Wednesday, December 06, 2023, 09:47

Target number of foils:370

Analysis discs 16 A and 16B interspersed on the end further from the laser

A are discs produced using new method and B are discs produced using milling.

Total length packed 16 cm (excluding the analysis discs)

container has 3 Ta heat shields (one inner around fins and center block, new type of 1st shield made up of three pieces)

No endcaps inserted to facilitate out-gassing

Ta coated spring at  front end

ramp to 120A @ 1A/min TGHT and to 120A on TBHT hold there until pressure drop, then ramp to 500A on TGHT and 230A TBHT.

max approx 700A on TGHT and 230A on TBHT (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 5.00 e -4 Torr

Bad vac at 5.00 e-2 Torr

 IGP1= 1e-06 Torr at start of initial ramp.

Wednesday, December 06, 2023, 09:56

System left to drop pressure over previous night and now at 120A.  waiting for pressure drop.

Wednesday, December 06, 2023, 11:18

increased ramp rate to 2A/min

Wednesday, December 06, 2023, 14:41

increased ramp to 3A/min on TGHT and stopping to allow pressure to stabilize before taking temperature readings

Top temperature 1800C at 710 A but started dropping.  Increased current to 750A and left there for 4 hours.

Cool down at -2A/min TGHT and -1A/min TBHT

Monday, November 06, 2023, 09:59

The coated container was wrapped in 4 Ta foil heatshields.

Vacuum IGP1 initial =3.1 e-07 Torr

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 2A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 Monday, November 06, 2023, 14:07

OMEGA =1852 C

IGP1= 3.14e-06 Torr

TGHT= 399A, 6.6V

TBHT= 233A, 4.1V

Tuesday, November 07, 2023, 12:28

Cooled down previous evening and took out today.

rampdown was @-2A/min for TGHT and -1A/min TBHT

Friday, October 20, 2023, 07:20

The coated container was wrapped in 4 Ta foil heatshields.

Vacuum IGP1 initial = 9.9 e-07 Torr

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Friday, October 20, 2023, 07:24

Starting initial ramp

Vacuum IGP1 initial = 9.9 e-07 Torr

Friday, October 20, 2023, 08:55

After initial pressure bump continued heating at 1A/min to 120A to observe any other possible pressure bump.

Friday, October 20, 2023, 09:05

increased ramp to 4A/min to 400 TGHT and 230 TBHT

Friday, October 20, 2023, 09:35

OMEGA=1280 C

TGHT= 221.5 A, 3.24V 

TBHT=228.9, 3.9V

Friday, October 20, 2023, 10:22

OMEGA 1852 C at TGHT = 390A, 6.5 V ; TBHT = 232 A, 4.0 V

Will leave for 4 hours

Friday, October 20, 2023, 14:16

About to start rampdown

TGHT @ -2A/min

TBHT@ -1A/min

Final OMEGA = 1840 C

IGP1 = 1.83e-06 Torr

Ta#(Spare) LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.033mm (0.0013") avg Measured. 

Target material batch: Ta 2023-1  Mt'l PO# TR-2022-03028

Target density = 12.515 g/cm3

Target length = 4.97 cm

Total Mass = 62.202 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven =  461g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Was labelled Ta#67 until the Thin foil target 45447-14 became so.

Thursday, October 05, 2023, 12:44: Roughing. 

Thursday, October 05, 2023, 13:10; TP1 on.  

Thursday, October 05, 2023, 13:11: TGHT / TBHT test. Tap up to 5 / 5 A & back to 0 A. Ok.

Thursday, October 05, 2023, 13:13: Slope Set @ 0.98 

Friday, October 06, 2023, 05:54: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. 

Friday, October 06, 2023, 11:50: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1716 C. Vacuum @ 2.76e-06T.

Friday, October 06, 2023, 12:20: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1809 C. Vacuum @ 3.77e-06T.

Friday, October 06, 2023, 12:37: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 665 A @ 2 A per min (650 A w/ offset). Temperature @ 1844 C. 

Friday, October 06, 2023, 12:53: Tapped up to TGHT / TBHT @ 670/ 230 A (657 / 233 A). Temperature @ 1880 C. Vacuum @ 4.94e-06T. 

Friday, October 06, 2023, 12:57: Tapped TGHT to 675.  TGHT / TBHT @ 675 / 230 A (662 / 233 A). Temperature @ 1889 C. Vacuum @ 5.03e-06T. 

Friday, October 06, 2023, 13:00: Tapped TGHT to 682.  TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1901 C. Vacuum @ 5.46e-06T. Desired Temperature reached.

Friday, October 06, 2023, 13:01: Auto-cooling @ 2 A per min.

Tuesday, October 10, 2023, 08:37: PS & TP off. 

 Ta#66 LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.033mm (0.0013") avg Measured. 

Target material batch: Ta 2023-1  Mt'l PO# TR-2022-03028

Target density = 12.446 g/cm3

Target length = 5.0 cm

Total Mass = 62.230 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Desired temperature 1900C

Wednesday, September 20, 2023, 14:18: Roughing. 

Wednesday, September 20, 2023, 14:35: TP Started. 

Wednesday, September 20, 2023, 14:43: TP on. 

Wednesday, September 20, 2023, 14:45: TGHT / TBHT raised to 5 / 5 A & lowered. Quick check ok. 

Thursday, September 21, 2023, 07:47: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Vacuum @ 8.30e-07T.

Thursday, September 21, 2023, 09:54: Slope set to 0.98 

Thursday, September 21, 2023, 13:42: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1748 C. Vacuum @ 2.47e-06T.

Thursday, September 21, 2023, 14:10: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1843 C. Vacuum @ 3.30e-06T.

Thursday, September 21, 2023, 14:23: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 660 A @ 2 A per min (648 A w/ offset). Temperature @ 1879 C. Vacuum @ 3.77e-06T.

Thursday, September 21, 2023, 14:29: Tapped TGHT to 662.  TGHT / TBHT @ 662 / 230 A (649 / 233 A). Temperature @ 1903 C. Vacuum @ 4.08e-06T. Desired Temperature reached.

Thursday, September 21, 2023, 14:33: Auto-cooling started @ 1 A per min.

Monday, September 25, 2023, 08:09: Turbo pump off. 

Tuesday, September 12, 2023, 09:51

The coated container was wrapped in 3 Ta foil heatshield and left in evap2 over night to attain vacuum.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~700A (adjustable)

Heating autoramp starged at 1A/min on  TGHT  and TBHT to 120A

Then at 2 A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Initial IGP1= 2.7e-06 Torr

Tuesday, September 12, 2023, 7:00

Started autoramp @1A/min to 120A on both TGHT and TBHT

Tuesday, September 12, 2023, 09:53

Heating ramp set to 230A for both TGHT and TBHT.  Rate at 2A/min for both heaters.

Tuesday, September 12, 2023, 11:21

Continued ramp on TGHT at 2A/min to 335A and now setting to 3A/min (1.5A/30s)

Tuesday, September 12, 2023, 11:47

Continue ramping @3A/min on TGHT

 Tuesday, September 12, 2023, 13:33

Reached 1840 C at TGHT =677A and 10.5V

Will keep for 4 hours

Thursday, August 31, 2023, 07:07

The coated container was wrapped in 3 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~500A (adjustable)

Heating autoramp starged at 1A/min on  TGHT  and TBHT to 120A

Then at 2 A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Initial IGP1= 7.7e-07 Torr

Thursday, August 31, 2023, 12:29

OMEGA=1238 C

IGP1=1.4e-06 Torr

Continue ramp

 ramp @ 4A/min (2A/30s)

Thursday, August 31, 2023, 12:50

IGP1= 2.23e-06 Torr

OMEGA=1392 C

Thursday, August 31, 2023, 13:04

IGP1=2.7e-06 Torr

OMEGA=1443 C

Thursday, August 31, 2023, 13:18

IGP1= 3.8e-06 Torr

OMEGA=1537 C

Thursday, August 31, 2023, 14:38

OMEGA=1852C

Tuesday, August 29, 2023, 12:46

The coated container was wrapped in 4 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Tuesday, August 29, 2023, 12:49

Initial heating start

IGP1= 6.0 e-06 Torr

Tuesday, August 29, 2023, 14:31

Paused ramping to take reading

IGP1= 5.98e-06 Torr

OMEGA = 1500 C

Tuesday, August 29, 2023, 15:24

OMEGA 1866 C

IGP1= 6.6e-6 Torr

Saturday, August 26, 2023, 09:39

The coated container was wrapped in 4 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Initial IGP1= 8.7e-07 Torr

Saturday, August 26, 2023, 10:54

IGP1= 1.2e-06 Torr

Start ramp up at 4A/min on both heaters (2A/30s) until TGHT = 400A and TBHT=230A

Saturday, August 26, 2023, 11:32

Paused ramp to allow temperature to stabilize and record data

OMEGA= 1396 C

IGP1= 2.47e-06 Torr

Saturday, August 26, 2023, 11:52

Paused ramp to record data

OMEGA = 1544 C

IGP1=3.4e-06 Torr

Saturday, August 26, 2023, 12:09

Paused ramp to record data

OMEGA = 1653

IGP1 = 4.5e-06 Torr

Saturday, August 26, 2023, 12:33

Omega went up to 1878C.  Lowered the current on TGHT to reach OMEGA = 1857 C

Will keep until 430 pm

IGP1- 3.4e-06 Torr

Saturday, August 26, 2023, 16:10

ramping down at -2A/min tght 1A/min tbht

1837 C OMEGA

 Nb#11 LP-IG-LIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm (0.001")

Target density =  7.13 g/cm3

Target length = 3.53 cm

Total Mass = 25.165 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  434 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Final desired temperature = 1900C.

Replacement for Nb#10

Thursday, August 24, 2023, 14:16: Roughing.

OMEGA slope = 0.98.

Thursday, August 24, 2023, 14:31: Turbo pump started. 

Thursday, August 24, 2023, 14:41: TGHT / TBHT PS on. Manually test @ 5 / 5 A. ok. Tap back to 0 A. 

Thursday, August 24, 2023, 18:26: Vacuum @ 4.35e-06T. Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per minute. 

Thursday, August 24, 2023, 22:00: TGHT / TBHT @ 414 / 230 A (406 / 233 A - Offset). Auto-ramping TGHT to 580 A @ 2 A per min continued. Temperature @ 1353 C. Vacuum @ 4.03e-06T. 

Thursday, August 24, 2023, 23:29: TGHT / TBHT @ 580 / 230 A (569 / 233 A). Auto-ramping TGHT to 610 A @ 2 A per min (approx 600 A w/ offset). Temperature @ 1708 C. Vacuum @ 6.61e-06T. 

Thursday, August 24, 2023, 23:49: TGHT / TBHT @ 610 / 230 A (598 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (620 A w/ offset). Temperature @ 1765 C. Vacuum @ 7.22e-06T. 

Friday, August 25, 2023, 00:04: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1808 C. Vacuum @ 7.54e-06T. 

Friday, August 25, 2023, 00:16: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 670 A @ 2 A per min (660 A w/ offset). Temperature @ 1845 C. Vacuum @ 7.72e-06T. 

Friday, August 25, 2023, 00:27: TGHT / TBHT @ 670 / 230 A (657 / 233 A). Auto-ramping TGHT to 680 A @ 2 A per min (668 A w/ offset). Temperature @ 1880 C. Vacuum @ 8.46e-06T. 

Manually tap up to temperature.

Friday, August 25, 2023, 00:34: TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1900-1901 C. Vacuum @ 8.59e-06T. Desired Temperature Reached.

Friday, August 25, 2023, 00:37: Auto-cooling @ 2 A per min. 

Friday, August 25, 2023, 06:15: 

Friday, August 25, 2023, 07:40: PS & TP off.

Tuesday, August 22, 2023, 09:29

The coated container was wrapped in 4 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 2 hours

Final Current TBHT= N/A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 IGP1 initial =2.2e-06 Torr

 Tuesday, August 22, 2023, 10:25

IGP1= 2.31e-06 Torr

TGHT 98.0 A (RD), 1.35 V

Start ramping at 2A/min to 400A

Tuesday, August 22, 2023, 11:54

Reached 1860 @ TGHT = 353A, 6.16V (RD)  Will leave for 2 hours

Tuesday, August 22, 2023, 14:07

1853C OMEGA

TGHT = 353 A, 6.2 V (RD)

IGP1= 2.88E-06 Torr

Starting ramp-down at -2A/min

Saturday, August 26, 2023, 09:37

Note: the coating looks really good .  The second sintering on the second coating was 2 hours.  Will test the coating during graphite material conditioning.

Tuesday, August 15, 2023, 10:48

The coated container was wrapped in 4 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= N/A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to 100 A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 IGP1 initial =8.9e-06 Torr

 Tuesday, August 15, 2023, 13:00

Tuesday, August 15, 2023, 13:00

Pressure stabilizing @8.8e-06 Torr

starting 2A/30s ramp to 400 A

Tuesday, August 15, 2023, 14:02

TGHT RD CURRENT = 331.4A, 5.8V, SET CURRENT=338 A. 

OMEGA = 1855

IGP1= 1.5e-05 Torr

Leave for 4 hours

Tuesday, August 15, 2023, 15:05

Temperature dropped slightly to 1820C so increased current set point to 345A, and RD was at 338A, 5.9V

OMEGA increased to 1842C

Tuesday, August 15, 2023, 17:59

OMEGA = 1823C

TGHT= RD 338A, 5.9V   SET= 345A

IGP1= 4.0e-06 Torr

Start rampdown at -2A/min

Nb#10 LP-IG-LIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm (0.001")

Target density =  7.36 g/cm3

Target length = 3.5 cm

Total Mass = 25.7576 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  438 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Wednesday, June 21, 2023, 10:37: Roughing.

Wednesday, June 21, 2023, 13:39: TP1 on. 

Wednesday, June 21, 2023, 13:55: TGHT / TBHT PS on. Vacuum @ 3.35e-05T

Thursday, June 22, 2023, 13:16: TGHT / TBHT Manually set to 5 / 5 A. Vacuum @ 8.17e-07T.

Final desired temperature = 1900C.

Thursday, June 22, 2023, 13:49: OMEGA slope = 0.98.

Friday, June 23, 2023, 06:24: Auto-ramping TGHT / TBHT to 580 / 230 @ 2 A per min. 

Friday, June 23, 2023, 12:11: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 610 A @ 2 A per min (600 A w/ offset). Temperature @ 1697 C. Vacuum @ 3.38e-06T.

Friday, June 23, 2023, 12:32: TGHT / TBHT @ 610 / 230 A (600 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (620 A w/ offset). Temperature @ 1748 C. Vacuum @ 4.61e-06T.

Friday, June 23, 2023, 12:44: TGHT / TBHT @ 630 / 230 A (617 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1790 C. Vacuum @ 5.74e-06T.

Friday, June 23, 2023, 13:07: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 670 A @ 2 A per min (660 A w/ offset). Temperature @ 1825 C. Vacuum @ 5.90e-06T.

Friday, June 23, 2023, 13:22: TGHT / TBHT @ 670 / 230 A (658 / 233 A). Auto-ramping TGHT to 680 A @ 2 A per min (668 A w/ offset). Temperature @ 1858 C. Vacuum @ 6.75e-06T. 

Friday, June 23, 2023, 13:29: TGHT / TBHT @ 680 / 230 A (667 / 233 A). Auto-ramping TGHT to 690 A @ 2 A per min (677 A w/ offset). Temperature @ 1877 C. Vacuum @ 6.99e-06T. 

Friday, June 23, 2023, 13:37: Manually tap up to temperature. 

Friday, June 23, 2023, 13:38: Vacuum @ 7.54e-06T. TGHT /  TBHT @ 694 / 230 A (680.5 / 233 A direct w/ offset). Temperature @ 1901-1902 C. Desired Temperature Reached.

Friday, June 23, 2023, 13:42: Auto-cooling @ 2 A per min. 

Thursday, June 08, 2023, 09:28

Using smaller particle size TaC no ball mill procedure.

Loaded 2 TaC coated end caps and 1 TaC coated springs.

OMEGA Slope 0.99

Will heat to 1850-1900 C and hold for 4 hours

Good Vac = 5.0e-4 Torr

Bad Vac= 5.0 e-02 Torr

 Initial IGP1= 4.07E-06 Torr

Thursday, June 08, 2023, 10:36

ramped @ 2A/min to 100A.  Then after pressure stabilized starting ramp at 4A/min (2A/30s) to 400A

Thursday, June 08, 2023, 12:24

reached 1850 C with Set current = 480 and RD current = 470.6A, V = 7.7

Will leave for 4 hours.

Thursday, June 08, 2023, 15:31

ramping down at -2A/min (-1A/30s)

Tuesday, June 06, 2023, 09:11

A Ta container tube was wrapped with 4 Ta heatshields.  Note final container is 45220-6

272 graphite discs were loaded.

a TaC coated Ta spring at the front end.

The system was left to establish vacuum over previous night.

Good vacuum set to5e-04Torr

Bad vacuum was set to 5e-2 Torr

Total weight of system including spring= 253.94 g

OMEGA slope = 0.99

The target will be heated to ~2000 C, held there for 10 hours. 

Initial ramp at 1A/min to 200A

Then ramp at 0.5A/min while taking temperature readings periodically unti l250A.

At 250 A will let pressure stabilize and then ramp at 1A/min to 2000C or 480A.  Will use read back current

Will hold at target Temperature or Current for 10 hours before starting ramp-down.

Tuesday, June 06, 2023, 09:14

 Starting ramt at 1A/min

initial IGP1= 8.2e-07

Tuesday, June 06, 2023, 21:25

@480 A on readback, 1823C on OMEGA.  ramping to 510A set point which should be around 490 RD.  (see heating profile for details)

Tuesday, June 06, 2023, 22:02

ramped to 516 on RD 527 on set.  Will leave for 10 hours

OMEGA =1930 C

Wednesday, June 07, 2023, 06:32

OMEGA at 1950 C this morning.  Will continue heating.  Lowered to 1940 C as in experiment 1 this was the top temperature.

Wednesday, June 07, 2023, 07:40

OMEGA= 1940 C

IGP1=1.7-6 Torr

TGHT= 513A, 9.4V

starting ramp down at -2A/min

 Previous TP would only spin up to 4KRPM. New TP installed.

Monday, June 05, 2023, 14:50: Roughing. 

Monday, June 05, 2023, 15:10: Controller reset. TP on. 

Wednesday, May 24, 2023, 15:22

A Ta container tube was wrapped with 4 Ta heatshields.  Note final container is 45220-11

219 graphite discs were loaded.

a TaC coated Ta spring at the front end.

The system was left to establish vacuum over previous night.

Good vacuum set to5e-04Torr

Bad vacuum was set to 5e-2 Torr

Total weight of system including spring= 250.1 g

OMEGA slope = 0.99

The target will be heated to 2000 C, held there for 10 hours. 

Initial ramp at 1A/min to 200A

Then ramp at 0.5A/min while taking temperature readings periodically unti l250A.

At 250 A will let pressure stabilize and then ramp at 1A/min to 2000C or 450A.  

Will hold at target Temperature or Current for 10 hours before starting ramp-down.

 Wednesday, May 24, 2023, 15:50

Currently heating at 0.5A/min to250A.  Taking temperature/current measurements

IGP1= 1.06e-06 Torr

Wednesday, May 24, 2023, 18:28

heating at 1A/min to 275A to collect more temperature data

Wednesday, May 24, 2023, 19:22

Slight offset between set and RD current observed. 

Ramping at 1A/min to 440A according to the regression below

Should be around 2000 C.

Wednesday, May 24, 2023, 20:22

Currently at 339 A, 4.8V

OMEGA = 1614 C, IGP1= 2.04e-06 Torr

Will ramp up at 2A/min to 450A as new data point suggests

Wednesday, May 24, 2023, 21:05

heating curve has new slope suggesting 500A as minimum to reach 2000 C

Increasing ramp to 1A/10s to reach 450A

Wednesday, May 24, 2023, 21:17

TGHT

IGP1= 3.9e-06 Torr

Continue ramping to 480A

Wednesday, May 24, 2023, 22:11

Offset between setpoint of current and readback.  readback 10A below. 

Will keep at this setting until 7:30 am tomorrow then start ramp down @-2A/min

Thursday, May 25, 2023, 07:25

OMEGA=1912C, IGP1 =1.29e-06 Torr, TGHT = 480A, 9.0V

begin ramp down at -2A/min

Thursday, May 25, 2023, 09:52

Some odd current readback behaeviour noticed.  Have contacted Gelo from controls.  He will look at it next week.  Discrepancy between read back and set point and drop in read back currrent. See picture

Tuesday, May 02, 2023, 14:03

Two np-TiO2 spun fibrous pellets and 1 batch of fibre mats were wrapped with graphite foils and loaded into a target boat.

Sample will be heated to 1875C, similar to the previous process, see e-log ID#605 (TGHT: 440A/7.6V).

TGHT will be autoramped to 350 A and monitor the conditions before ramping up further.

Good vacuum: 3e-5 Torr

Bad vacuum: 5e-5 Torr

Omega slope: 1.08

In the previous process (ID#605), Ta-foil was inserted at both ends of the tubes to hold the sample together. However, it was observed that the out-gassing of the material reacted with the Ta-foil, causing issues. Therefore, it's decided not to cover the ends with Ta-foil, and the sensor is now looking at the graphite foil. It had previously determined the slope for SiC material set for its emissivity, but need to note any errors that may have arisen due to the change in the sample setup.

See attachment#1 for sample setup - note that Omega sensor is slightly looking at the edge of the Ta-boat tube. 

Initiate autoramp: 1 A/min

Chamber has been pumped down below 5.6e-6 Torr.

 Tuesday, May 02, 2023, 15:31

Vacuum spike TGHT at 75A, auto-ramping down kicked in.

 Wednesday, May 03, 2023, 12:18Thursday, May 04, 2023, 15:16

TGHT has been holding at 350A/5.7V (1995W) for almost 2hrs, temp is reading at 1368C - 232C lower than the previous process (ID#605) with TGHT = 348/5.8V (2018W).

Pressure started to come down around 344A/5.5V, temp 1331C - see attachment #2.

Current status overall view - see attachment #3

Continue to ramp up t0 440A at 1A/min and monitor.

 Wednesday, May 03, 2023, 14:47

TGHT reached 440A/7.5V, temp reading at 1672C.  Pressure is coming down, currently at 1.8e-6 Torr.  Will keep at this setting overnight and will check the Omega/emmissivity to confirm the temperature.

 Thursday, May 04, 2023, 10:54

Eractic vacuum spikes started just over 3 hrs ago.  Temp at 1681 C; TGHT has been stable at 440A/7.6V. Pressure ranging between 5.0e-7 to 1.5 e-6 and gradually decreasing, see attachment #4. 

Will perform the omega/emmissivity measurement.

 Thursday, May 04, 2023, 15:16

Temperature was checked with the digital and analogue pyrometers. 

With the analogue pyrometer on the Ta-container (left end, top surface), measured temp = 1360 C, with e=0.22, correction + 200 C => 1560 C

With the Omega pyrometer (right end), 1-color mode with e= 0.22, temp = 1585 C. 

Setting Omega pyrometer to 2-color mode with e= 0.99 temp = 1516 C --  this is in agreement with the measurements for Ta.  Note that the pyrometer is looking at some part of the Ta container which is not covered by the sample wrapped with the graphite foil (see attachment #5). 

From e-log#596, temp was reported at 1520 C (slope at 0.99) with a Ta-foil at the end of the tube, but from e-log#605, temp was reported at 1864 C (slope at 0.99) - possibly an error occurred during that time.

In conclusion, the temp should be at 1530 C +/- 10C with TGHT = 440A/7.7V (3388W).

 Thursday, May 04, 2023, 15:43

Vacuum spikes continue every 30 min lasting for 10 min. 

Tapped down TGHT to 430A/7.5V, temp reading at 1500 C.  Will monitor if any improvement with the vacuum.

 Friday, May 05, 2023, 09:34

Vacuum spikes continue to happen; see attachment #6 for the striptool overview.

Lower TGHT to 420A/7.3V, temp = 1480 C.

 Friday, May 05, 2023, 10:10

Vacuum spikes continue every 20-30 min lasting for 10 min. 

Lower TGHT to 410A/7.1V, temp = 1450 C

 Friday, May 05, 2023, 11:25

Vacuum spikes continue,

Lower TGHT to 400A/6.93V, temp = 1433 C

 Friday, May 05, 2023, 12:20

Vacuum spikes - lower TGHT to 390A/6.7V, temp at 1407C

Friday, May 05, 2023, 13:19

Vacuum spikes - lower TGHT to 380A/6.5V, temp at 1388C

Friday, May 05, 2023, 13:47

Vacuum spikes - lower TGHT to 370A/6.3V, temp at1373 C

Friday, May 05, 2023, 14:16

Vacuum spikes - lower TGHT 360A/6.1V, temp at 1348 C

Friday, May 05, 2023, 15:11

Vacuum spikes - lower TGHT 350A/5.9V, temp at 1308 C

Friday, May 05, 2023, 16:34

Vacuum spikes - lower TGHT 340A/5.7V, temp at 1371 C

Friday, May 05, 2023, 16:56

Vacuum spikes continue; container possibly broken.

Slow ramp down TGHT at -0.5A/min to see when the vacuum spikes would stop.

 Monday, May 08, 2023, 09:54

TGHT was ramped down over the weekend.  Chamber was kept under vacuum and vacuum continued to spike; suspecting problem with the gauge?! see attachment &7 for an over view.

Will take out the samples for exam.

Friday, April 28, 2023, 11:29

loaded 14 TaC coated end caps and 2 TaC coated springs.

OMEGA Slope 0.99

Will heat to 1850-1900 C and hold for 4 hours

Good Vac = 5.0e-4 Torr

Bad Vac= 5.0 e-02 Torr

 2 end caps had slight damage and were disposed of.  12 good caps and 2 good springs.

John Wong wrote:

Darwin Ortiz Rosales wrote: John Wong wrote: Carla Babcock wrote: Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A  Wednesday, April 26, 2023, 22:12 TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight. Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview.  TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.         Thursday, April 27, 2023, 06:27 IGP1= 1.7e-06 Torr OMEGA= 1097 C TGHT= 400A, 6.2V TBHT= 273A, 3.7 V Starting ramp up of TGHT @0.2A/min set to 550A  Thursday, April 27, 2023, 22:04 TGHT has reached 580A/10.33V. Temp = 1540C.  The two out-gassing peaks were observed: 1st peak around 1300C and 2nd peak 1370C.  See attachments 1 & 2. A few minutes after TGHT reached to 580A, there was a small jump in TGHT current/voltage and also the pressure, but didn't notice any change in the temp, see attachment 3&4.  Pressure is currently at 3.4e-6 Torr; will hold TGHT until pressure reaches close to 1e-6 Torr before cooling down.   Friday, April 28, 2023, 01:06 Pressure has reached 1.8 e-6 Torr; TGHT has been holding at 580A for 3.5 hrs, a slight increase in voltage, reading at 10.45V and temperature, 1548C.  See attachment #5 for overview. Initiating auto-cooling TGHT at -2A/min, TBHT at -1A/min.

 Friday, April 28, 2023, 09:27

IGP1= 1.20e-07 Torr

Will dismount target around 10:15 am

Heating curve below.  Non-linear behavior

 Final weight = 517.08 g

Target looks good see attached picture