Monday, October 25, 2021, 11:52

Ta IGLIS tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

Good vacuum = 3.00 e-3 Torr

Bad vacuum = 5.00 e-2 Torr

Initial total weight = 439.0 g

Final weight after sintering = 438.8 g

Tuesday, October 26, 2021, 07:18 

IGP1= 9.2 e-07 Torr

Will ramp to 50A at 1A/min on both TGHT and TBHT.

Tuesday, October 26, 2021, 08:37 

IGP1= 3.0 e-05 Torr

TGHT= 50.2 A, 0.6 V

TBHT = 49.4 A, 0.5 V

Will allow pressure to drop further then start further ramp up

Tuesday, October 26, 2021, 14:36

TGHT =  100 A, 1.3 V

TBHT = 99 A, 1.0 V

IGP1 = 3.e-5 Torr

ramp up TGHT to 400 A and TBHT to 230 A at 1.5 A/ min

Tuesday, October 26, 2021, 18:46 

 Will keep at 430A on TGHT and 230A on TBHT for 4 hours.

OMEGA reading = 1653  C is suspicious based on previous coating.  

Tuesday, October 26, 2021, 23:05

TGHT = 430.5 A, 6.9 V

TBHT = 232.09A, 2.8 V

IGP1= 8.8e-06 Torr

Start cooling THGT at -2A/min and TBHT at -1A/min 

 Wednesday, March 09, 2022, 06:25

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

Good vacuum = 3.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 1.2 e-06 Torr

Start autoramp @1A/min to 60 A

Wednesday, March 09, 2022, 09:29

 TGHT= 60 A 0.67 V

TBHT = 60A 0.59V

IGP1= 1.77e-6 Torr

autoramp @ 2A/min to 120 A and monitor (both TGHT and TBHT)

Wednesday, March 09, 2022, 10:19

IGP1 was increasing to fast.  Manually lowered current to 105A on both TGHT and TBHT.

Will allow pressure to stabilize

Plant group requested maintenance work for EF12/13

Therefore, keeping system as is until further instructions from plant group.

Thursday, March 10, 2022, 15:18

Will resume ramp up to 120 A for both TGHT and TBHT @ 1A/min

 IGP1= 6.4 e-07 Torr

Thursday, March 10, 2022, 15:30

Increase ramp rate to 2A/min 

Thursday, March 10, 2022, 17:41

@ 245 A TGHT and 230A TBHT ramp back down to 100 A for both as OMEGA not displaying Temperature.  Will need to go in tomorrow to fix OMEGA 

Friday, March 11, 2022, 14:25

Ramping at 2A/min to 230A for both TGHT and TBHT

Friday, March 11, 2022, 15:17

IGP1= 1.23e-6 Torr

Continue Ramping TGHT @ 3A/min to 400 A keep TBHT at 230A

Friday, March 11, 2022, 22:22

@ TGHT 725 A 1800 C was reached on OMEGA

Kept there since 7:20 pm.  Start rampdown at 11:20 pm.

Friday, March 11, 2022, 23:19  

 IGP1= 6.9e-6 Torr

OMEGA= 1805C

TGHT= 725 A, 10.9V

TBHT= 232A, 3.1V

Start rampdown at -2A/min on TGHT and -1A/min for TBHT

Wednesday, March 23, 2022, 10:49

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3.5 layers) (two pieces around the fins only and 3 layers around the whole )

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).  TGHT expected to reach desired Temperature @~700A

Evap 2 was pumped down over previous night

Good vacuum = 3.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 1.2 e-06 Torr

Start autoramp @0.5 A/min to 60 A

 Wednesday, March 23, 2022, 11:37

Increase autoramp to 1A/min to 60A for both TGHT and TBHT

Wednesday, March 23, 2022, 12:24

Pressure increasing at 60A so will leave at this current until pressure drops

Wednesday, March 23, 2022, 13:32

IGP1 = 2.9e-06 Torr

Will autoramp at 0.5A/min to 90A both TGHT and TBHT

Thursday, March 24, 2022, 16:35

1800C reached at 724A TGHT .  TBHT @ 230A.  Will keep at this temperature for 4 hours. 

Thursday, March 24, 2022, 20:20

 IGP1 = 6.9 e-06 Torr

OMEGA= 1828 C

TGHT = 724 A, 11.6 V

TBHT = 232.8 A, 3.1 V

Will start ramp-down at 2035 @ -2A/min TGHT and -1A/min TBHT

Thursday, April 21, 2022, 09:43

TaC coated Target container was placed in Evaporator 2 yesterday and left pressuring down.

Ta Heatshields: 3

Target temperature on OMEGA = 1800-1850 C

OMEGA slope: 0.990

Target time at temperature = 4 hours

Target final TBHT current: 230A

Approximate final TGHT current: 420A (will adjust manually)

Heating autoramp started @ ~2A/min on both TGHT and TBHT

initial IGP1 = 9.3e-7 Torr

Thursday, April 21, 2022, 10:38

Pressure trending down after peak.  Start autoramp at 1A/min to 50A on both TGHT and TBHT.

Thursday, April 21, 2022, 10:56

Pressure continues to decrease.  Will ramp up faster @4A/min to 90A for both TGHT and TBHT.

Thursday, April 21, 2022, 11:07

Second peak has  begun to form .  Will keep at 90A awaiting stabilization

Thursday, April 21, 2022, 11:35

pressure stable.  Continue to autoramp at 1A/min and if pressure stable increase ramp to 4A/min

Thursday, April 21, 2022, 11:49

small peak observed and stabilizing.  Autoramp @ 6A/min to 400A on TGHT and to 230A on TBHT

Thursday, April 21, 2022, 12:35

Regression plot .  1800C should be reached ~1800C. 

Thursday, April 21, 2022, 12:44

Target current reached. 

OMEGA = 1762 C

Will manually bump current to 415 A

OMEGA = 1802 @ 415 A @ 12:51 pm

Thursday, April 21, 2022, 16:50

 OMEGA=1823 C

IGP1= 2.9e-06 Torr

TGHT= 417 A, 7.2 V

TBHT= 232A, 3.0V

Rampdown will start at -2A/min for both TGHT and -1A/min TBHT

Wednesday, June 29, 2022, 10:07

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

OMEGA slope= 0.990

Good vacuum = 3.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 1.2 e-06 Torr

Start autoramp @2A/min to 80 A then autoramp heat @1A/min to 150 A.  Then autoramp TGHT to 675A and TBHT to 230A.1

Wednesday, June 29, 2022, 10:13

Chamber isolation performed and no change of pressure observed.

Water leak test performed and no pressure change detected.

Starting ramp up

Wednesday, June 29, 2022, 13:23

Ramping to 675A on TGHT and 230A on TBHT @ 2A/min

Ramped TGHT to 680A, 10.6V  and held for 4 hours

Wednesday, June 29, 2022, 21:52

Started rampdown @-2A/min TGHT and -1A/min TBHT

Thursday, September 01, 2022, 10:34

The coated container was wrapped in three Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp starged at 2A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-05 Torr

Bad vacuum = 5.0E-04 Torr

Thursday, September 01, 2022, 12:39

Has been stabilizing at 40A on both heaters.

Starting 1A/min autoramp to 80A

A discrepancy between setpoint and readback currents was observed for both TGHT and TBHT.  The difference is substancial and warrants investigation.  This process will be paused until further notice

Tuesday, September 06, 2022, 14:45

Controls has been troubleshooting EVAP2.  In the process TBHT has been damaged. Arthur will take a look at it ASAP and his group will try and fix it tomorrow. 

Regarding our initial problem, it appears that when an electrical safety box was installed, the copper water lines connected to output terminals of the power supply, were moved so that they were in contact with the evaporator cage.  See the figure below.

Thursday, September 08, 2022, 12:47

 Target has been removed and a new test target (HP-FEBIAD) has been placed inside.  System left to generate enough vacuum and then testing will be performed.

Friday, September 09, 2022, 15:58

System was tested and all seems good.  This coat/sintering will continue after conditioning of graphite material

Saturday, September 24, 2022, 09:13

Continuation of process. 

IGP1= 4.3e-07 Torr

ramping @ 1A/min to 230 A on both TGHt and TBHT

Saturday, September 24, 2022, 16:28

ramped to 430A, 7.2V on TGHT and 233A, 4.2V on TBHT.  Will leave until 7 pm.

Saturday, September 24, 2022, 19:44

Starting rampdown @-2A/min TGHT -1A/min TBHT

camera offline

IGP1= 1.2e-6 Torr

Monday, September 26, 2022, 09:41

IGP1=2.2e-07 Torr.  Shutting off TBHT and TGHT.

Thursday, September 29, 2022, 09:53

Final notes: coating looks good .  Probably 3 hours at final temperature is better to prevent material degradation.

Thursday, September 22, 2022, 07:13

Each endcap is separated with a disc of graphite foil and rolled into 3 packs of 4 within a foil envelope in a target boat.

There are also 2 coated springs

The boat is wrapped with 3-layers of Ta heatshields.

Chamber pumped down over previous night

Good vacuum = 5.0e-04 Torr

bad vacuum = 5.e-02 Torr

OMEGA slope = 0.99

Will ramp TGHT up to 40 A then autoramp to 400A at 1A/min.

Final desired temperature on OMEGA (tap)= 1800C

IGP1= 3.8e-7 Torr

Thursday, September 22, 2022, 10:08

TGHT= 168A,

IGP1= 4.7E-07=6Torr

Increased  ramp to 2A/min

Thursday, September 22, 2022, 12:08

TGHT= 400A, 6.7V

OMEGA= 1604C

Continuing autoramp to 450A @2A/min

Thursday, September 22, 2022, 12:36

TGHT=450A, 7.7V

OMEGA=1700C

Tapping to 1800C manually

Thursday, September 22, 2022, 12:54

OMEGA = 1750C at 505A, 8.8 V 

Tapped to 540A, 9.5V

Will leave there for two more hours

OMEGA= 1800+/- 10 C

Thursday, September 22, 2022, 15:00

TGHT = 540A, 9.3V

OMEGA= 1713

start rampdown at-2A/min
 

Friday, September 23, 2022, 09:49

IGP1= 4.0e-7 Torr

Will dismount container

Saturday, September 24, 2022, 09:10

Endcaps looked good.  The front spring sintered onto container and not usable.  signs of overheating.

Monday, October 17, 2022, 10:03

The coated container was wrapped in 4 Ta foil heatshields. (The 4 shields appear to work well)

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp started at 2A/min on both TGHT and TBHT to40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Monday, October 17, 2022, 12:45

Autoramping @4A/min on both TGHT and TBHT to 400 and 30A respectively

Monday, October 17, 2022, 12:56

slowed ramp to 2A/min on both heaters as pressure was increasing too fast.  (1A/30s).

Monday, October 17, 2022, 13:30

increased ramp rate to 4A/min on TGHT as TBHT is already at 230A

Monday, October 17, 2022, 14:16

leaving at TGHT : 393A, 6.5V ; TBHT  233A, 4.2V

OMEGA reads 1864C.  Will start rampdown at 6:17 pm

Monday, October 17, 2022, 18:16

OMEGA read 1875C at max and now reads 1856C

starting ramp down at -2A/min TGHT and -1A/min TBHT

Final IGP1= 1.4e-06 Torr

Tuesday, October 18, 2022, 09:37

IGP1= 2.72e-7 Torr

Turning heaters off on epics and turning vacuums off. 

Tuesday, October 25, 2022, 12:18

Container wrapped in 4 Ta foil heatshields

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp started at 2A/min on both TGHT and TBHT to40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Wednesday, October 26, 2022, 07:07

IGP1= 7.5e-7 Torr

start ramp at 2A/min to 40A

Ramped at 1A/min to 120A then held until pressure drop.  Then ramped @ 4A/min to 400A on TGHT.

Wednesday, October 26, 2022, 14:09 

Manually rampted TGHT to 415A, 6.9V will hold for 4 hours 

OMEGA reads 1870 C initially

Thursday, October 27, 2022, 09:44

was held for 5 hours due to technical issues but should be ok.

OMEGA @ time of rampdown = 1830C

Rampdown @-2A/min TGHT and -1A/min TBHT

IGP1= 3.5e-07 Torr

Friday, October 28, 2022, 07:58

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 IGP1 initial = 4.5e-07 Torr

Friday, October 28, 2022, 10:50

after reaching 120A and leaving until pressure drop, autoramp at 2.5A/30s (5A/min) towards 400A TGHT and 230A TBHT.

Friday, October 28, 2022, 11:22

OMEGA= 1890 @ 412A, 7.1 V on TGHT

Leaving for 4 hours

Monday, November 07, 2022, 14:24

The coated container tube was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 IGP1 initial =

Thursday, November 10, 2022, 07:40

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 IGP1 initial = 2.8e-07 Torr

Thursday, November 10, 2022, 10:31

 TGHT 230A 3.4V and TBHT at 230A , 3.9V

Continue ramp up for TGHT at 4A/min (2A/30s) to 380A

Thursday, November 10, 2022, 11:30

OMEGA =1886 C @ 430A, 7.1V TGHT; will leave for 4 hours

Thursday, November 10, 2022, 15:43

rampdown at -2A/min TGHT and -1A/min TBHT

Thursday, November 17, 2022, 08:11

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= N/A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on  TGHT  40A

Then at 2A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 IGP1 initial = 2.7e-07 Torr

Thursday, November 17, 2022, 10:41

OMEGA=1897C at 358A, 6.0V

Will ramp down at 230 pm

Thursday, November 17, 2022, 14:34

starting rampdown at -2A/min

OMEGA reads 1865C and IGP1=7.6e-07 Torr

Friday, November 18, 2022, 15:08

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1860-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 2A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

leaving to pressure down over weekend

Sunday, November 20, 2022, 12:11

start heatup IGP1=1.63e-07 Torr

Sunday, November 20, 2022, 14:21

OMEGA= 1900 at 395A, 6.6V on TGHT

Will leave until 6;20 pm

Tuesday, November 22, 2022, 14:58

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1860-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 2A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

leaving to pressure down. 

 Wednesday, November 22, 2022, 19:10 

OMEGA = 1942 C @ 396A on TGHT

lowered to 386A to 1900 and left for 4 hours.

After four hours, started rampdown at-2A/min TGHT and -1A/min TBHT

4 TaC coated springs and 4 Tac coated caps loaded into a target boat.

Target boat wrapped in 4 Ta heatshields

Target boat type was with endcaps at both ends.

Left in Evap2 over previous night to depressurize.

Target temperature= 1850-1900C for 4 hours

Good vacuum = 5e-04 Torr

Bad vacuum = 5e-02 Torr

Friday, December 16, 2022, 10:01

Heated @1A/min to 100A on TGHT

Then heated 2A/min to 120A

Friday, December 16, 2022, 10:08

started autoramp @4A/min  to 300A

Friday, December 16, 2022, 11:15

TGHT=450 A, 7.6 V

OMEGA= 1863 C

IGP1= 7.2e-06 Torr

Will keep for 4 hours

Monday, December 19, 2022, 10:30

Sintering was perfect.  Repeat same configuration next time.

Thursday, February 23, 2023, 18:20

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers) and 1 under layer that doesn't cover the middle section.

Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down to 5e-06 Torr range

OMEGA slope= 0.990

Good vacuum = 5.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1=2.5 e-06 Torr

Start autoramp @1A/min to 80 A then autoramp heat @1A/min to 150 A.  Then autoramp TGHT to approx 675A and TBHT to 230A.1

Friday, February 24, 2023, 09:10

heated overnight @0.5 A/min to 400 A.  Then started heating at 1A/min to 600 A while taking readings for current/Temp regression.

regression so far points to 682A to get to 1800C.  Will continue taking readings and possible heat to 1850 C. 

Friday, February 24, 2023, 09:43

autoramping to 690A at 1A/min

Friday, February 24, 2023, 11:24

ramping manually to 690A from 650A

Friday, February 24, 2023, 11:32

4 hours at 330pm

TGHT 492A, 10.6V

TBHT = 230A, 3.2V

IGP1=5.11e-06 Torr

OMEGA =1840 C

Friday, February 24, 2023, 15:36

TGHT = 692A, 10.6V

TBHT = 230 A, 3.2V

OMEGA = 1835 C

IGP1= 2.4e-06 Torr

Starting rampdown at -2A/min TGHT and -1A/min TBHT

Thursday, March 16, 2023, 13:38

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1860-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 Thursday, March 16, 2023, 22:21

Started ramping TGHT and TBHT @ 1.5A/min to 387 A and 230A respectively.

IGP1 initial = 9.6 e-07 Torr

Cooling projected at 6:48 am tomorrow. 

Friday, March 17, 2023, 06:59

Final IGP1= 1.6e-o6 Torr

Started rampdown @-2A/min TGHT and -1A/min TBHT

Coating looks good uniformely.

OMEGA 1850 C (was 1868 initially)

TGHT was 387A, 6.6 V and TBHT was 230A, 4.1 V

Coating very nice

Tuesday, April 04, 2023, 12:48

Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers + 1 inner layer around fins including center fins)

Desired temperature = 1850 C , TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

OMEGA slope= 0.990

Good vacuum = 5.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

OMEGA target temp = 1850 C

Wednesday, April 05, 2023, 07:37

IGP1= 4.3e-07 Torr

starting autoramp @ 1A/min to 230A on both TGHT and TBHT

Wednesday, April 05, 2023, 10:56

Starting Autoramp at 4A/min to 400 A on TGHT

Wednesday, April 05, 2023, 14:14

OMEGA Reached 1877C  @ 743A, 11.3V TGHT

rampdown  @ 6:00 pm

Wednesday, April 05, 2023, 14:38

Decreased TGHT current to 736A because temperature was creeping up

rampdown was started at 6:05 pm

Final pressure at 0 V - 1.7e-07 Torr

Wednesday, April 12, 2023, 09:53

The coated container was wrapped in 3 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= N/A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on  TGHT  40A

Then at 2A/min  to 90 A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 IGP1 initial = 4.7e-07 Torr

Wednesday, April 12, 2023, 10:46

heating at 2A/min to 90A

Wednesday, April 12, 2023, 11:18

Autoramping at 2A/min to 230A

Wednesday, April 12, 2023, 11:53

Autoramping at 4A/min to 230 A

Wednesday, April 12, 2023, 13:57

Autoramping to 380A

Wednesday, April 12, 2023, 14:07

manually adjusted TGHT to 384A. 6.6 V

OMEGA reads 1859 C.   Leaving for 4 hours. 

Wednesday, April 12, 2023, 18:36

Started rampdown at -2A/min