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Message ID: 645     Entry time: Tuesday, September 12, 2023, 09:54
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 41369-2 
Source: HP-SIS 
Status: Done 
Subject: TaC coating sintering 

Tuesday, September 12, 2023, 09:51

The coated container was wrapped in 3 Ta foil heatshield and left in evap2 over night to attain vacuum.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~700A (adjustable)

Heating autoramp starged at 1A/min on  TGHT  and TBHT to 120A

Then at 2 A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

Initial IGP1= 2.7e-06 Torr


Tuesday, September 12, 2023, 7:00

Started autoramp @1A/min to 120A on both TGHT and TBHT


Tuesday, September 12, 2023, 09:53

Heating ramp set to 230A for both TGHT and TBHT.  Rate at 2A/min for both heaters.


Tuesday, September 12, 2023, 11:21

Continued ramp on TGHT at 2A/min to 335A and now setting to 3A/min (1.5A/30s)


Tuesday, September 12, 2023, 11:47

 

 

  TGHT  
Temperature ( C ) Voltage (V) Current (A)
1205 5.5 392.0

Continue ramping @3A/min on TGHT


 Tuesday, September 12, 2023, 13:33

Reached 1840 C at TGHT =677A and 10.5V

Will keep for 4 hours

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