Tuesday, March 20, 2012, 14:35, John Wong, , , , Done, Evap#2 Backing up muffler not connected to the exhaust system.
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Tuesday, March 20, 2012, 14:22
The Evaporator #2 backing pump (IEVAP2:BP1) muffler has not connected to the exhaust duct.
See attachment#1 as to where the muffler should be connected to the exhaust ducting system.
The Evaporator chamber is currently under vacuum; the BeO sintering process will be pending for now until the backing pump is properly installed.
(ISAC E-fault 5880)
Wednesday, March 21, 2012, 13:55
Edi Dalla Valle is connecting the evaporator backing scroll pump exhaust to the existing nuclear exhaust. (See attachment#2: scroll_pump_exhause.jpg). A filter is also added between the exhaust line
to prevent any back flow of oil from the Evaporator #1 backing pump (An oil pump).
Work is covered under ISAC WP# 2012-03-21-3.
The evaporator is now operational.
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Tuesday, September 11, 2018, 10:47, Aaron Schmidt, , , , , Evap 2 step discrepancy
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Tuesday, September 11, 2018, 10:45:
TGHT: 53.4 A TBHT: 57.75
Actual
TGHT: 60.0A TBHT: 59.0A
Uploaded the rest to Word doc. Screenshots included. |
Monday, June 11, 2012, 12:26, John Wong, SiC, 38481-2, HP-SIS, Problems, End caps vaporized
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John Wong wrote: |
Nikita Bernier wrote: |
John Wong wrote: |
Nikita Bernier wrote: |
John Wong wrote: |
Tuesday, May 15, 2012, 12:24
The HP-SIS SiC target was made on Nov 03, 2010. The target consists of 405 discs, 18.5cm in length. It was sintered in the Evaporator#1.
This target is going into Evap#2 for re-conditioning. It is currently being pumped down.
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Friday, May 18, 2012, 12:19
The target is wrapped with only one heat shield.
Evaporator #2 Target Heater is now auto-ramping at 0.5 A/min, up to 820 A, with the maximum voltage limited at 2 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). Tube Heater is auto-ramping at 0.5 A/min, up to 230 A, with the maximum voltage limited at 1 V. See attachments.
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Friday, May 18, 2012, 13:15
Increased TBHT voltage to 5V, and TGHT to 15V. Currently, TBHT =83A, 0.986V, TGHT= 144A, 1.65V, IGP1 = 5.2e-7 Torr, IGP2 = 4.3e-7 Torr.
Continue ramping up...
Tuesday, May 22, 2012, 12:02
TGHT and TBHT were ramped up to 830A/13.65V (local), and 235A/3.85V, respectively. The target was conditioned over the long weekend.
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Tuesday, May 22, 2012, 12:13
Initiating the cool-down process at 5 A/min.
See archive plots of the Target Heater (Attachment 1) and the Tube Heater (Attachment 2).
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Tuesday, May 22, 2012, 15:24
TGHT/TBHT were ramped down to 0A. The target has cooled for about 45 min. All pumps and chillers are off. The chamber has been vented.
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Monday, June 11, 2012, 12:20
After the re-conditioning, the target's end-caps vaporized. This is something happened before (see elog entries below):
https://elog.triumf.ca/TIS/Evaporator_1/20
https://elog.triumf.ca/TIS/Evaporator_1/22
The caps were removed and yellow crystals were observed. (see attachment#1).
The D-caps will be inserted in both ends and will be re-conditioned again to see if the yellow crystals can be removed at high temperature.
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Wednesday, August 14, 2024, 07:23, Marla Cervantes, C, 44139-5 SK, LP TUBE, Problems, EVAP2 Calibration - Vanadium
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Tuesday, August 13, 2024, 17:20 Pressure kept increasing when turning the turbo pump on
Tuesday, August 13, 2024, 18:00 Pressure stayed constant when turning the turbo pump on |
Wednesday, August 14, 2024, 16:22, Marla Cervantes, C, 44139-5 SK, LP TUBE, Problems resolved, EVAP2 Calibration - Vanadium
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Marla Cervantes wrote: |
Tuesday, August 13, 2024, 17:20 Pressure kept increasing when turning the turbo pump on
Tuesday, August 13, 2024, 18:00 Pressure stayed constant when turning the turbo pump on
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Wednesday, August 14, 2024, 10:18
The turbo pump started up normally. System is purging. and tomorrow the target will be heated.
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Wednesday, August 14, 2024, 16:24, Marla Cervantes, C, 44139-5 SK, LP TUBE, In progress, EVAP2 Calibration - Vanadium
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Marla Cervantes wrote: |
Marla Cervantes wrote: |
Tuesday, August 13, 2024, 17:20 Pressure kept increasing when turning the turbo pump on
Tuesday, August 13, 2024, 18:00 Pressure stayed constant when turning the turbo pump on
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Wednesday, August 14, 2024, 10:18
The turbo pump started up normally. System is purging. and tomorrow the target will be heated.
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Wednesday, August 14, 2024, 16:19
A vanadium wire was introduced in a tantalum pouch and snug among the graphite foils of a conditioned graphite target. The V wire was introduced in the Ta pouch to prevent the direct contact of the wire with the carbon and avoid the reaction between them.
As a first approach, the target will be heated to approximately 1377 °C, aiming at the vaporization temperature of the V wire. If the wire does not vaporize, heating with the turbo pump off would be considered to aim at the vanadium's melting point of 1910 °C.
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Vaporization (at 3e-6 Torr)
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In case of outgassing, let the pressure reduce
- Next ramping: 0.5 A/ 2min to 250 A.
Very slow rate to allow thermal equilibrium and temperature measurements. Estimated time 3h.
Thursday, August 15, 2024, 08:21
IGP1 = 5.3e-7 Torr
Good vacuum 3e-5 Torr
Bad vacuum 5e-5 Torr
Initial ramping: 2 A/min to 200 A.
Thursday, August 15, 2024, 09:01. Pressure starting to increase at 74 A
Thursday, August 15, 2024, 09:15. Pressure stabilizing 1.8e-6 Torr. Current 103 A, voltage 1.3 V
Thursday, August 15, 2024, 09:21. Pressure increasing (116 A).
Thursday, August 15, 2024, 09:29 Pressure dropping (Current approx. 120 A)
Thursday, August 15, 2024, 10:54
Started ramping to find a pressure peak corresponding to V vaporization.
IGP1 = 6.4e-7
TGHT = 200 A, 2.9 V, omega 1152 °C
Next ramping: 0.5 A/ 2min to 250 A
Thursday, August 15, 2024, 11:17
Ramp seem to slow. The temperature change was too subtle (according to the omega).
IGP1 = 6.5e-7
TGHT = 205 A, 3.03 V, omega 1157 °C
Next ramping: 1 A/ 2min to 250 A
Thursday, August 15, 2024, 11:32
Ramp changed to 0.5 A/min
Thursday, August 15, 2024, 11:54
Ramp was stopped because the pressure was increasing, suggesting the V vaporization.
IGP1 = 6.9e-7
TGHT = 222 A, 3.3 V
Omega 1210 °C, filament 1280 °C
The difference between pyrometers is negligible, suggesting that the V vaporization temperature at 6e-7 Torr of approx. 1300 °C
Thursday, August 15, 2024, 13:15
IGP1 = 7.9e-7
TGHT = 250 A, 3.8 V
Omega 1289 °C
Thursday, August 15, 2024, 13:16
Ramp set to 0.5 A/min to 300 A
Pressure mini-spike at 13:18
Omega reading 1291 °C
Thursday, August 15, 2024, 14:08
IGP1 = 8.5e-7
TGHT = 270 A, 4.18 V
Omega 1375 °C, filament 1400 °C
The system stayed at those conditions for 15min
Thursday, August 15, 2024, 14:11
Ramping to 0A at 2A/min
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Thursday, April 07, 2016, 15:23, John Wong, SiC, , TARGET BOAT, Done, E-spun SiC/PAN thermal treatment
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Thursday, April 07, 2016, 15:18
E-spun SiC/PAN fiber mats were produced at UBC.
12%PAN solution; 50% SiC to weight of PAN.
Materials used:
1.2g PAN, 8.8g DMF, 0.6g SiC, SDS ~0.1% to SiC
Fiber mats were heat treated at 250C in air. Then cut into 18" discs and loaded into Ta target boat with heatshield wrapped.
3 temperature treatments will carry out: 1200C, 1400C and 1600C
Chamber is being pumped down
Friday, April 08, 2016, 10:02
TGHT at 285A, Temp at ~1200C. Will remain at this temp for a few hours before cooling down.
Some samples will be taken out for analysis.
Next week, temperature treatment will continue at 1400C
Friday, April 08, 2016, 14:26
Samples have been heated at 1200C for just over 4 hours.
Initiated auto-cooling at 2A/min
Tuesday, April 12, 2016, 17:51
Heat treatment #2 - 1400C.
Initial mass after 1200C = 0.0312g
Monday, April 18, 2016, 12:55
Samples was heated at 1400C (TGHT maintained at ~370A) for 4 days (see attachment 1).
Chamber is vented; samples will be inspected.
Tuesday, April 19, 2016, 17:49
Results
Sample mass after 1200C = 0.0312g
Sample mass after 1400C = 0.0294g
~5.78% mass loss.
Tuesday, April 19, 2016, 17:57
Heat Treatment#3: 1600C
sample mass before heating = 0.0238g (this sample is taken from the batch after it was heated at 1400C)
Chamber is being pumped.
Thursday, April 21, 2016, 11:07
TGHT stepped up to 330A, temp measured at 1422C.
Thursday, April 21, 2016, 12:05
TGHT at 415A/7.16V; temp at 1610C
Thursday, April 21, 2016, 17:49
Temp dropped to 1590. Increased TGHT to 425A; temp reads 1602A.
Friday, April 22, 2016, 10:57
Voltage increased to 7.33V, TGHT stepped down to 418A, temp maintained at 1610A.
Monday, April 25, 2016, 12:08
Sample was heat treated for almost 4 days. Temperature dropped to 1578C, TGHT at 418/7.26V. (see attachment #2)
Ramping down TGHT 2A/min.
Monday, April 25, 2016, 16:00
Result:
Mass after 1600C = 0.0104g, 5.63% mass loss.
Will do XRD/EDX
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Thursday, August 05, 2021, 11:18, Darwin Ortiz Rosales, SiC, 44691-2, LP-SIS, Done, Dr blade and non-Dr blade Material Experiment (sintering)
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Thursday, August 05, 2021, 11:10
Total number of foils: 380
Total length packed 13.5 cm
container has 3 Ta heat shields.
No endcaps inserted to facilitate out-gassing
Two Ta discs at either end and three graphite discs as separators
[Left end [ blade--no blade--blade---no blade] Right end ]
Initially to ramp TGHT and TBHT to 50A at0.5 A/min
Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically to reach 430A A (Omega slope set = 0.990)
Then temperature = 1800C
TBHT will be set fixed at 230 A (max). TBHT heated manually and automatically to max.
Good vac at 3.00 e -5 Torr
Bad vac at 5.00 e-5 Torr
Total weight into Evap2 =503.8 g
Friday, August 06, 2021, 11:33
IGP1= 8.3e-07 Torr
Start heating at 0.5 A/min on both TGHT and TBHT up to 50A
Friday, August 06, 2021, 22:34
IGP1= 7.0e-06 Torr
TGHT= 50.1 A, 0.6 V TBHT = 50.0A, 0.6V
Continue heating at 0.5A/min to 400A on TGHT and 230A on TBHT
Saturday, August 07, 2021, 10:11
Stopped autoramping. Will allow some time at 63 A on both TGHT and TBHT
Saturday, August 07, 2021, 12:19
IGP1= 1.9e-05 Torr
Manually increase TGHT and TBHT to 65 A
Saturday, August 07, 2021, 23:01
IGP1= 5.8e-06 Torr
TGHT= 64.5 A, 08V TBHT=64.6A, 0.8V
Ramp up manually while monitoring pressure
Sunday, August 08, 2021, 08:46
IGP1= 6.0e-06 Torr
TGHT = 69A, 0.85V TBHT = 69A, 0.90V
ramp up manually
Monday, August 09, 2021, 08:54
IGP1= 1.38e-05 Torr
TGHT= 90.0 A, 1.1V, TBHT= 90.0A 1.3V
Start autoramp at 0.5 A/min on both TGHT and TBHT to 400A and 230A respectively.
Changed bad vacuum to 5e-04 Torr
Monday, August 09, 2021, 21:37
IGP1= 6.6e-06 Torr
TGHT= 300.3 A, 5.0 V, TBHT = 233.0 A, 4.1V
Increase ramp rate to 2A/min for TGHT to 400 A,
OMEGA = 1430 C
Monday, August 09, 2021, 22:09
Will autoramp at 2A/min up to 424A as per regression line on attached file
Monday, August 09, 2021, 22:58
Temperature drop on OMEGA. Unexpected. Will lower current on TGHT to 418A and keep there for 4 hours. OMEGA may not be reliable
Tuesday, August 10, 2021, 3:16
IGP1=8.8e-07 Torr
TGHT = 414A, 7.5V TBHT = 233A, 4.1V
ramp down at -2A/min for TGHT and -1A/min for TBHT
Tuesday, August 10, 2021, 10:35
IGP1= 3.6e-07 Torr
Dismount
Some discs, especially end sections were coated with a golden layer. |
Tuesday, October 29, 2013, 15:50, Anders Mjos, , , , In progress, Copper bars on TGHT and TBHT
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Tuesday, October 29, 2013, 15:50: Pumping down
Wednesday, October 30, 2013, 09:32: Turbo started
Wednesday, October 30, 2013, 14:50: The Cu-bars were heated to 600A and 300A for TGHT and TBHT respectively.
Wednesday, October 30, 2013, 15:17: PS off. Turbo off.
Results can be found on DocuShare and in the attached plot. |
Tuesday, August 11, 2020, 10:17, Ferran Boix Pamies, Empty, 41882-1, TARGET BOAT, In progress, Contamination foils temperature test
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The target was prepared and put under vacuum on 2020-08-10
2020-08-11 10:16am The pressure is 1e-6Torr. Leak checked performed, water on no problem. Starting to set target heating curve. 1A/10s up to 300A
2020-08-11 11:23am target at 300A-1200degC Temperatures on exposed foil show to be higher than expected. 300degC already, 70degC on covered by foil thermocouple. Putting 50 more amps at 1A/10s
2020-08-11 12:11pm target at 350A-1340degC. 350degC on exposed thermocouple. Ramping to 400A 1A/10s.
2020-08-11 12:28pm target at 400A-1420degC. 400degC on exposed thermocouple. Ramping to 450A 1A/10s. |
Thursday, July 30, 2015, 17:07, John Wong, , , , Maintenance, Connect NALCW to EVAP1
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Thursday, July 30, 2015, 17:02
EVAP1 cooling system is now on the NALCW. The city water has been removed from the system.
Tested all the cooling system interlocks by shutting off each individual valve, and the main supply valve to the lab - All Passed!
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Tuesday, November 26, 2019, 15:21, Darwin Ortiz Rosales, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH)
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Tuesday, November 26, 2019, 14:53
Total number of foils: 504
Total length packed 17.4 cm
container has 3 Ta heat shields.
No endcaps inserted to facilitate out-gassing
Two TaC coated Ta wire springs inserted at either end.
Initially to ramp TGHT and TBHT to 50A at 1A/min
Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically to reach 530A A (Omega slope set = 0.990)
Then temperature= (Correected to 1800C) 1900 C, Omega Slope set = 0.990, manually and automatically ramp to 700A, TGHT will be tapped up accordingly to reach desired Temp.
TBHT will be set fixed at 230 A (max). TBHT heated manually and automatically to max.
Good vac at 3.00 e -5 Torr
Bad vac at 5.00 e-5 Torr
System experienced some vacuum issues due to cooling water leak in a heatshield line.
Evaluation discs not included because no space.
Total Green disc mass measured = 58.250 g
Tuesday, November 26, 2019, 15:00
IGP1= 7.4e-06 Torr. No leak issues found after last fix (Anders will add details).
Tuesday, November 26, 2019, 15:33
TGHT= 52.7A, .22V TBHT= 49.3A, .52V
IGP1= 7.202 e-06 Torr (trending up so will allow to stabilize).
Wednesday, November 27, 2019, 06:09
left with autoramp waiting for vac to drop but no advance overnight.
Pressure did not seem to drop back below 3e-5 Torr magnitude, therefore not much advance in current ramp.
Thursday, November 28, 2019, 11:15
Continued ramping manually
OMEGA = 1429 C (0.99 slope), TGHT = 542A, 7.8V
With slope = 1.08 OMEGA = 1724 C, therefore staying at 0.99 slope
TaC coating sintering plot suggests 753A to reach 1800C (See attachment 1)
Windows a little bit coated but not enough to disturb laser.
Thursday, November 28, 2019, 12:17
TGHT =753A, 11.8V since 12:00 noon.
TBHT= 233.4A, 3.3V
OMEGA= 1735 C (0.99 slope)
Thursday, November 28, 2019, 13:01
OMEGA = 1860C (1.08 slope)
Thursday, November 28, 2019, 14:38
OMEGA temperature began to creep up to ~1880. Tapped TGHT current down to 733.5A, 11.4V
Thursday, November 28, 2019, 15:12
Checked windows and no significant additional buildup of obstructive material.
Temperature creeping up again. Tap down TGHT current to 729 A, 11.2 V
OMEGA = 1870C at slope 1.08
Thursday, November 28, 2019, 16:03
Temperature increase to 1880C
Tap down TGHT current to 715A, 10.9V
OMEGA= 1870 C (slope = 1.08)
Thursday, November 28, 2019, 16:22
Temperature creep to 1880 C
Tap down TGHT to 700A, 10.8V
OMEGA= 1845C
IGP1=2.2e-06 Torr
Thursday, November 28, 2019, 16:37
IGP1= 1.9e-06 Torr
OMEGA = 1850C (1.08 slope)
TGHT = 692A, 10.5V TBHT= 233A, 3.2V
Initiating pressure ramp at -2A/min on TGHT and -1A/min on TBHT
Thursday, November 28, 2019, 16:45
IGP1= 1.28e-06 Torr
OMEGA= 1770 C (1.08 slope)
TGHT = 650A, 9.8V
ramp TGHT at -3.5A/min maintain TBHT at -1A/m in
Thursday, November 28, 2019, 17:11
IGP1= 1.14e-06 Torr
OMEGA = 1730 C (1.08 slope)
ramp TGHT at -5A/min maintain TBHT at -1A/m
Thursday, November 28, 2019, 17:20
IGP1- 8.9e-07 Torr
OMEGA=1636C
ramp TGHT at -6A/min maintain TBHT at -1A/min
Thursday, November 28, 2019, 17:34
IGP1= 7e-07 Torr
OMEGA= 1500 C (1.08 slope)
ramp TGHT at -8A/min maintain TBHT at -1A/min
TBHT = 183A
OMEGA 1180C
TGHT =300 A
TBHT = 155A
Initiated -15A/min TGHT and -4A/min TBHT
IGP1= 5.2e-07 Torr
OMEGA below 1000C
begin manual tapdown
Thursday, November 28, 2019, 19:42
Target was dismounted after cooling. Two graphite discs and end caps inserted.
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Wednesday, November 27, 2019, 17:45, John Wong, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH)
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Darwin Ortiz Rosales wrote: |
Tuesday, November 26, 2019, 14:53
Total number of foils: 504
Total length packed 17.4 cm
container has 3 Ta heat shields.
No endcaps inserted to facilitate out-gassing
Two TaC coated Ta wire springs inserted at either end.
Initially to ramp TGHT and TBHT to 50A at 1A/min
Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically to reach 530A A (Omega slope set = 0.990)
Then temperature= 1900 C (Correction = 1800 C, NOT 1900 - JW), Omega Slope set = 0.990 (use 1.08, check temp, JW), manually and automatically ramp to 700A (check temp to see if it's matching with the 1.08 slope), TGHT will be tapped up accordingly to reach desired Temp.
TBHT will be set fixed at 230 A (max). TBHT heated manually and automatically to max.
Good vac at 3.00 e -5 Torr
Bad vac at 5.00 e-5 Torr
System experienced some vacuum issues due to cooling water leak in a heatshield line.
Evaluation discs not included because no space.
Total Green disc mass measured = 58.250 g
Tuesday, November 26, 2019, 15:00
IGP1= 7.4e-06 Torr. No leak issues found after last fix (Anders will add details).
Tuesday, November 26, 2019, 15:33
TGHT= 52.7A, .22V TBHT= 49.3A, .52V
IGP1= 7.202 e-06 Torr (trending up so will allow to stabilize).
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Wednesday, November 27, 2019, 17:44
I'll take over from here to step up the target heater, and I'll coordinate it with Darwin.
Wednesday, November 27, 2019, 20:36
Note: Sintering temp should be at 1800 C, NOT 1900. Use Omega slope 1.08 and check temperature. Correction made on elog #471.
Continue to step up TGHT and TBHT, keeping vacuum below 1.5 e-5 Torr.
Thursday, November 28, 2019, 03:06
TGHT reached to 400A/5.29V, TBHT at 230A/3.13V.
Vacuum coming down from 1.3 e-5 Torr.
OMEGA = 1105 C (slope at 0.99).
Instructions for Darwin:
1. Confirm temperature - check the temp plot from the TaC coating step.
2. Change OMEGA slop to 1.08 - check to see if this matches the temp plot. If not, bring it back to 0.99.
3. Continue to step up TGHT, check temp at 1400C (change slop 1.08 and check), 1500 C, 1600 C (check windows for coating - if any coating, then OMEGA is no longer useful hereon)
4. Use the temp plot and continue to tap up TGHT to reach 1800 C and hold it for at least 4 hours or until the vacuum goes below 1 e-6 Torr then proceed with cooling down.
5. Use the auto cooling program for TGHT (-2A/min) and TBHT (-1A/min)
Note: For ramping up TGHT, keep vacuum below 1.5 e-4 Torr and keep tapping up to reach 1800 C. Above 1100 C, this should be a quick step to get to 1800 C; should take < 2 hrs to get there.
See the striptool or the attachment below to see how I did it.
Once the chamber is cool down, take out a few samples for SEM analysis.
Good luck!
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Monday, June 24, 2019, 08:42, Darwin Ortiz Rosales, SiC, 42464-4, HP-FEBIAD, Done, Conditioning of BSiC discs
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Monday, June 24, 2019, 08:24
Total number of foils: 484
Total mass in including container = 1495 grams
Total length packed 17.28 cm
container has 3 Ta heat shields.
No endcaps inserted to facilitate outgassing
Two TaC coated Ta wire springs inserted at either end.
Initially will heat via autoramp to OMEGA 1400 C , ramping TGHT at 0.1 A/min to reach 530A A (Omega slope set = 0.990)
Then temperature= (Correction to 1800C) 1900 C, Omega Slope set = 0.990, Auto TGHT at 0.2A/min to reach 700A, TGHT will be tapped up accordingly to reach desired Temp.
TBHT will be set fixed at 230 A (max). TBHT at 0.1 A/min.
Good vac at 3.00 e -5 Torr
Bad vac at 5.00 e-5 Torr
System was pumped down on Friday June 24th, 2019.
IGP1= 3.3 e-07 Torr
(EPICS was down this morning and came back up around 930 a.m.)
Will proceed to manually tap up TGHT and TBHT to 40A as soon as EPICS stability confirmed
Mondayy, June 24, 2019, 15:30
TBHT = 39 A, 0.4V
TGHT=40 A, 0.1V
IGP1= 4.3 e-06 Torr and trending down
Autoramp increments to 0.1 A/min , to 400A on TGHT and 230A on TBHT
Tuesday, June 25, 2019, 08:40
Current has only increased to 53 A and pressure limit reached. Lowered current back to 51 A on TGHT and TBHT. Waiting for pressure to stabilize.
Tuesday, June 25, 2019, 12:16
TGHT 51.3 A, 0.39 V
TBHT 51.1 A, 0.58 V
IGP1 = 1.91 e-05 Torr
Starting autoramp with increments to 0.1 A/min , to 400A on TGHT and 230A on TBHT
Saturday, June 29, 2019, 22:45
Autoramp increments for TGHT set to 0.2 A/min
IGP1=2.4 e-06 Torr
Sunday, June 30, 2019, 07:46
Autoramp incrementsTGHT set to 0.1 A/min to prevent pressure spike.
IGP1= 1.5 e-05 Torr
Sunday, June 30, 2019, 08:26
Set autoramp increments on TGHT back to 0.2 A/min
Sunday, June 30, 2019, 15:47
Set autoramp max on TGHT to 500 A
Sunday, June 30, 2019, 21:15
OMEGA = 1240C
TGHT= 465A, 7.0V
TBHT = 233A, 3.2V
IGP1= 1.6 e-05 Torr
Set autoramp max on TGHT to 600A
Monday, July 01, 2019, 09:48
OMEGA = 1605 C
TGHT = 599A, 9.7V
TBHT = 233A, 3.2V
IGP1= 1.3 e-06 Torr
Set autoramp max on TGHT to 650A
Monday, July 01, 2019, 18:21
OMEGA = 1630 C
TGHT = 650 A, 10.6V
TBHT = 233A, 3.2V
IGP1 = 9.7 e-07 Torr
Set utoramp max on TGHT to 700A
Monday, July 01, 2019, 22:07
OMEGA = 1663 C
TGHT = 682A, 11.4V
TBHT = 233A, 3.2V
IGP1= 1.5 e-06 Torr
Set autoramp max on TGHT to 730A
Tuesday, July 02, 2019, 08:15
OMEGA =1700 C
TGHT = 730A, 12.0V
TBHT = 233A, 3.2V
IGP1= 1.1 e-06 Torr
Set autoramp max on TGHT to 750A and increments to 0.4A/min
Tuesday, July 02, 2019, 09:49
Temperature on OMEGA began dropping. Changed OMEGA slope to 1.09 (Elog 371) and temperature reading = 1884 C. Aborted autoramp and lowered TGHT current to 740A.
Tuesday, July 02, 2019, 12:14
Temperature and pressure have dropped at a consistent rate.
IGP1= 9.6 e-07 Torr
OMEGA = 1715 C
Will tap up manually to 750A on TGHT
No appreciable increase in pressure will tap back down to 745A on TGHT
Tuesday, July 02, 2019, 13:11
OMEGA = 1675 C
TGHT = 745A, 12.4V
TBHT = 233A, 3.2V
IGP1 = 1.03 e-06Torr
Will start to ramp- down TGHT @ -2.0A/min
OMEGA = 1354 C
TGHT = 495A, 7.01V
TBHT = 233.2A, 3.2V
IGP1= 2.2 e-07 Torr
Continue ramp-down TGHT @ -2.0A/min
Tuesday, July 02, 2019, 17:14
TGHT = 285.5A, 3.4V
TBHT = 232A, 3.1V
IGP1= 1.4 e-07 Torr
Start TBHT ramp-down at -1.0 A/min
Wednesday, July 03, 2019, 08:37
Turned off TGHT and TBHT
IGP1 = 7.8 e-08 Torr
Wednesday, July 03, 2019, 13:18
Final total weight of Target = 1489.5 g
Removed 18 discs after weighing.
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Monday, September 21, 2020, 17:01, Marla Cervantes, , 44139-8-SK, TARGET BOAT, Done, Conditioning graphite target #3
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Monday, September 21, 2020, 16:50
450 graphite foils coated with graphite slurry were loaded in a tantalum tube, the tantalum tube was wrapped with 3 Ta heat shields and installed in the EVAP, to measure the temperature, a pack of 4 Ta foils were inserted in each side of the tube.
System is currently pumping down.
Tuesday, September 22, 2020, 07:54
IGP1 = 2e-6 Torr
Good vacuum of 3e-2 Torr and Bad vacuum 5e-2 Torr
The autoramp is set to 50 A at 1 A each 10 s
Tuesday, September 22, 2020, 08:18
IGP1 = 3.7e-6 Torr
TGHT = .586 V, 50.06 A
Autoramp is set to 80 A same conditions.
Tuesday, September 22, 2020, 08:26
IGP1 = 0.0006 Torr
TGHT = .97 V 80.3 A
Autoramp is set to to 100 A at 1 A each 20 s
Tuesday, September 22, 2020, 08:45
IGP1 = 0.003 Torr
TGHT = 1.3 V, 100.5 A
Autoramp is set to 120 A at same conditions
Tuesday, September 22, 2020, 09:36
IGP1 = 0.0001 torr
TGHT = 1.6 v, 122 A
Autoramp is set to 200 A at 2 A each 10 s
Tuesday, September 22, 2020, 10:19
IGP1 = 5.4e-5 Torr
TGHT = 2.9 V, 200.5 A
Omega = 1123 °C
AP = 1164 °C
Autoramp is set to 450 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Tuesday, September 22, 2020, 11:24
TGHT = 447.8 A, 7.4 V
IGP1 = 3.7e-5 Torr
Omega = 1750 °C
AP = 1720.4 °C
Autoramp set to 520 A at same conditions
Tuesday, September 22, 2020, 11:38
TGHT = 8.9 V, 525.8 A
IGP1 = 4.8e-5 Torr
Omega = 1914 °C
AP = 1835.6 °C
Autoramp set to 560 A at same conditions
Tuesday, September 22, 2020, 12:13
Omega 2038 °C
Tuesday, September 22, 2020, 12:14
Current manually reduced to 555 A
TGHT = 9.8 V, 560.8 A
IGP1 = 2.5e-5 Torr
Tuesday, September 22, 2020, 12:17
Omega = 2030 °C
Tuesday, September 22, 2020, 12:19
Current manually reduced to 550 A
TGHT = 9.8 V, 547.8 A
IGP1 = 2.3e-5 Torr
Tuesday, September 22, 2020, 12:27
Omega = 2027 °C
Tuesday, September 22, 2020, 12:27
Current manually reduced to 540 A
TGHT = 9.6 V, 541.6 A
IGP1 = 2e-5 Torr
Tuesday, September 22, 2020, 12:34
Voltage suddenly increased!
TGHT = 10.3 V, 533.8 A
IGP1 = 2.9e-5 Torr
Omega = 2129 °C
Current reduced manually to 520 A to compensate the voltage increment
Tuesday, September 22, 2020, 12:52
Another voltage increment
TGHT = 9.9 V, 519.75 A
IGP1 = 1.9 e-5 Torr
Omega 2108 °C
Current reduced manually to 500 A to compensate the voltage increment
Omega = 2070 °C
Tuesday, September 22, 2020, 13:05
TGHT = 9.4 V, 492.4 A
Omega = 2063 °C
Tuesday, September 22, 2020, 13:08
Another voltage increment! this time it was an spike
Tuesday, September 22, 2020, 16:13
After 5 hours
IGP1 = 6e-6 Torr
TGHT = 9.5 V, 488 A
Autoramp was set to 0 A at 2 A/min
Omega = 2044 °C
AP = 2003.7 °C
Wednesday, September 23, 2020, 16:18
EVAP2 vented with air, target removed. |
Wednesday, May 27, 2020, 13:04, Marla Cervantes, , 44139-7-SK, , Done, Conditioning graphite target #2
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Wednesday, May 27, 2020, 10:22
IGP1 = 3.2e-7 Torr
TGHT = 0.186 V, 0.028 A
The autoramp is set to 50A:
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 10:40
TGHT = 1.17 V, 50.9 A
PS = 1.21 V, 50 A
IGP1 = 8e-4 Torr and going down
Autoramp is set to 80 A same conditions
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 12:29
TGHT = 1.59 V, 80.04 A
PS = 1.58 V, 80 A
IGP1 = 2e-4 Torr and going down
Autoramp is set to 100 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 12:38
TGHT = 1.97 V, 100.35 A
IGP1 = 4e-4 Torr
Autoramp is set to 120 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 12:48
TGHT = 2.27 V, 119.1 A
IGP1 = 4e-4 Torr
Autoramp is set to 190 A,conditions:
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 13:03
TGHT = 3.4 V, 191.25 A
IGP1 = 3e-4 Torr
Autoramp is set to 190 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 13:36
TGHT = 7.8 V, 423 A
IGP1 = 3e-4 Torr
Autoramp is set to 450 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 13:43
TGHT = 8.5 V, 451.6 A
IGP1 = 2e-4 Torr
Autoramp is set to 520 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Wednesday, May 27, 2020, 14:02
TGHT = 10.3 V, 508.16 A
Power supply = 10.39 V, 506 A
Omega = 2000 degC
AP = 2046.4 degC
After 3 hours at 2000 degC, the autoramp was set to 0 A,
conditions: -2 A each 10 s.
Note: There was a voltage drop of 0.6 V (fig. elog-484-fig2) |
Monday, March 23, 2020, 07:50, Marla Cervantes, , 41882-1, TARGET BOAT, Done, Conditioning graphite target #1 (T2)
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Friday, March 20, 2020, 19:39
The target material is loaded in a graphite cartridge.
The graphite cartridge is placed in a new tantalum boat previously without TaC,
the Ta boat was wrapped with three new Ta heat shields.
The system is currently pumping down.
Monday, March 23, 2020, 07:49
IGP1 = 2.2e-7 Torr
Good vacuum= 3.00 e-5 Torr
Bad vacuum = 5.00 e-5 Torr
Ramping TGHT to 40A at 0.5A/min
Monday, March 23, 2020, 10:35
Due to the COVID-19, non-essential activities are wrapped up,
the conditioning of the carbon target will be postponed until further notice |
Wednesday, May 20, 2020, 12:54, Marla Cervantes, , 41882-1, TARGET BOAT, Done, Conditioning graphite target #1 (T2)
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Marla Cervantes wrote: |
Friday, March 20, 2020, 19:39
The target material is loaded in a graphite cartridge.
The graphite cartridge is placed in a new tantalum boat previously without TaC,
the Ta boat was wrapped with three new Ta heat shields.
The system is currently pumping down.
Monday, March 23, 2020, 07:49
IGP1 = 2.2e-7 Torr
Good vacuum= 3.00 e-5 Torr
Bad vacuum = 5.00 e-5 Torr
Ramping TGHT to 40A at 0.5A/min
Monday, March 23, 2020, 10:35
Due to the COVID-19, non-essential activities are wrapped up,
the conditioning of the carbon target will be postponed until further notice
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Wednesday, May 20, 2020, 12:50
On May 19 the pumps of EVAP2 were turned on to purge the system
Today Aaron made a leak check, for details, visit elog-481
Currently IGP1 = 8.17e-7 Torr
Thursday, May 21, 2020, 09:41
IGP1 = 4.5e-7 Torr
TGHT = 0.03 V, 0.028 A
Current will be increased manually to 10 A, and then it will be autoramp to 500 A
Whit this power supply the current increments are register since the beging
TGHT = 0.145 V, 10.35 A
During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to 50A:
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 10:39
The autoramp reached the 50 A set
TGHT = 0.65 V, 49.05 A
Power supply = 0.64 V, 50 A
IGP1 = 4.7e-7 Torr
Everything looks good, autoramp is set to 80 A same conditions
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 10:49
The autoramp reached the 80 A set
TGHT = 1.075 V, 79.36 A
Power supply = 1.07 V, 80 A
IGP1 = 1.7e-6 Torr and increasing
Autoramp is set to 100 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
There was a jump in the vacuum e-log-482-fig-1.
Thursday, May 21, 2020, 11:01
The autoramp reached the 100 A set
TGHT = 1.4V, 99.9 A
Power supply = 1.4V, 100 A
IGP1 = 0.001 Torr and increasing
Autoramp is set to 120 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 11:12
TGHT = 1.75 V, 120.6 A
Power supply = 1.74 V, 120 A
IGP1 = 0.0018 Torr
The current will be hold and to let the vacuum reduce
Thursday, May 21, 2020, 11:34
TGHT = 1.8 V, 120.825 A
Power supply = 1.74 V, 120 A
IGP1 = 9.8e-5 Torr
Thursday, May 21, 2020, 11:37
Autoramp is set to 300 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 12:21
TGHT = 5.015 V, 298.125 A
Power supply = 5 V, 300 A
IGP1 = 4.77e-5 Torr
Omega = 1130 degC
Note: Measurments will be taken with ARIEL's pyrometer (I will call it AP in this elog).
The emmisivity this pyrometer accounts for is 0.91 for the range of 1000 C to 1800 C
Above 01800 it will use 0.93 as the emissivity
AP = 977.7 degC
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Monday, March 16, 2020, 13:47, Marla Cervantes, , 40282-5, TARGET BOAT, Done, Conditioning graphite target #1
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Monday, March 16, 2020, 13:47
Target material characteristics: Graphite cast of 0.965g/cm3, 287 D-shaped discs, disc area 0.969cm2, total mass of 9.972g, length 10.657cm.
The target material is loaded in a graphite cartridge.
The graphite cartridge is placed in a tantalum boat previously coated with TaC,
the Ta boat was wrapped with two used Ta heat shields.
The system is currently pumping down.
Tuesday, March 17, 2020, 08:11
IGP1 = 3.18e-7 Torr
Current will be increased manually to 10 A, and then it will be autoramp to 500 A
During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to:
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Tuesday, March 17, 2020, 09:03
After 30 min:
TGHT: 98.1 A, 1.48 V (the voltage is increasing)
IGP1 = 3e-4 Torr
The autoramp is set to 2 A each 10 s to 500 A
Tuesday, March 17, 2020, 09:52
At 500 A the temperature was ~1243 C
So, the autoramp was re started 2 A each 10 s to 520 A
Tuesday, March 17, 2020, 09:56
TGHT= 510 A, 9.18 V
IGP1= 8.2e-5 Torr
Pressure decreasing.
Temperature register in iR2C: 1272 C
The target will stay at 520 A for 15 min to account for thermal equilibrium, and then the current will be increased to go to 1800 C
Tuesday, March 17, 2020, 10:11
The temperature stayed at 1270 C,
The autoramp is re started: 2 A each 10 s to 600 A
Tuesday, March 17, 2020, 10:24
TGHT: 10.693 V, 588.5 A
IGP1 max 7.4e-5 Torr
Temperature after 3 min at 588.5 A: 1368 C
Tuesday, March 17, 2020, 10:34
The autoramp is re started: 2 A each 10 s to 650 A
Tuesday, March 17, 2020, 10:46
TGHT=11.99 V, 637.6 A
IGP1=5.5e-5 Torr (8e-5 Torr max)
Temperature 1459 C
The current and voltage drop 10 A and 0.3 V respectively when the autoramp is stopped
Tuesday, March 17, 2020, 10:53
The autoramp is re started: 2 A each 10 s to 700A
Tuesday, March 17, 2020, 11:04
TGHT: 13 V, 686.59 A
IGP1: 6.2e-5 Torr (Max 8.7e-5Torr)
Temperature: 1507 C
Tuesday, March 17, 2020, 11:05
The autoramp is re started: 2 A each 10 s to 800A
Tuesday, March 17, 2020, 11:16
TGHT=14.29 V, 759 A
IGP1: 8.6e-5 Torr (Max 1e-4 Torr)
Temperature 1527 C
There is a current discrepancy in EPICs (see current discrepancy picture),
the autoramp stopped at 761 A because EPICS? reads 800 A
Increasing current manually.
Increasing the current manually did not work, because set current is at fake maximum
Tuesday, March 17, 2020, 13:43
The temperature stabilized to 1567 C. The current however was not stable ( look at the CarbonTarget - Max current)
an autoramp is set to -2 A each 10 s to 0A
The set current is going down but not the epics reading current neither the temperature. I assume the current will star going down when the set and the reading current from epics are the same.
Tuesday, March 17, 2020, 13:50
Autoramp was stopped, and current was reduced manually, at around 652 A (set current) the reading current started going down (639.5 A)
Autoramp is set to -2 A each 10s to 0 A
The tantalum boat deformed and the graphite cartridge rim broke |
Wednesday, February 11, 2015, 16:12, Laura Lambert, Empty, 41077-2, LP-SIS, Done, Conditioning graphite insert inside container - with heat shield
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Wednesday, February 11, 2015, 16:10
Container loaded into EVAP2.
3xTa heat shields.
Chamber currently being pumped down.
TGHT/ TBHT will be ramped up to 580A/ 230A or 1800C tapped up manually.
Thursday, February 12, 2015, 09:39
HS water valves opened, no leaks detected.
Tapping up manually.
Thursday, February 12, 2015, 12:07
OMEGA reached 1805C; TGHT = 415A, TBHT = 205A
Will continue to tap up manually to 2000C
Thursday, February 12, 2015, 15:19
Reached TGHT = 500A, TBHT = 230A, OMEGA = 2035C.
Sat for ~2hrs.
Tapping up a further 25A on the TGHT.
Thursday, February 12, 2015, 16:05
Tapped up manually to:
OMEGA = 2250C
DV = 5.65V
TGHT = 580A
TBHT = 230A
Friday, February 13, 2015, 10:05
Reached max setpoint last night.
Voltage starting to increase at contant TGHT @ 580A. Lower TGHT to 525A, temp at 2150C (time 6:30pm)
Initiating manual cool down.
Friday, February 13, 2015, 15:31
vented and opened up this afternoon.
everything looked good, container not broken! graphite insert looked good! the container was slightly bent, but nothing of significance.
however, the graphite insert bonded to the container so it was not taken out in one piece... |
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