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Message ID: 603     Entry time: Friday, November 18, 2022, 15:13
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 45220-1 
Source: LP-SIS 
Status: Done 
Subject: TaC coating sintering 

Friday, November 18, 2022, 15:08

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1860-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 2A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

leaving to pressure down over weekend

 


Sunday, November 20, 2022, 12:11

start heatup IGP1=1.63e-07 Torr

 


Sunday, November 20, 2022, 14:21

OMEGA= 1900 at 395A, 6.6V on TGHT

Will leave until 6;20 pm

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