4 TaC coated springs and 4 Tac coated caps loaded into a target boat.
Target boat wrapped in 4 Ta heatshields
Target boat type was with endcaps at both ends.
Left in Evap2 over previous night to depressurize.
Target temperature= 1850-1900C for 4 hours
Good vacuum = 5e-04 Torr
Bad vacuum = 5e-02 Torr
Friday, December 16, 2022, 10:01
Heated @1A/min to 100A on TGHT
Then heated 2A/min to 120A
Friday, December 16, 2022, 10:08
started autoramp @4A/min to 300A
Friday, December 16, 2022, 11:15
TGHT=450 A, 7.6 V
OMEGA= 1863 C
IGP1= 7.2e-06 Torr
Will keep for 4 hours
Monday, December 19, 2022, 10:30
Sintering was perfect. Repeat same configuration next time. |