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Message ID: 598     Entry time: Friday, October 28, 2022, 07:59
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 45220-6 
Source: LP-SIS 
Status: Done 
Subject: TaC coating sintering 

Friday, October 28, 2022, 07:58

The coated container was wrapped in four Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-02 Torr

Bad vacuum = 5.0E-04 Torr

 IGP1 initial = 4.5e-07 Torr


Friday, October 28, 2022, 10:50

after reaching 120A and leaving until pressure drop, autoramp at 2.5A/30s (5A/min) towards 400A TGHT and 230A TBHT.


Friday, October 28, 2022, 11:22

OMEGA= 1890 @ 412A, 7.1 V on TGHT

Leaving for 4 hours

 

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