Monday, October 25, 2021, 11:52
Ta IGLIS tube was coated with TaC and wrapped with Ta heat-shields (3 layers)
Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).
Evap 2 will be pumped down over previous night
Good vacuum = 3.00 e-3 Torr
Bad vacuum = 5.00 e-2 Torr
Initial total weight = 439.0 g
Final weight after sintering = 438.8 g
Tuesday, October 26, 2021, 07:18
IGP1= 9.2 e-07 Torr
Will ramp to 50A at 1A/min on both TGHT and TBHT.
Tuesday, October 26, 2021, 08:37
IGP1= 3.0 e-05 Torr
TGHT= 50.2 A, 0.6 V
TBHT = 49.4 A, 0.5 V
Will allow pressure to drop further then start further ramp up
Tuesday, October 26, 2021, 14:36
TGHT = 100 A, 1.3 V
TBHT = 99 A, 1.0 V
IGP1 = 3.e-5 Torr
ramp up TGHT to 400 A and TBHT to 230 A at 1.5 A/ min
Tuesday, October 26, 2021, 18:46
Will keep at 430A on TGHT and 230A on TBHT for 4 hours.
OMEGA reading = 1653 C is suspicious based on previous coating.
Tuesday, October 26, 2021, 23:05
TGHT = 430.5 A, 6.9 V
TBHT = 232.09A, 2.8 V
IGP1= 8.8e-06 Torr
Start cooling THGT at -2A/min and TBHT at -1A/min |