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Message ID: 592     Entry time: Thursday, September 22, 2022, 07:15
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: Done 
Subject: TaC coated endcaps and spring sintering 

Thursday, September 22, 2022, 07:13

Each endcap is separated with a disc of graphite foil and rolled into 3 packs of 4 within a foil envelope in a target boat.

There are also 2 coated springs

The boat is wrapped with 3-layers of Ta heatshields.

Chamber pumped down over previous night

Good vacuum = 5.0e-04 Torr

bad vacuum = 5.e-02 Torr

OMEGA slope = 0.99

Will ramp TGHT up to 40 A then autoramp to 400A at 1A/min.

Final desired temperature on OMEGA (tap)= 1800C

IGP1= 3.8e-7 Torr

 


Thursday, September 22, 2022, 10:08

TGHT= 168A,

IGP1= 4.7E-07=6Torr

Increased  ramp to 2A/min


Thursday, September 22, 2022, 12:08

TGHT= 400A, 6.7V

OMEGA= 1604C

Continuing autoramp to 450A @2A/min


Thursday, September 22, 2022, 12:36

TGHT=450A, 7.7V

OMEGA=1700C

Tapping to 1800C manually


Thursday, September 22, 2022, 12:54

OMEGA = 1750C at 505A, 8.8 V 

Tapped to 540A, 9.5V

Will leave there for two more hours

OMEGA= 1800+/- 10 C


Thursday, September 22, 2022, 15:00

TGHT = 540A, 9.3V

OMEGA= 1713

start rampdown at-2A/min
 


Friday, September 23, 2022, 09:49

IGP1= 4.0e-7 Torr

Will dismount container


Saturday, September 24, 2022, 09:10

Endcaps looked good.  The front spring sintered onto container and not usable.  signs of overheating.

 

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