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Message ID: 640     Entry time: Tuesday, August 22, 2023, 09:35
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 44692-11 
Source: TARGET BOAT 
Status: Done 
Subject: TaC coating sintering (second coating on same tube) 

Tuesday, August 22, 2023, 09:29

The coated container was wrapped in 4 Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 2 hours

Final Current TBHT= N/A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A.

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 IGP1 initial =2.2e-06 Torr

 


 Tuesday, August 22, 2023, 10:25

IGP1= 2.31e-06 Torr

TGHT 98.0 A (RD), 1.35 V

Start ramping at 2A/min to 400A

 


Tuesday, August 22, 2023, 11:54

Reached 1860 @ TGHT = 353A, 6.16V (RD)  Will leave for 2 hours


Tuesday, August 22, 2023, 14:07

1853C OMEGA

TGHT = 353 A, 6.2 V (RD)

IGP1= 2.88E-06 Torr

Starting ramp-down at -2A/min

 


Saturday, August 26, 2023, 09:37

Note: the coating looks really good .  The second sintering on the second coating was 2 hours.  Will test the coating during graphite material conditioning.

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