Tuesday, May 21, 2019, 17:57
A tantalum tube previously coated with TaC and sintered was loaded with graphite foils.
The mass of the foils was 20.04 g.
The system will be heated to 2000 C to find out the corresponding current.
After that the tantalum tube will be trasferred to the EVAP1
and it will be heated there for 5 days.
EVAP2 currently pumping down
Thursday, May 23, 2019, 05:48
IGP1 = 2.516e-7 Torr
Manually tap to 50 A
Autoramp set to 1 A/min to 400 A
Thursday, May 23, 2019, 13:09
IGP1 = 3.78e-6 Torr
TGHT = 6.4 V, 401.3 A
Temperature reading = 1629
Thursday, May 23, 2019, 13:09
Autoramp was set to 550 A at 1 A/min
Stopped at 530 A
Thursday, May 23, 2019, 21:27
IGP1 = 6.77e-7 Torr
TGHT = 9.2175 V, 507.375 A
After 6 hours at ~2000 C the autoramp was set to -2 A/min to 0 A
Friday, May 24, 2019, 8:46
EVAP2 was vented with air and the tantalum tube was removed, examined and transferred to EVAP1 |