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Entry  Thursday, June 04, 2015, 11:10, Laura Lambert, Empty, , LP-IG-LIS, In progress, Sintering TaC coating container for UCx 
    Reply  Friday, June 05, 2015, 12:19, John Wong, Empty, , LP-IG-LIS, In progress, Sintering TaC coating container for UCx 
       Reply  Friday, June 05, 2015, 13:22, Laura Lambert, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx IMG_20150608_145926159.jpgIMG_20150608_145950384.jpg
          Reply  Wednesday, June 10, 2015, 12:15, John Wong, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx 
             Reply  Friday, June 12, 2015, 14:59, Laura Lambert, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx 
                Reply  Friday, June 12, 2015, 16:08, John Wong, Empty, 40860-1, LP-IG-LIS, In progress, Re-Sintering TaC coating container for UCx 
                   Reply  Sunday, June 14, 2015, 09:40, John Wong, Empty, 40860-1, LP-IG-LIS, Done, Re-Sintering TaC coating container for UCx 2coats.png
Message ID: 211     Entry time: Wednesday, June 10, 2015, 12:15     In reply to: 209     Reply to this: 214
Author: John Wong 
Target Material: Empty 
Target Oven W.O#: 40860-1 
Source: LP-IG-LIS 
Status: In progress 
Subject: Sintering TaC coating container for UCx 

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

 Thursday, June 04, 2015, 9:07

Container was sprayed with TaC and let dry.

Container has 3x Ta heat shields including center block.

Container was loaded into EVAP2 yesterday and pumped down overnight.

HS water valves were opened up this morning, no leaks detected.

IGP1 = 4.6e-7 Torr.

Tapped up manually to 40A.

Waited ~25min, Vacuum stable.

IGP1 = 5.0e-7 Torr.

Initiating auto-ramp.

TGHT will be ramped to reach 2000C


 Friday, June 05, 2015, 10:01

IGP1 = 4.5e-7 Torr.

TGHT = 313A, 4.47V

OMEGA = 1444C

Increasing ramping rate to 1.0A/min


 Friday, June 05, 2015, 11:31

IGP1 = 1.2e-6 Torr.

Increasing ramping rate to 2.0A/min


 

 Friday, June 05, 2015, 12:01

TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down

Cooling down process can be initiated after 4 hours. 


 

 Friday, June 05, 2015, 13:21

OMEGA = 1995C

Increasing TGHT to 470A to achieve desired max temperature of 2000C


Friday, June 05, 2015, 15:59

TGHT sat at max desired temperature of 2000C for ~4hrs.

TGHT = 470A, 7.7V

Initiating auto-cool at 1.0A/min.


 Monday, June 08, 2015, 11:31

Vented in air and opened up this morning.

Target container mostly sintered, two tiny patches near both ends not fully sintered.

Will re-install and re-sinter next week as another container with priority needs to be sintered first.


 Tuesday, June 09, 2015, 10:45

See attachements for 'not-fully-sintered' photos


 

 Wednesday, June 10, 2015, 12:06

After inspecting the target container,  the inner tube surface has "dark" patches, which may not be evenly coated or the coating layer was too think.  

See link for photos:  https://www.dropbox.com/sh/m94mjuuodwhz5jb/AADEBv_Kha_p_1An40eftWNHa?dl=0 

Attempt to re-spray the container and re-sinter.  


 

 

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