Tuesday, August 22, 2023, 09:29
The coated container was wrapped in 4 Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 2 hours
Final Current TBHT= N/A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A.
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
IGP1 initial =2.2e-06 Torr
Tuesday, August 22, 2023, 10:25
IGP1= 2.31e-06 Torr
TGHT 98.0 A (RD), 1.35 V
Start ramping at 2A/min to 400A
Tuesday, August 22, 2023, 11:54
Reached 1860 @ TGHT = 353A, 6.16V (RD) Will leave for 2 hours
Tuesday, August 22, 2023, 14:07
1853C OMEGA
TGHT = 353 A, 6.2 V (RD)
IGP1= 2.88E-06 Torr
Starting ramp-down at -2A/min
Saturday, August 26, 2023, 09:37
Note: the coating looks really good . The second sintering on the second coating was 2 hours. Will test the coating during graphite material conditioning. |