Tuesday, June 09, 2015, 9:16

Target container is coated with TaC. No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min.

TBHT will be ramped up to 230A at 01A/min.

Chamber is currently being pumped down.

 Tuesday, June 09, 2015, 15:37

HS water valves were opened. no leaks detected.

Tapped up manually to 35A.

Once vacuum stabilized after ~45min, initiated auto-ramp.

 Wednesday, June 10, 2015, 08:02

IGP1 = 5.3e-7 Torr.

TGHT = 250A and TBHT = 140A.

Increasing auto ramp to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

John Wong wrote:

Laura Lambert wrote:  Thursday, June 04, 2015, 9:07 Container was sprayed with TaC and let dry. Container has 3x Ta heat shields including center block. Container was loaded into EVAP2 yesterday and pumped down overnight. HS water valves were opened up this morning, no leaks detected. IGP1 = 4.6e-7 Torr. Tapped up manually to 40A. Waited ~25min, Vacuum stable. IGP1 = 5.0e-7 Torr. Initiating auto-ramp. TGHT will be ramped to reach 2000C  Friday, June 05, 2015, 10:01 IGP1 = 4.5e-7 Torr. TGHT = 313A, 4.47V OMEGA = 1444C Increasing ramping rate to 1.0A/min  Friday, June 05, 2015, 11:31 IGP1 = 1.2e-6 Torr. Increasing ramping rate to 2.0A/min    Friday, June 05, 2015, 12:01 TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down Cooling down process can be initiated after 4 hours.

 Friday, June 05, 2015, 13:21

OMEGA = 1995C

Increasing TGHT to 470A to achieve desired max temperature of 2000C

Friday, June 05, 2015, 15:59

TGHT sat at max desired temperature of 2000C for ~4hrs.

TGHT = 470A, 7.7V

Initiating auto-cool at 1.0A/min.

 Monday, June 08, 2015, 11:31

Vented in air and opened up this morning.

Target container mostly sintered, two tiny patches near both ends not fully sintered.

Will re-install and re-sinter next week as another container with priority needs to be sintered first.

 Tuesday, June 09, 2015, 10:45

See attachements for 'not-fully-sintered' photos

Laura Lambert wrote:

Thursday, June 04, 2015, 9:07 Container was sprayed with TaC and let dry. Container has 3x Ta heat shields including center block. Container was loaded into EVAP2 yesterday and pumped down overnight. HS water valves were opened up this morning, no leaks detected. IGP1 = 4.6e-7 Torr. Tapped up manually to 40A. Waited ~25min, Vacuum stable. IGP1 = 5.0e-7 Torr. Initiating auto-ramp. TGHT will be ramped to reach 2000C  Friday, June 05, 2015, 10:01 IGP1 = 4.5e-7 Torr. TGHT = 313A, 4.47V OMEGA = 1444C Increasing ramping rate to 1.0A/min  Friday, June 05, 2015, 11:31 IGP1 = 1.2e-6 Torr. Increasing ramping rate to 2.0A/min

 Friday, June 05, 2015, 12:01

TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down

Cooling down process can be initiated after 4 hours. 

 Thursday, June 04, 2015, 9:07

Container was sprayed with TaC and let dry.

Container has 3x Ta heat shields including center block.

Container was loaded into EVAP2 yesterday and pumped down overnight.

HS water valves were opened up this morning, no leaks detected.

IGP1 = 4.6e-7 Torr.

Tapped up manually to 40A.

Waited ~25min, Vacuum stable.

IGP1 = 5.0e-7 Torr.

Initiating auto-ramp.

TGHT will be ramped to reach 2000C

 Friday, June 05, 2015, 10:01

IGP1 = 4.5e-7 Torr.

TGHT = 313A, 4.47V

OMEGA = 1444C

Increasing ramping rate to 1.0A/min

 Friday, June 05, 2015, 11:31

IGP1 = 1.2e-6 Torr.

Increasing ramping rate to 2.0A/min

John Wong wrote:

John Wong wrote: Laura Lambert wrote:  Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C    Monday, June 01, 2015, 17:59 After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly.  There is a film coated on the window port and that could affect the temp reading. To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C.  Will keep at 830A for 4 hours and cool down this evening.  Recommend: Using Ta-heat shields for sintering next time.  Monday, June 01, 2015, 22:55 TGHT at 830A for almost 5 hours.   TEMP has gone up to 1994C.  Voltage has also gone up to 19V.   Cooling down at 2A/min for TGHT and 1A/min for TBHT.     Tuesday, June 02, 2015, 12:37 Chamber was vented and the target was inspected.  Some stressed marks on the target container can be observed. The container is also slightly curved but otherwise it's fine.  The materials packed length has expended outward so 3 discs were removed in order to insert the end caps.  The packed length is now 16cm. Two extra graphite foils were inserted on both ends, and previously coated/sintered TaC-end caps are inserted and expended.  Rn foil is inserted & Std solutions are added.  Ready for test-stand. Link to photos for more details: https://www.dropbox.com/sh/0cra7viqs9ro8q3/AADEGk8goGI4c-uzRQSGwWmxa?dl=0

 see attachment for data recorded during ZrC conditioning 

John Wong wrote:

Laura Lambert wrote:  Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C    Monday, June 01, 2015, 17:59 After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly.  There is a film coated on the window port and that could affect the temp reading. To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C.  Will keep at 830A for 4 hours and cool down this evening.  Recommend: Using Ta-heat shields for sintering next time.  Monday, June 01, 2015, 22:55 TGHT at 830A for almost 5 hours.   TEMP has gone up to 1994C.  Voltage has also gone up to 19V.   Cooling down at 2A/min for TGHT and 1A/min for TBHT.

 Tuesday, June 02, 2015, 12:37

Chamber was vented and the target was inspected. 

Some stressed marks on the target container can be observed.

The container is also slightly curved but otherwise it's fine. 

The materials packed length has expended outward so 3 discs were removed in order to insert the end caps. 

The packed length is now 16cm.

Two extra graphite foils were inserted on both ends, and previously coated/sintered TaC-end caps are inserted and expended. 

Rn foil is inserted & Std solutions are added. 

Ready for test-stand.

Link to photos for more details:

https://www.dropbox.com/sh/0cra7viqs9ro8q3/AADEGk8goGI4c-uzRQSGwWmxa?dl=0

Laura Lambert wrote:

Friday, May 29, 2015, 11:21 Total number of foils: 425 discs Total mass of materials [incl graphite foils]: 44.41g Total length packed: 12.3cm Container has no heat shields. No endcaps inserted to allow outgassing. Currently being pumped down.  Friday, May 29, 2015, 14:13 HS water valves opened, no leaks detected. IGP1 = 5.4e-6 Torr. Tapping up manually. Friday, May 29, 2015, 16:48 Tapped up manually to 20A. IGP1 = 5.9e-6 Torr. Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT. Max setpoints set to 580A and 230A for the TGHT and TBHT respectively. Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.  Monday, June 01, 2015, 09:17 IGP1 = 3.8e-6 Torr. TGHT = 478A. TBHT reached max setpoint of 230A. Increasing ramping rate to 0.5A/min.  Monday, June 01, 2015, 13:15 Checked window for temperature readings, good visibility, no coating on window.  IGP1 = 9.1e-6 Torr. TGHT reached max setpoint of 580A 30min ago. Stepping up manually to a target temperature of 2000C...  Monday, June 01, 2015, 16:25 IGP1 = 6.5e-6 Torr. TGHT = 870A, 17.90V OMEGA = 1948C

 Monday, June 01, 2015, 17:59

After almost an hour at 870A, the temperature went up from 1948C to 1980C; however temperature around the target container/legs are >2000C.  The voltage on the power supply also went up slightly. 

There is a film coated on the window port and that could affect the temp reading.

To be safe, I lowered the TGHT to 830A/17.38V, temp at 1930C. 

Will keep at 830A for 4 hours and cool down this evening. 

Recommend: Using Ta-heat shields for sintering next time.

 Monday, June 01, 2015, 22:55

TGHT at 830A for almost 5 hours.  

TEMP has gone up to 1994C.  Voltage has also gone up to 19V.  

Cooling down at 2A/min for TGHT and 1A/min for TBHT. 

 Friday, May 29, 2015, 11:21

Total number of foils: 425 discs

Total mass of materials [incl graphite foils]: 44.41g

Total length packed: 12.3cm

Container has no heat shields.

No endcaps inserted to allow outgassing.

Currently being pumped down.

 Friday, May 29, 2015, 14:13

HS water valves opened, no leaks detected.

IGP1 = 5.4e-6 Torr.

Tapping up manually.

Friday, May 29, 2015, 16:48

Tapped up manually to 20A.

IGP1 = 5.9e-6 Torr.

Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.

Max setpoints set to 580A and 230A for the TGHT and TBHT respectively.

Good Vacuum = 3.0e-5 Torr. Bad Vacuum = 4.0e-5 Torr.

 Monday, June 01, 2015, 09:17

IGP1 = 3.8e-6 Torr.

TGHT = 478A.

TBHT reached max setpoint of 230A.

Increasing ramping rate to 0.5A/min.

 Monday, June 01, 2015, 13:15

Checked window for temperature readings, good visibility, no coating on window. 

IGP1 = 9.1e-6 Torr.

TGHT reached max setpoint of 580A 30min ago.

Stepping up manually to a target temperature of 2000C...

 Monday, June 01, 2015, 16:25

IGP1 = 6.5e-6 Torr.

TGHT = 870A, 17.90V

OMEGA = 1948C

John Wong wrote:

Laura Lambert wrote:  Thursday, May 28, 2015, 11:34 Endcaps were sintered [see elog#199] A Ta foil is placed in the target boat with separate slots for each endcap [see image] The target boat is wrapped with 3-layers of Ta-heat shield. The boat is installed in EVAP2, chamber is currently being pumped down.  Thursday, May 28, 2015, 14:01 HS water valves opened, no leaks detected. IGP1 = 1.4e-6 Torr. Initiating manual tap up.  Thursday, May 28, 2015, 15:10 Manually tapped up TGHT  to 108A, 1.1V Initiating auto-ramp at 2.0A/min with a max setpoint of 300A  Thursday, May 28, 2015, 15:22 Hoping to speed up the process... IGP1 = 1.0e-6 Torr. Increasing ramping rate to 4.0A/min with a max setpoint of 500A Final desired temperature = 1800C    Thursday, May 28, 2015, 17:42 TGHT at 500A. Temp at 1780C. Increased TGHT to 580A (online operating current),  Temp 1945C, vac 2.9e-6 torr and coming down.  Will remain at that current for the sintering process. Cooling it down later this evening. Thursday, May 28, 2015, 21:27   Temp stabilized at 1960C with TGHT at 580A for almost 4 hours.  Vacuum at 1.8e-7 Torr. Cooling down initiated at 2A/min.

 Friday, May 29, 2015, 11:16

Vented in air and opened up this morning.

Endcaps look great!  

Sintering was spot on [see pictures]

Laura Lambert wrote:

Thursday, May 28, 2015, 11:34 Endcaps were sintered [see elog#199] A Ta foil is placed in the target boat with separate slots for each endcap [see image] The target boat is wrapped with 3-layers of Ta-heat shield. The boat is installed in EVAP2, chamber is currently being pumped down.  Thursday, May 28, 2015, 14:01 HS water valves opened, no leaks detected. IGP1 = 1.4e-6 Torr. Initiating manual tap up.  Thursday, May 28, 2015, 15:10 Manually tapped up TGHT  to 108A, 1.1V Initiating auto-ramp at 2.0A/min with a max setpoint of 300A  Thursday, May 28, 2015, 15:22 Hoping to speed up the process... IGP1 = 1.0e-6 Torr. Increasing ramping rate to 4.0A/min with a max setpoint of 500A Final desired temperature = 1800C

 Thursday, May 28, 2015, 17:42

TGHT at 500A. Temp at 1780C.

Increased TGHT to 580A (online operating current),  Temp 1945C, vac 2.9e-6 torr and coming down.  Will remain at that current for the sintering process.

Cooling it down later this evening.

Thursday, May 28, 2015, 21:27  

Temp stabilized at 1960C with TGHT at 580A for almost 4 hours.  Vacuum at 1.8e-7 Torr.

Cooling down initiated at 2A/min.

 Thursday, May 28, 2015, 11:34

Endcaps were sintered [see elog#199]

A Ta foil is placed in the target boat with separate slots for each endcap [see image]

The target boat is wrapped with 3-layers of Ta-heat shield.

The boat is installed in EVAP2, chamber is currently being pumped down.

 Thursday, May 28, 2015, 14:01

HS water valves opened, no leaks detected.

IGP1 = 1.4e-6 Torr.

Initiating manual tap up.

 Thursday, May 28, 2015, 15:10

Manually tapped up TGHT  to 108A, 1.1V

Initiating auto-ramp at 2.0A/min with a max setpoint of 300A

 Thursday, May 28, 2015, 15:22

Hoping to speed up the process...

IGP1 = 1.0e-6 Torr.

Increasing ramping rate to 4.0A/min with a max setpoint of 500A

Final desired temperature = 1800C

John Wong wrote:

Laura Lambert wrote:  Tuesday, May 26, 2015, 13:06 Endcaps were sprayed with TaC coating and let dry. Each endcap is wrapped separately with a sheet of graphite foil and stacked in the target boat [see image] The target boat is wrapped with 3-layers of Ta-heat shield. The boat is installed in EVAP2, chamber is currently being pumped down.  Wednesday, May 27, 2015, 08:50 HS water valves opened, no leaks detected. Stepped up manually to 35A. Initiated auto-ramp at 0.2A/min yesterday afternoon. TGHT = 254A, 3.56V. IGP1 = 5.9e-7 Torr. Increasing ramping rate to 1.0A/min with a max setpoint of 400A.    Wednesday, May 27, 2015, 17:51 TGHT has been at 400A for almost 6 hours.  Temp at 1500C. Cooling down to 0A at 1A/min. Chamber will be vented to inspect the caps.  May have to remove the graphite foil wrapped on the caps and re-sintered the caps to 1800C.

 Thursday, May 28, 2015, 08:13

Vented in air and opened up this morning.

Not fully sintered [see pictures]

Laura Lambert wrote:

Tuesday, May 26, 2015, 13:06 Endcaps were sprayed with TaC coating and let dry. Each endcap is wrapped separately with a sheet of graphite foil and stacked in the target boat [see image] The target boat is wrapped with 3-layers of Ta-heat shield. The boat is installed in EVAP2, chamber is currently being pumped down.  Wednesday, May 27, 2015, 08:50 HS water valves opened, no leaks detected. Stepped up manually to 35A. Initiated auto-ramp at 0.2A/min yesterday afternoon. TGHT = 254A, 3.56V. IGP1 = 5.9e-7 Torr. Increasing ramping rate to 1.0A/min with a max setpoint of 400A.

 Wednesday, May 27, 2015, 17:51

TGHT has been at 400A for almost 6 hours.  Temp at 1500C.

Cooling down to 0A at 1A/min.

Chamber will be vented to inspect the caps. 

May have to remove the graphite foil wrapped on the caps and re-sintered the caps to 1800C.

 Tuesday, May 26, 2015, 13:06

Endcaps were sprayed with TaC coating and let dry.

Each endcap is wrapped separately with a sheet of graphite foil and stacked in the target boat [see image]

The target boat is wrapped with 3-layers of Ta-heat shield.

The boat is installed in EVAP2, chamber is currently being pumped down.

 Wednesday, May 27, 2015, 08:50

HS water valves opened, no leaks detected.

Stepped up manually to 35A.

Initiated auto-ramp at 0.2A/min yesterday afternoon.

TGHT = 254A, 3.56V.

IGP1 = 5.9e-7 Torr.

Increasing ramping rate to 1.0A/min with a max setpoint of 400A.

John Wong wrote:

Laura Lambert wrote:  Friday, May 22, 2015, 11:43 A target boat was sprayed with TaC coating and let dry yesterday. The target boat is wrapped with 3-layers of Ta-heat shield. The boat was installed in EVAP2, chamber is currently being pumped down.  Friday, May 22, 2015, 14:22 HS water valves opened, no leaks detected. IGP1 = 2.4e-6 Torr. Tapping up manually...  Friday, May 22, 2015, 14:33 Tapped up to 20A. Vacuum jumped up to 7e-6 Torr. Backed off to 5A before vacuum started to drop again. IGP1 = 5e-6 Torr. Tapping up manually again...just more slowly...  Friday, May 22, 2015, 15:31 Tapped up to 12A, unable to tap up very fast due to volatile content in coating. IGP1 = 3.6e-6 Torr. Initiating auto-ramp at 0.1A/min with a max current of 580A.  Monday, May 25, 2015, 09:03 IGP1 = 3e-7 Torr. TGHT = 397.5A, 6.43V Increasing ramping rate to 1.0A/min.    Monday, May 25, 2015, 17:06 TGHT at been at 580A for over 4 hours.  Cooling down in process at 1A/min.

 Vented in air and opened up this morning.

Target boat looks good! fully sintered! 

Laura Lambert wrote:

Friday, May 22, 2015, 11:43 A target boat was sprayed with TaC coating and let dry yesterday. The target boat is wrapped with 3-layers of Ta-heat shield. The boat was installed in EVAP2, chamber is currently being pumped down.  Friday, May 22, 2015, 14:22 HS water valves opened, no leaks detected. IGP1 = 2.4e-6 Torr. Tapping up manually...  Friday, May 22, 2015, 14:33 Tapped up to 20A. Vacuum jumped up to 7e-6 Torr. Backed off to 5A before vacuum started to drop again. IGP1 = 5e-6 Torr. Tapping up manually again...just more slowly...  Friday, May 22, 2015, 15:31 Tapped up to 12A, unable to tap up very fast due to volatile content in coating. IGP1 = 3.6e-6 Torr. Initiating auto-ramp at 0.1A/min with a max current of 580A.  Monday, May 25, 2015, 09:03 IGP1 = 3e-7 Torr. TGHT = 397.5A, 6.43V Increasing ramping rate to 1.0A/min.

 Monday, May 25, 2015, 17:06

TGHT at been at 580A for over 4 hours.  Cooling down in process at 1A/min. 

 Friday, May 22, 2015, 11:43

A target boat was sprayed with TaC coating and let dry yesterday.

The target boat is wrapped with 3-layers of Ta-heat shield.

The boat was installed in EVAP2, chamber is currently being pumped down.

 Friday, May 22, 2015, 14:22

HS water valves opened, no leaks detected.

IGP1 = 2.4e-6 Torr.

Tapping up manually...

 Friday, May 22, 2015, 14:33

Tapped up to 20A.

Vacuum jumped up to 7e-6 Torr.

Backed off to 5A before vacuum started to drop again.

IGP1 = 5e-6 Torr.

Tapping up manually again...just more slowly...

 Friday, May 22, 2015, 15:31

Tapped up to 12A, unable to tap up very fast due to volatile content in coating.

IGP1 = 3.6e-6 Torr.

Initiating auto-ramp at 0.1A/min with a max current of 580A.

 Monday, May 25, 2015, 09:03

IGP1 = 3e-7 Torr.

TGHT = 397.5A, 6.43V

Increasing ramping rate to 1.0A/min.

 Tuesday, May 19, 2015, 13:33

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min.

TBHT will be ramped up to 230A at 0.1A/min.

Chamber is currently being pumped down

 Tuesday, May 19, 2015, 15:04

Opened up HS water, no leaks detected.

Stepped up to 35A.

Waited ~35min, vacuum stable.

IGP1 = 1.7e-6 Torr.

Initiating auto-ramp.

 Wednesday, May 20, 2015, 11:43

IGP1 = 3e-7 Torr.

TGHT = 282A, 3.8V

TBHT = 156A, 2.2V

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.

 Thursday, May 21, 2015, 10:42

IGP1 = 2.9e-7

Direct voltage = 5.48V

OMEGA = 1703C.

Initiating auto-cool at 2.0A/min  and 1.0A/min for the TGHT and TBHT.

 Friday, May 22, 2015, 11:41

Vented in air and opened up this morning.

TaC coating fully sintered, looks good! 

 Wednesday, May 13, 2015, 15:21

Three different samples of ZrC are loaded into a target boat.

Sample A: ZrC + NO graphite

Sample B: ZrC + graphite [1:0.5 molar ratio]

Sample C: ZrC + graphite [1:1 molar ratio]

Each sample consists of 20 discs, stacked together and wrapped in graphite sheet

The target boat is wrapped with 3 x Ta heat shield.

EVAP2 pumping down overnight...

 Thursday, May 14, 2015, 08:20

HS water valves opened up this a.m, no leaks detected.

IGP1 = 6.6e-7 Torr

Tapping up manually to 35A.

Good Vacuum = 3.00 e-5 Torr. Bad Vacuum = 4.00 e-5 Torr.

Thursday, May 14, 2015, 09:51

Tapped up manually to 30A.

After ~25min, vacuum gone up to IGP1 = 3.5e-5 Torr!

Backed off to 20A.

Waited ~10min. IGP1 = 1.75e-5 Torr.

Tapped back up to 25A.

Waited ~20min, IGP1 = 1.4e-5 Torr.

Tapped up to 30A.

Waited ~20min, IGP1 = 2.2e-5 Torr.

Tapped up to 35A

Waited ~50min, IGP1 = 2.5e-5 Torr.

Continuing manual tap-up...

 Thursday, May 14, 2015, 13:27

IGP1 = 9e-6 Torr

Tapped up to 40A.

Waited ~45min, IGP1 = 1e-5 Torr

Initiating auto-ramp at 0.1A/min for the TGHT with a max setpoint of 275A/ 8.0V

 Friday, May 15, 2015, 08:25

Max setpoints were changed to 400A/ 8.0V last night.

Reached 400A ~4.5hrs ago.

IGP1 = 4.9e-5 Torr

Initiating manual tap up and recording data.

 Friday, May 15, 2015, 15:50

Samples remained at ~2000C for ~4 hours [see attachment for data]

IGP1 = 7.8e-7 Torr.

Initiating auto-cool at 1.0A/min.

 Tuesday, May 19, 2015, 08:27

Vented in air and opened up this morning.

John Wong wrote:

Laura Lambert wrote:  Friday, May 01, 2015, 10:27 Four different samples of ZrC are loaded into a target boat. Sample A: ZrC + NO graphite / hand cut Sample B: ZrC + NO graphite / laser cut Sample C: ZrC + graphite / hand cut Sample D: ZrC + graphite / laser cut A picture showing the different samples is attached [one face-up/ one face-down sample of each side-by-side] Each sample consists of ~20-25 discs, stacked together and wrapped in graphite sheet [see attachment for photo] The target boat is wrapped with 3 x Ta heat shield. EVAP1 pumped down overnight. HS water valves were opened this morning, no leaks detected. IGP1 = 5.5e-7 Torr. Tapping up TGHT manually to 30A...  Friday, May 01, 2015, 10:54 Tapped up manually to 30A. Over the course of 20min the vacuum climbed to IGP1 = 1.0 e-5 Torr. Backed off TGHT to 20A to allow vacuum to stabilize. Waited ~10min. Vacuum dropped to IGP1 = 6.5e-6 Torr. Tapped back-up manually to 30A. Waited ~45min. Vacuum stable, IGP1 = 1.2e-5 Torr. Initiating auto-ramp at 0.1A/min for the TGHT with a max setpoint of 300A / 5.00V. Good Vacuum = 3.00e-5 Torr. Bad vacuum = 4.00e-5 Torr.  Monday, May 04, 2015, 11:17 IGP1 = 2e-7 Torr. TGHT = 274A, 4.75V Ramp-up limited to 275A due to max voltage being set at 5.0V Increased max voltage to 10V Tapping up manually to 1800C and recording data.    Monday, May 04, 2015, 17:24 Samples have been heated at 1800C for >2 hours.  Vaccum at 4.3e-7 Torr, TGHT 475A/9.1V. (Direct Vol = 5.3V). Initiated cooling down process.  Chamber will be vented tomorrow.  Tuesday, May 05, 2015, 10:22 TGHT reached to 0A. Chamber has already vented.  Samples will be taken out for examination.

 Friday, May 08, 2015, 15:55

see attachment for data results.