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Entry  Tuesday, June 09, 2015, 10:44, Laura Lambert, Empty, 41177-2, LP-SIS, In progress, Sintering TaC coating container for ZrC back-up 
    Reply  Wednesday, June 10, 2015, 16:35, John Wong, Empty, 41177-2, LP-SIS, In progress, Sintering TaC coating container for ZrC back-up 
       Reply  Thursday, June 11, 2015, 16:10, Laura Lambert, Empty, 41177-2, LP-SIS, In progress, Sintering TaC coating container for ZrC back-up 
          Reply  Monday, June 15, 2015, 15:30, John Wong, Empty, 41177-2, LP-SIS, Done, Re-Sintering TaC coating container for ZrC back-up 
Message ID: 213     Entry time: Thursday, June 11, 2015, 16:10     In reply to: 212     Reply to this: 217
Author: Laura Lambert 
Target Material: Empty 
Target Oven W.O#: 41177-2 
Source: LP-SIS 
Status: In progress 
Subject: Sintering TaC coating container for ZrC back-up 

John Wong wrote:

Laura Lambert wrote:

 Tuesday, June 09, 2015, 9:16

Target container is coated with TaC. No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min.

TBHT will be ramped up to 230A at 01A/min.

Chamber is currently being pumped down.


 Tuesday, June 09, 2015, 15:37

HS water valves were opened. no leaks detected.

Tapped up manually to 35A.

Once vacuum stabilized after ~45min, initiated auto-ramp.


 Wednesday, June 10, 2015, 08:02

IGP1 = 5.3e-7 Torr.

TGHT = 250A and TBHT = 140A.

Increasing auto ramp to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 

 Wednesday, June 10, 2015, 16:32

TGHT/TBHT are at 580A/230A for almost 6 hours, temp at 1728C.

Vac at 8.5e-7 Torr. 

Cooling down initiated at 1A/min.

Target container should be inspected once the chamber is vented.


 

 Thursday, June 11, 2015, 10:55

Vented in air and opened up this morning.

Same as last container sintered in evap2 [IG-LIS for UCx#13] - ends not quite fully sintered and coating not very good.

most likely due to old TaC spray.

See link for photos.

https://www.dropbox.com/sh/75o43x8y2z16e7j/AABc8Z1fTTaTRtJ5_Jr1eacWa?dl=0


 

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