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Message ID: 597     Entry time: Tuesday, October 25, 2022, 12:25
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 44139-15-SK 
Source: LP-SIS 
Status: Done 
Subject: TaC coating sintering 

Tuesday, October 25, 2022, 12:18

Container wrapped in 4 Ta foil heatshields

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp started at 2A/min on both TGHT and TBHT to40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


Wednesday, October 26, 2022, 07:07

IGP1= 7.5e-7 Torr

start ramp at 2A/min to 40A


Ramped at 1A/min to 120A then held until pressure drop.  Then ramped @ 4A/min to 400A on TGHT.


Wednesday, October 26, 2022, 14:09 

Manually rampted TGHT to 415A, 6.9V will hold for 4 hours 

OMEGA reads 1870 C initially


Thursday, October 27, 2022, 09:44

was held for 5 hours due to technical issues but should be ok.

OMEGA @ time of rampdown = 1830C

Rampdown @-2A/min TGHT and -1A/min TBHT

IGP1= 3.5e-07 Torr

 

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