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Entry  Wednesday, June 08, 2022, 10:00, Flora Wu, , boat, , Done, carbonize PAN 10% discs 
    Reply  Thursday, June 09, 2022, 19:20, John Wong, , boat, , Done, carbonize PAN 10% discs evap2-screenshot_01.PNGevap2-screenshot_02.pngevap2-screenshot_3.pngtemp-current-plot.xlsxevap2-screenshot_04.PNG
Message ID: 579     Entry time: Wednesday, June 08, 2022, 10:00     Reply to this: 581
Author: Flora Wu 
Target Material:  
Target Oven W.O#: boat 
Source:  
Status: Done 
Subject: carbonize PAN 10% discs 

Thursday, June 09, 2022, 11:25

Total number of foils: 14 electrospun fiber pellets 

Total weight = 208.3 g

container has 3 Ta heat shields.

Desired temperature at 1800 C

Omega slope set at 0.990 

Good vac = 3.0e-5 Torr,

Bad vac = 5.0e-5 Torr.

Pumping down in progress


 Thursday, June 09, 2022, 11:25

chamber pumped down below 5e-5

initiate auto ramping, 1A/min ----> 100 A


 (see eLog 581)

 

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