp up TGHT 1A/10s to 200A.

Tuesday, June 28, 2022, 1:20 pm, Ramped from 0-500A. thermocouple reading 900C while pyrometer reads 1600C. begin ramping down to 0A.

  584   Tuesday, June 21, 2022, 09:48 Darwin Ortiz RosalesSiC37978-1HP-FEBIADDoneT-220617 sintering

Tuesday, June 21, 2022, 09:43

Total number of foils: 377 ( including 6 analysis discs on the right side of the container)

Total weight = 1454 g (includes heatshields, spring and T bar)

Total length packed 15.5 cm (excluding 6 analysis discs that will be removed)

container has 3 Ta heat shields and is coated

No endcaps inserted to facilitate out-gassing

Ta coated spring at  front (right) side

Initially to ramp TGHT and TBHT to 80A at 2 A/min

then to 120A and slow down ramp when pressure begins to increase

max approx 675A on TGHT and 230A on TBHT (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -4 Torr

Bad vac at 5.00 e-2 Torr

 IGP1=3.6 e-07 Torr at start of initial ramp.

 


Tuesday, June 21, 2022, 13:54

IGP1= 7.1 e-05 and dropping.  Start ramp to 150A for both TGHT and TBHT @1A/min


Tuesday, June 21, 2022, 21:27

Increased ramp rate to 3A/min for TGHT to 675A


Tuesday, June 21, 2022, 22:38

Ramp up to 685 A on TGHT and leave for 4 hours. 

OMEGA = 1645 C but suspect reading not on Ta surface.


Wednesday, June 22, 2022, 02:28

IGP1=7.7e-6 Torr

OMEGA =1610C

TGHT = 685A, 10.5V

TBHT = 230A, 3V

initiate rampdown at -2A/min and -1Amin TGHT and TBHT

  583   Monday, June 20, 2022, 14:52 Darwin Ortiz RosalesEmpty  Donesoftstart of new TP

Monday, June 20, 2022, 14:50

A new Turbo pump was installed this morning and it was soft started.  It has operated correctly and it is ready for use.  Derek O.  installed it.

Previous pump had issues at start-up and was diagnosed as finished by Edi/

 

  582   Tuesday, June 14, 2022, 09:04 Darwin Ortiz RosalesTa37978-1HP-FEBIADDoneTaC coating sintering

Tuesday, June 14, 2022, 08:47

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

OMEGA slope= 0.990

Good vacuum = 3.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 1.2 e-06 Torr

Start autoramp @2A/min to 80 A then autoramp heat @1A/min to 150 A.  Then autoramp TGHT to 675A and TBHT to 230A.


Tuesday, June 14, 2022, 08:49

IGP1= 0.13 Torr

*had timed out and it was off.  I RST and turned back on.*

Will wait for the pressure to drop to start heating


 Tuesday, June 14, 2022, 09:36

IGP1= 9.4e-06 Torr

Start autoramp @2A/min to 80A


Tuesday, June 14, 2022, 11:27

IGP1= 8.7 e-06 Torr Trending down. 

TGHT= 146A, 1.6V

TBHT= 146A, 1.7V

Has been ramping at 1A/min

Change ramp rate to 2A/min to 700A on TGHT and 230A on TBHT


Tuesday, June 14, 2022, 14:48

Change final current on TGHT to 675A, according to plot.  May change again. 

Currently TGHT=  537A, 7.7V 

IGP1= 4.4e-06 Torr


Tuesday, June 14, 2022, 18:46

Top temperature was 1825 Celsius at TGHT = 675A

Will start rampdown at 8:00 pm

 


 Tuesday, June 14, 2022, 20:01

TGHT= 675A, 10.3 V

TBHT= 230A, 3V

OMEGA= 1815C

IGP1= 3.9e-06 Torr

ramping down @-2A/min TGHT and -1A/min TBHT

  581   Thursday, June 09, 2022, 19:20 John Wong boat Donecarbonize PAN 10% discs

Flora Wu wrote:

Thursday, June 09, 2022, 11:25

Total number of foils: 14 electrospun fiber pellets 

Total weight = 208.3 g

container has 3 Ta heat shields.

Desired temperature at 1800 C

Omega slope set at 0.990 

Good vac = 3.0e-5 Torr,

Bad vac = 5.0e-5 Torr.

Pumping down in progress


 Thursday, June 09, 2022, 11:25

chamber pumped down below 5e-5

initiate auto ramping, 1A/min ----> 100 A


 

 

 Thursday, June 09, 2022, 19:16

Pressure came down below 10e-5 Torr as TGHT ramped up to 100A.

Continue auto ramping to reach 250A at 1A/min.


 Thursday, June 09, 2022, 22:52

TGHT is hovering around 127A/1.68 V due to erractic pressure, see attachment #1..  Notice the backing line is at atm pressure - I don't recall this happened in the past

Temp is still low to be detected on Omega.  Will leave this overnight.


 Friday, June 10, 2022, 09:07

TGHT has been holding at 250A/3.76V since 2:45am.  Pressure comes down as THGT above 200 A.  Backing line is back down normal.

Temp reading at 1040 C. 

see attachment #2.

Continue to ramp up to 300A, monitoring temp/pressure.


 Friday, June 10, 2022, 10:31

TGHT reached to 300A/4.63V, temp at 1145C.  Pressure at 1.8e-6 and coming down. 

Continue to ramp up to 350A.


 Friday, June 10, 2022, 11:59

TGHT at 350A/5.66V, temp at 1300 C, Pressure at 8.1e-7 Torr, and coming down.

Continue to ramp up to 400A.


Friday, June 10, 2022, 13:19

TGHT reached to 400A/6.73V.  Pressure coming down from 1.04e-6 Torr. 

Temp at 1690.  Will set up manually to reach 1800 C. 


 Friday, June 10, 2022, 13:50

TGHT stepped up to 432A/7.42V.  Pressure coming down from 1.3 e-6 Torr. 

Temp at 1800 C.  See attachment#3 and #4 for the screenshot and temp-current plot.

Dumped striptool data to /usr1/evpr/carbonize_pan10_elog581_a and b.

Will keep at this setting over the weekend, and cooling down will take place on Sunday evening. 

 


 Sunday, June 12, 2022, 22:30

TGHT has been holding at 432A/7.40V since Friday.  Temperature has gone up slightly to 1825. 

See attachment#5 for the overall process. 

Initiated cooling down at -2A/min.

Chamber will be vented on Monday morning.


 

  580   Thursday, June 09, 2022, 09:09 Darwin Ortiz RosalesTa HP-FEBIADDoneTroubleshooting

Thursday, June 09, 2022, 09:07

Yesterday, Wednesday June 08, 2022 @ ~3.00 pm a "dummy" target container was installed in EVAP 2 after the heatshield assembly had been swapped.

The purpose is to test correct functioning of the system.  Melting and evaporation on one of the bolts of the previous target container (eLog578) prompted the change in heatshield assembly and current testing.

TGHT was ramped up to 740A @ 4A/min, left to run at the final current for ~4.5 hours and then ramped down @-2A/min to 0A.

Will dismount dummy container this morning.

IGP1=2.5e-07 Torr


Thursday, June 09, 2022, 11:16

The target appears in good shape.  No abnormal behaviour. 

Picture attached are of the previous failed target eLog 578

 

  579   Wednesday, June 08, 2022, 10:00 Flora Wu boat Donecarbonize PAN 10% discs

Thursday, June 09, 2022, 11:25

Total number of foils: 14 electrospun fiber pellets 

Total weight = 208.3 g

container has 3 Ta heat shields.

Desired temperature at 1800 C

Omega slope set at 0.990 

Good vac = 3.0e-5 Torr,

Bad vac = 5.0e-5 Torr.

Pumping down in progress


 Thursday, June 09, 2022, 11:25

chamber pumped down below 5e-5

initiate auto ramping, 1A/min ----> 100 A


 (see eLog 581)

 

  578   Tuesday, June 07, 2022, 07:31 Darwin Ortiz RosalesSiC42464-2HP-FEBIADDoneT-220524 Sintering SiC

Tuesday, June 07, 2022, 07:19

Total number of foils: 403 ( including 5 analysis discs on the right side of the container)

Total weight = 1535.3 g (includes heatshields, spring and T bar)

Total length packed 16.4 cm (excluding 5 analysis discs that will be removed)

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Ta coated spring at  front (right) side

Initially to ramp TGHT and TBHT to 50A at 3 A/min

then continue to 80A and slow down ramp when pressure begins to increase

max approx 700A on TGHT and 230A on TBHT (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -4 Torr

Bad vac at 5.00 e-2 Torr

 IGP1= 7.6 e-07 Torr at start of initial ramp.


 Tuesday, June 07, 2022, 11:14

Ramping to 150A on TGHT and TBHT at 1A/min


Ramped TGHT and TBHT to 230A at 2A/min

Tuesday, June 07, 2022, 13:12

Ramping TGHT to 600A at 4A/min

TBHT at 230A, 3.0V


Tuesday, June 07, 2022, 16:41

TGHT= 740 A, 12.1V

TBHT= 232A, 3.0 V

OMEGA reading 1616C but questionable.  Will leave for 4 hours at 740A top TGHT.


Wednesday, June 08, 2022, 22:15

Early Wednesday morning the left TGHT bolt was found damaged.  The target leg was coated with bolt material rendering the Target inoperable.   

The Heatshield assembly was swapped and surfaces cleaned.  A "dummy" FEBIAD was installed to test if the system can withstand high current. 

The system was pumped down and ramped to 740A on TGHT at 4A/min.  It was then left at that current for 4 to 5 hours.

Currently starting rampdown at -2A/min to 0A. 

Photos of the incident attached in *eLog 580*.  IGP1= 5.7e-06 Torr

TGHT= 742A, 11.4V

  577   Thursday, June 02, 2022, 16:53 Aaron SchmidtTa44691-12LP-SISIn progressConditioning Ta#64

 Ta#64 LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.0254mm (0.0010") Measured.

Target density = 12.005 g/cm3

Target length = 3.35 cm

Total Mass = 40.2166 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven= 446 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (Not expanded). No Ta foil heat shield added


Final desired temperature = 1900C.

Thursday, June 02, 2022, 16:49: Roughing 

Thursday, June 02, 2022, 17:02: OMEGA slope = 0.98. 

Thursday, June 02, 2022, 17:10: TP1 on.

Thursday, June 02, 2022, 17:21: TP1 is up to speed. PS on. 


Friday, June 03, 2022, 05:22: Auto-ramping TGHT / TBHT to 500 / 200 A @ 2 A per min. Vacuum @ 1.78e-06T.

Friday, June 03, 2022, 08:59: TGHT / TBHT @ 424 / 200 A. Vacuum @ 3.42e-06T. Temperature @ 1318 C. Auto ramp ongoing.

Friday, June 03, 2022, 09:40: TGHT / TBHT @ 500 / 200 A. Vacuum @ 4.47e-06T. Temperature @ 1469 C. Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min

Friday, June 03, 2022, 10:47: TGHT / TBHT @ 580 / 230 A. Vacuum @ 6.26e-06T. Temperature @ 1620 C. Auto-ramping TGHT to 600 @ 2 A per min 

Friday, June 03, 2022, 11:08: TGHT / TBHT @ 600 / 230 A. Vacuum @ 6.54e-06T. Temperature @ 1655 C. Auto-ramping TGHT to 630 @ 2 A per min  

Friday, June 03, 2022, 11:30: TGHT / TBHT @ 630 / 230 A. Vacuum @ 7.73e-06T. Temperature @ 1708 C. Auto-ramping TGHT to 650 @ 2 A per min

Friday, June 03, 2022, 11:45: TGHT / TBHT @ 650 / 230 A. Vacuum @ 8.32e-06T. Temperature @ 1748 C. Auto-ramping TGHT to 660 @ 2 A per min

Friday, June 03, 2022, 11:53: TGHT / TBHT @ 660 / 230 A. Vacuum @ 8.83e-06T. Temperature @ 1755 C. Auto-ramping TGHT to 670 @ 2 A per min

Friday, June 03, 2022, 12:05: TGHT / TBHT @ 670 / 230 A. Vacuum @ 9.03e-06T. Temperature @ 1780 C. Auto-ramping TGHT to 680 @ 2 A per min

Friday, June 03, 2022, 12:11: TGHT / TBHT @ 680 / 230 A. Vacuum @ 9.14e-06T. Temperature @ 1795 C. Auto-ramping TGHT to 700 @ 2 A per min 

Friday, June 03, 2022, 12:23: TGHT / TBHT @ 700 / 230 A. Vacuum @ 9.50e-06T. Temperature @ 1822 C. Auto-ramping TGHT to 720 @ 2 A per min

Friday, June 03, 2022, 12:29: TGHT / TBHT @ 720 / 230 A. Vacuum @ 1.00e-05T. Temperature @ 1853 C. Auto-ramping TGHT to 730 @ 2 A per min

Friday, June 03, 2022, 12:36: TGHT / TBHT @ 725 / 230 A. Vacuum @ 1.04e-05T. Temperature @ 1860 C. Manually tap up TGHT to reach desired temperature

Friday, June 03, 2022, 13:04: TGHT / TBHT @ 760 / 230 A. Vacuum @ 1.07e-05T. Temperature @ 1901 C. Desired temperature reached

 

Friday, June 03, 2022, 13:13: Auto-cooling at 2 A per min. 

 


Monday, June 06, 2022, 07:07: PS off. BV1 closed & TP1 off.

Monday, June 06, 2022, 08:47: Venting. 

  576   Wednesday, May 18, 2022, 09:59 Darwin Ortiz RosalesSiC44692-9HP-FEBIADDoneT-220516 Sintering SiC

 Wednesday, May 18, 2022, 09:46

Total number of foils: 415 ( including 10 analysis discs on the right side of the container)

Total weight = 1580 g (includes heatshields and T bar)

Total length packed 17 cm (including 10 analysis discs that will be removed)

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Ta coated spring at  front (right) side

Initially to ramp TGHT and TBHT to 30A at 3 A/min

then continue to and slow down ramp when pressure begins to increase

max approx 700A on TGHT and 230A on TBHT (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -4 Torr

Bad vac at 5.00 e-2 Torr

 IGP1= 7.1 e-07 Torr at start of initial ramp.  Note, first real operation with new noisy Turbo Pump.


Wednesday, May 18, 2022, 10:18

Pressure increase observed starting around 60A.  Ramped to 70 A and will leave until pressure stabilizes

After about 30 minutes pressure dropped so ramped up to 90 A @1A/min on both TGHT and TBHT


Wednesday, May 18, 2022, 11:37

pressure spike around 90A.  will leave until pressure stabilizes 


Wednesday, May 18, 2022, 12:54  

start autoramp to 100A at 1A/min.  IGP1= 1.4e-4 Torr


Wednesday, May 18, 2022, 13:15

autoramp to 150A @1A/min 


Wednesday, May 18, 2022, 13:41

 At 110A another spike in pressure.  System waiting for good vacuum


Wednesday, May 18, 2022, 15:24

ramped to 150A on both TGHT and TBHT.  Ramping to 200 A at @A/min for both TGHT and TBHT

currently IGP1=  2.0e-4 Torr


Wednesday, May 18, 2022, 15:33  

Pressure still trending down; therefore will start ramp at 4A/min to 400 amp on TGHT and 230A to TBHT


Wednesday, May 18, 2022, 16:22 

Increasing ramp to 4A/min on TGHT


Wednesday, May 18, 2022, 17:26 

switched to 6A/min in 1A/10s increments on TGHT


Wednesday, May 18, 2022, 17:43 

Set final current to 730 A as per regression attached.

 

 

 

 

 

 

 


Wednesday, May 18, 2022, 17:54

Final current on TGHT = 740A, 11.9 V

OMEGA = 1775 C

TBHT = 230A, 

Will leave for 4 hours

 


Wednesday, May 18, 2022, 19:56

Temperature dropped so increased current to 755A for the remaining of the time.


Friday, May 20, 2022, 08:58

Final notes:  The difference between initial and final mass was 6 g as expected.  Slight coating on window of evaporator may explain apparent temperature drop.  Next time will keep current at projected setting.  The material looks good with slight overheating on the outer discs of left side.

 

 

  575   Tuesday, May 10, 2022, 14:43 Aaron Schmidt   MaintenanceActive TP removed / Swap / Slow start TP

 Tuesday, May 10, 2022, 14:42: TV551 Varian. SN: 202311 (Slightly active from BL1A - will not cross contaminate. Field only - Tagged) was removed as it was meant to be a temporary fix. Replacement (Refurbished) pump is to be installed. (Tomorrow - Use slow start function as per vacuum group) 


Thursday, May 12, 2022, 13:30: Agilent TP & hardware installed.

SN: IT21381010 

Thursday, May 12, 2022, 13:41: Roughing.

Thursday, May 12, 2022, 13:46: Halt. 


Friday, May 13, 2022, 07:05: Roughing. 

Friday, May 13, 2022, 07:18: TP1 on.

Friday, May 13, 2022, 07:23: Up to 14 KRPM. Pause/Halted startup (Whining?). Slow start w/ vacuum group.

Process to perform a TP slow start:

- Hold both top buttons on the controller for about 3 seconds

- Right Yes/No left to continue. 

- Advance to soft start - 20 min. 

- Back to remote start & go.

Friday, May 13, 2022, 08:26: TP1 on w/ slow start.

Friday, May 13, 2022, 08:39: 13 KRPM & climbing.

Friday, May 13, 2022, 09:10: TP at full speed. 38 KRPM. 0.5A 9w. This pump whines, but is operating fine. Likely will switch again when another is available. (It appears to have been dropped, Noted by Edi. Likely when shipped) 

Friday, May 13, 2022, 09:14: TP off. Slow start function off. Back to normal function. 

  574   Monday, April 25, 2022, 08:31 Ferran Boix PamiesEmptyTa boat used for annealingTARGET BOATDonePEEK sample test 2

Setup in vacuum over the weekend.

Monday, April 25, 2022, 08:31 IGP1:6.7e-7T . Ramping up 1A/10s to 500A. 

Monday, April 25, 2022, 10:05 500A reached, waiting 1h. TC at 50degC

Monday, April 25, 2022, 10:59 TC at 58degC. Ramping down 1A/10s to 0 A. 

Monday, April 25, 2022, 13:37 TGHT at 0A , venting system. 

  573   Thursday, April 21, 2022, 09:45 Darwin Ortiz RosalesTaC42218-2LP-IG-LISDoneTaC coating

Thursday, April 21, 2022, 09:43

TaC coated Target container was placed in Evaporator 2 yesterday and left pressuring down.

Ta Heatshields: 3

Target temperature on OMEGA = 1800-1850 C

OMEGA slope: 0.990

Target time at temperature = 4 hours

Target final TBHT current: 230A

Approximate final TGHT current: 420A (will adjust manually)

Heating autoramp started @ ~2A/min on both TGHT and TBHT

initial IGP1 = 9.3e-7 Torr

 


Thursday, April 21, 2022, 10:38

Pressure trending down after peak.  Start autoramp at 1A/min to 50A on both TGHT and TBHT.


Thursday, April 21, 2022, 10:56

Pressure continues to decrease.  Will ramp up faster @4A/min to 90A for both TGHT and TBHT.


Thursday, April 21, 2022, 11:07

Second peak has  begun to form .  Will keep at 90A awaiting stabilization


Thursday, April 21, 2022, 11:35

pressure stable.  Continue to autoramp at 1A/min and if pressure stable increase ramp to 4A/min


Thursday, April 21, 2022, 11:49

small peak observed and stabilizing.  Autoramp @ 6A/min to 400A on TGHT and to 230A on TBHT


Thursday, April 21, 2022, 12:35

 

Regression plot .  1800C should be reached ~1800C. 


Thursday, April 21, 2022, 12:44

Target current reached. 

OMEGA = 1762 C

Will manually bump current to 415 A

OMEGA = 1802 @ 415 A @ 12:51 pm


Thursday, April 21, 2022, 16:50

 OMEGA=1823 C

IGP1= 2.9e-06 Torr

TGHT= 417 A, 7.2 V

TBHT= 232A, 3.0V

Rampdown will start at -2A/min for both TGHT and -1A/min TBHT

 

  572   Sunday, April 17, 2022, 10:37 Ferran Boix PamiesEmptyTa boat used for annealingTARGET BOATDonePEEK samples heat test

 Thursday, April 14, 2022, 10:36 Setup, PEEK samples installed on heatshield with TC. Pump down over the weekend.

Sunday, April 17, 2022, 10:37 Vacuum 3e-7T, ramp up TGHT 1A/10s to 500A 

Sunday, April 17, 2022, 12:00 500A reached, waiting 1hour. TC at 42degC. 

Sunday, April 17, 2022, 12:57 after 1h, TC at 45degC. Ramping down 1A/10s. Vacuum 2.7e-6Torr.

Sunday, April 17, 2022, 14:33 ramped down to 0A. Turning off turbo and venting. 

  571   Tuesday, April 12, 2022, 13:41 Aaron Schmidt   MaintenanceNew Flex - line HS installed

Old HS sprang a leak in the copper tubing.  

HS#44378-15

Tuesday, April 12, 2022, 13:35: Roughing. 

Tuesday, April 12, 2022, 13:49: TP1 switched on. 

Tuesday, April 12, 2022, 13:57: TP1 stable (green).

Tuesday, April 12, 2022, 14:10: Vacuum @ 3.71e-05T & dropping.

Tuesday, April 12, 2022, 14:11: HS waterline opened. 

Tuesday, April 12, 2022, 14:12: Vacuum @ 3.32e-05T.

Tuesday, April 12, 2022, 14:22: Vacuum @ 2.19e-05T (Stable).

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