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Message ID: 648     Entry time: Friday, October 20, 2023, 07:24
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 45447-11 
Source: LP-SIS 
Status: Done 
Subject: TaC coating sintering 

Friday, October 20, 2023, 07:20

The coated container was wrapped in 4 Ta foil heatshields.

Vacuum IGP1 initial = 9.9 e-07 Torr

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 2A/min(1A/30s) on  TGHT  100A

Then at 4A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr

 


Friday, October 20, 2023, 07:24

Starting initial ramp

Vacuum IGP1 initial = 9.9 e-07 Torr

 


Friday, October 20, 2023, 08:55

After initial pressure bump continued heating at 1A/min to 120A to observe any other possible pressure bump.


Friday, October 20, 2023, 09:05

increased ramp to 4A/min to 400 TGHT and 230 TBHT

 


Friday, October 20, 2023, 09:35

OMEGA=1280 C

TGHT= 221.5 A, 3.24V 

TBHT=228.9, 3.9V

 


Friday, October 20, 2023, 10:22

OMEGA 1852 C at TGHT = 390A, 6.5 V ; TBHT = 232 A, 4.0 V

Will leave for 4 hours

 


Friday, October 20, 2023, 14:16

About to start rampdown

TGHT @ -2A/min

TBHT@ -1A/min

Final OMEGA = 1840 C

IGP1 = 1.83e-06 Torr

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