Thursday, February 16, 2017, 15:04

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block

The target consists of 200 discs of UCx with 7.3cm in length [6 packs of 5 + 170 single discs].

Discs in target are arranged as follows: 5singles / 1pack / 40singles / 1pack / 40singles / 2packs / 40singles / 1pack / 40singles / 1pack / 5singles

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 475A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog340 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

NOTE: small bug in evap1 IOC. when current is tapped up 1A, it auto-taps back down 0.01A. should be OK, but will keep an eye on evaporator during conditioning process and acct for changes.

 Friday, February 17, 2017, 09:56

IG1 = 1.56e-6 Torr

Tapped up manually to 35A

Vacuum stable.

IG1 = 1.56e-6 Torr.

Initiating auto-ramp.

 Friday, February 24, 2017, 15:09

Local TGHT 473 A 4.63 V

Monday, February 27, 2017, 09:06 

Target has remained at max setpoints for 20+hrs [epics problems and archives currently not working so unable to find out exact time]

TGHT = 475A, 4.67V

IG1 = 1.48e-6 Torr

Conditioning process is now complete.

Initiating auto-cool at 1.0A/min

 Tuesday, February 28, 2017, 12:00

UCx conditioning process complete.

Vented in Ar and transferred to glove box this morning.

 Tuesday, April 11, 2017, 09:44

A few photos taken of the target post-conditioning.

Note a few flakes came out from one end - end disc from 'open' side flaked off.

 Wednesday, October 19, 2016, 16:47

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block using one single foil/ layer

The target consists of 165 discs of UCx with 5.4cm in length

Materials: 4 packs of 5 {all made with 'modified' UC2cast} + 145 single discs{20 from 'modified cast'}

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 430A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog327 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

Thursday, October 20, 2016, 10:11

Tapped up manually to 40A

Vacuum stable.

IG1 = 4.45e-6 Torr.

Initiating auto-ramp.

 Monday, October 24, 2016, 11:19

TGHT = 254A, 2.46V

Still ramping up...~half way to final setpoint

Vacuum dropped, looks good, IG1 = 6.77e-6 Torr

 Wednesday, October 26, 2016, 09:38

Target has remained at max setpoints for ~16hrs.

TGHT = 430A, 4.25V

IG1 = 2.3e-6 Torr

Conditioning/ re-carbonization process is now complete.

Initiating auto-cool at 1.0A/min

 Thursday, October 27, 2016, 15:35

UCx done.

Vented in Ar and transferred to glove box.

Looked inside before inserting 2nd endcap - clean view all the way through the materials to the endcap/ no visible shifting.

Ta coated spring helped hold materials in place, materials expanded minimally ~0.5cm

Pushed materials back to desired length.

Successfully removed a single disc for further analysis.

Second endcap now in with 2x graphite foils.

Both endcaps need expanding.

Ready for assembly.

Requires Rh foil - to be inserted during assembly.

Monday, July 11, 2016, 15:54

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block - new wrapping method-see elog112 evap2

The target consists of 216 discs of UCx with 7.6cm in length [4 packs of 5 + 196 single discs].

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 410A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog308 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

 Tuesday, July 12, 2016, 08:50

IG1 = 5.3e-6 Torr

Tapped up manually to 35A

Vacuum stable.

IG1 = 5.25e-6 Torr.

Initiating auto-ramp.

 Friday, July 15, 2016, 16:59

With evap2 not working, water was turned off to check valves...this tripped off evap1 since this also turned off the water to evap1.

TGHT was ~115A when evap1 tripped off.

Vacuum stable = 2.9e-6 Torr.

Tapped back up manually to 115A, 1.08V

Vacuum stable = 2.8e-6 Torr.

Restarting auto ramp at 0.1A/min.

 Friday, July 22, 2016, 16:25

Target has remained at max setpoints for 4.5days.

TGHT = 410A, 3.99V

IG1 = 2.5e-6 Torr

Voltage has wavered a small amount, between 3,91V-4.02V; this can be seen in the photo attached of the screenshot of the striptool.

Conditioning process is now complete.

Initiating auto-cool at 1.0A/min

 Tuesday, July 26, 2016, 16:48

Vented in Ar and currently transfering into glove box

will update elog tomorrow...

 Wednesday, July 27, 2016, 14:56

had a few problems with the transfer chamber in the glove box, but managed to get the target into the glove box okay last night.

was exposed to oxygen for minimal amount of time - transfer chamber wasnt flushing properly/ leak in james bond box

 Wednesday, May 18, 2016, 15:05

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block - new wrapping method-see elog112 evap2

The target consists of 200 discs of UCx with 7.4cm in length [4 packs of 5 + 180 single discs].

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 460A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog291 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

 Thursday, May 19, 2016, 09:25

IG1 = 3.4e-6 Torr

Tapped up manually to 35A

Vacuum stable.

IG1 = 3.5e-6 Torr.

Initiating auto-ramp.

 Wednesday, May 25, 2016, 13:05

Target has been heated at 460A, 4.5V for 5 hrs.

Vacuum at 6.4e-6 Torr. 

Initiated cool down at 1A/min. 

 Friday, May 27, 2016, 11:14

UCx done.

Vented in Ar and put in glove box yesterday.

Looked inside before inserting 2nd endcap - clean view all the way through the materials to the endcap/ not much visible shifting.

Ta coated spring helped hold materials in place.

Slightly darker markings on legs of container on side that was open in evap1.

2nd endcap put in.

Ready for assembly.

 Thursday, February 18, 2016, 15:34

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block - same method as for sintering TaC coating [new wrapping method-see elog112 eva2].

The target consists of 244 discs of UCx with 7.8cm in length.

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open

The chamber is currently pumping down.

TGHT will be ramped up to 520A at 0.1A/min

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

 Friday, February 19, 2016, 08:28

IG1 = 4.7e-6 Torr

Tapped up manually to 35A.

Waited ~1hr, vacuum stable

IG1 = 3.8e-6 Torr.

Initiating auto-ramp.

Laura Lambert wrote:

Thursday, February 18, 2016, 15:34 Target container was previously coated with TaC spray and sintered. Container is wrapped with 3 layers of Ta-heat shield, including the center block - same method as for sintering TaC coating [new wrapping method-see elog112 eva2]. The target consists of 244 discs of UCx with 7.8cm in length. A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open The chamber is currently pumping down. TGHT will be ramped up to 520A at 0.1A/min Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.  Friday, February 19, 2016, 08:28 IG1 = 4.7e-6 Torr Tapped up manually to 35A. Waited ~1hr, vacuum stable IG1 = 3.8e-6 Torr. Initiating auto-ramp.

 Friday, February 26, 2016, 10:26

Target has been heated at 520A for 10 hrs.

Vacuum at 5.3e-6 Torr. 

Initiated cool down at 1A/min. 

Remember to vent with Ar. 

John Wong wrote:

Laura Lambert wrote:  Thursday, February 18, 2016, 15:34 Target container was previously coated with TaC spray and sintered. Container is wrapped with 3 layers of Ta-heat shield, including the center block - same method as for sintering TaC coating [new wrapping method-see elog112 eva2]. The target consists of 244 discs of UCx with 7.8cm in length. A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open The chamber is currently pumping down. TGHT will be ramped up to 520A at 0.1A/min Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.  Friday, February 19, 2016, 08:28 IG1 = 4.7e-6 Torr Tapped up manually to 35A. Waited ~1hr, vacuum stable IG1 = 3.8e-6 Torr. Initiating auto-ramp.    Friday, February 26, 2016, 10:26 Target has been heated at 520A for 10 hrs. Vacuum at 5.3e-6 Torr.  Initiated cool down at 1A/min.  Remember to vent with Ar.

 Monday, February 29, 2016, 16:15

Vented in Ar.

Target removed from evap1 this morning.

Currently sitting in glovebox.

Weird red discharge on the end of the right side, inside the container [wrt ionizer tube into page] - same side with no endcap during carbonization.

Materials look good, both endcaps inserted.

Rh foil still needs to be implanted.

 Wednesday, March 02, 2016, 10:13

The discoloration appears to be a simple change in the morphology of the TaC coating, future tests would need to be done to confirm this estimation.

This should not effect the container/ target.

See photo attached.

Thursday, October 15, 2015, 15:52

Target container previously sintered with TaC in Evap#2 - Target current at 440A, temp measured at 1900C.  A few tests on the temp measured were done (see Evap#2 elog #251 & 252). 
Note:  This is the new design container with a small back block.

Container is loaded with 245 discs of UC2; measured disc length 7.5 cm

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring.

3 layers of Ta-heat shield is used. 

Target heater will be ramped up to 440A (according to the achieved temperature from Evap#2). 

Ramping rate at 0.1A/min.

Monitor closely on the vacuum around 400A to see if the carbonization process is complete. 

Chamber is currently being pumped down. 

 Friday, October 16, 2015, 10:33

Chamber has pumped down to 2e-6 Torr. 

Stepping up TGHT to 70A/0.23V. 

 Friday, October 16, 2015, 14:55

TGHT stepped up to 70A, pressure went to max 5.7e-5 Torr and it's coming down.

Initated autoramping.  (good vac at 5e-5 Torr, bad at 6.0e-5 Torr)

 Thursday, October 22, 2015, 12:26

TGHT has reached 440A/4.403V and stablized for about 5 hours. 

Pressure started coming down at around 370A which indicated the ending of the carbonization process. 

Currently vacuum is at 5.6e-6 torr. 

Initiated cooling down process at 2A/min.

John Wong wrote:

Thursday, October 15, 2015, 15:52 Target container previously sintered with TaC in Evap#2 - Target current at 440A, temp measured at 1900C.  A few tests on the temp measured were done (see Evap#2 elog #251 & 252).  Note:  This is the new design container with a small back block. Container is loaded with 245 discs of UC2; measured disc length 7.5 cm A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring. 3 layers of Ta-heat shield is used.  Target heater will be ramped up to 440A (according to the achieved temperature from Evap#2).  Ramping rate at 0.1A/min. Monitor closely on the vacuum around 400A to see if the carbonization process is complete.  Chamber is currently being pumped down.   Friday, October 16, 2015, 10:33 Chamber has pumped down to 2e-6 Torr.  Stepping up TGHT to 70A/0.23V.   Friday, October 16, 2015, 14:55 TGHT stepped up to 70A, pressure went to max 5.7e-5 Torr and it's coming down. Initated autoramping.  (good vac at 5e-5 Torr, bad at 6.0e-5 Torr)  Thursday, October 22, 2015, 12:26 TGHT has reached 440A/4.403V and stablized for about 5 hours.  Pressure started coming down at around 370A which indicated the ending of the carbonization process.  Currently vacuum is at 5.6e-6 torr.  Initiated cooling down process at 2A/min.

 Monday, October 26, 2015, 16:18

Target vented in argon, taken out and currently in glove box.

Target looks good, last one of the year! 

Endcaps inserted and need to be expanded, Rh foil still needs to be added.

Friday, June 13, 2014, 15:02

Target container was previously coated and sintered with TaC.  It's wrapped with 3-layers of Ta heat shield, including the center block.

The target consists of 280 discs of UCx with 9cm in length.

A regular TaC coated/sintered endcap is inserted on right, wrt to the ionizer tube pointing down, so the left end is open with no cap to allow out-gassing.

The chamber is being dumping down.

TGHT will be ramped up to 520A - keep heating at that current for ~4 to 5 hours.

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac. The auto-ramping rate is set to 0.1A/min.

 Friday, June 13, 2014, 16:26

Pressure at 1.9e-5 Torr. 

Initiate auto-ramping- stepping up from 0A at 0.1A/min - leaving for the weekend.

 Wednesday, June 25, 2014, 11:45

TGHT has reached 520A and target has been conditioned at that current for 13hrs. 

Auto-cooling initiated at 2A/min.

Once the target is cooled, the chamber will be vented in Ar.

 Friday, July 04, 2014, 10:06

Process is complete.  Target is stored in the Ar-glove box and ready for assembly.

Thursday, May 30, 2013, 16:16

The target container was previously coated with TaC and sintered in Evap 2.

The target is loaded with 250 discs of UCx (material from batch#03_02042013)

Total length = 8.9cm

The container is wrapped with 3 layers of Ta-heat shield, including the back block.

A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap. 

(Did not use a D-cap... trying out this method.  Need to be careful when handling the target!)

The chamber is dumping down.

 Instructions for conditioning the UCx target:

1.  TGHT will need to heat up to ~175A to burn off the organics. 

      Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min.

2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min.

3.  Purge the glovebox with argon gas. 

4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented.

5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap. 

6.  Clean the chamber with TCE and remove all the gunge.

7.  Install the target back

8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process.

9.  Auto-ramp the TGHT current to 175A at 1A/min.

10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min.

11.  At 520A, keep heating the target for at least 4-5 hours.

12.  Auto ramp TGHT to 0A at 2A/min.

13.  Purge the glovebox with argon for at least 5 min

14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented.

15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box.

Done!

 Friday, May 31, 2013, 18:17

Chamber has pumped down to 6.7e-6 Torr. 

Ramping up TGHT to 175A.

 Wednesday, June 05, 2013, 11:14

TGHT reached to 227A/1.99V. (see attachment#1)

TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.

John Wong wrote:

Thursday, May 30, 2013, 16:16 The target container was previously coated with TaC and sintered in Evap 2. The target is loaded with 250 discs of UCx (material from batch#03_02042013) Total length = 8.9cm The container is wrapped with 3 layers of Ta-heat shield, including the back block. A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap.  (Did not use a D-cap... trying out this method.  Need to be careful when handling the target!) The chamber is dumping down.  Instructions for conditioning the UCx target: 1.  TGHT will need to heat up to ~175A to burn off the organics.        Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min. 2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min. 3.  Purge the glovebox with argon gas.  4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented. 5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap.  6.  Clean the chamber with TCE and remove all the gunge. 7.  Install the target back 8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process. 9.  Auto-ramp the TGHT current to 175A at 1A/min. 10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min. 11.  At 520A, keep heating the target for at least 4-5 hours. 12.  Auto ramp TGHT to 0A at 2A/min. 13.  Purge the glovebox with argon for at least 5 min 14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented. 15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box. Done!  Friday, May 31, 2013, 18:17 Chamber has pumped down to 6.7e-6 Torr.  Ramping up TGHT to 175A.  Wednesday, June 05, 2013, 11:14 TGHT reached to 227A/1.99V. (see attachment#1) TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.

 Wednesday, June 05, 2013, 16:45

Glove box purged with Ar, ~30min

Chamber vented with Ar

Target removed. chamber cleaned with TCE.

Chamber pumped back down

IG1 currently at 1.4E-4 torr

See attachment 1 before chamber was cleaned

Thursday, June 06, 2013, 11:38

Chamber has been pumped down overnight

IG1 currently at 4.7E-06 Torr, BP at 30 mTorr

TGHT will be ramped up to 220A at 1A/min

Laura Lambert wrote:

John Wong wrote: Thursday, May 30, 2013, 16:16 The target container was previously coated with TaC and sintered in Evap 2. The target is loaded with 250 discs of UCx (material from batch#03_02042013) Total length = 8.9cm The container is wrapped with 3 layers of Ta-heat shield, including the back block. A regular TaC coated/sintered endcap is inserted on left, wrt to the ionizer tube pointing out of the page.  The right end is open with no cap.  (Did not use a D-cap... trying out this method.  Need to be careful when handling the target!) The chamber is dumping down.  Instructions for conditioning the UCx target: 1.  TGHT will need to heat up to ~175A to burn off the organics.        Parameter setup:  5.0e-5 good vac, 6.0-5 bad vac.  The auto-ramping rate is set to 0.1A/min. 2.  Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min. 3.  Purge the glovebox with argon gas.  4.  Vent the chamber with Ar gas.  Close the valve when it is completely vented. 5.  Remove the target.  Be careful the left end (view from the top) is open with the D-cap.  6.  Clean the chamber with TCE and remove all the gunge. 7.  Install the target back 8.  Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process. 9.  Auto-ramp the TGHT current to 175A at 1A/min. 10.  Once the TGHT reach to 175A.  Auto-ramp TGHT to 520A at 0.1A/min. 11.  At 520A, keep heating the target for at least 4-5 hours. 12.  Auto ramp TGHT to 0A at 2A/min. 13.  Purge the glovebox with argon for at least 5 min 14.  Vent the chamber with argon gas.  Close the vavle when it is completely vented. 15.  Remove the target from the chamber and put in the "orange box" and transport to the Ar-glove box. Done!  Friday, May 31, 2013, 18:17 Chamber has pumped down to 6.7e-6 Torr.  Ramping up TGHT to 175A.  Wednesday, June 05, 2013, 11:14 TGHT reached to 227A/1.99V. (see attachment#1) TGHT is ramping down to 0A  to clean up the chamber before continue with the conditioning.      Wednesday, June 05, 2013, 16:45 Glove box purged with Ar, ~30min Chamber vented with Ar Target removed. chamber cleaned with TCE. Chamber pumped back down IG1 currently at 1.4E-4 torr See attachment 1 before chamber was cleaned     Thursday, June 06, 2013, 11:38 Chamber has been pumped down overnight IG1 currently at 4.7E-06 Torr, BP at 30 mTorr TGHT will be ramped up to 220A at 1A/min

 Thursday, June 06, 2013, 16:53

TGHT has reached to 220A; continue ramping up to 520A at 0.1A/min rate.

 Monday, June 10, 2013, 12:28

TGHT has reached to 520A; target has been heated at the current over the weekend.

IG is stabilizing at 3.7e-6 Torr. 

Initiating auto-cooling to 0A at 2A/min.

Chamber will be vented in Ar tomorrow.

 Monday, June 10, 2013, 17:50

TGHT reached to 0A. See attachment #1 for the overall process. 

 Tuesday, June 30, 2015, 13:28

Target container was previously coated with TaC spray and sintered.

It's is wrapped with 3 layers of Ta-heat shield, including the center block.

The target consists of 221 discs of UCx with 7.3cm in length.

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring.

The chamber is currently pumping down.

TGHT will be ramped up to 520A at 0.1A/min

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

 Tuesday, June 30, 2015, 14:43

IG1 = 1.8e-5 Torr.

Tapped up manually to 30A.

Vacuum stable; IG1 = 1.2e-5 Torr.

Initiating auto-ramp.

 Thursday, July 02, 2015, 08:41

EVAP1 was tripped off due to backflow preventer test this morning.

IG1 - 4.2e-6 Torr.

Tapping back-up manually before re-initiating auto-ramp.

 Thursday, July 02, 2015, 11:49

Tapped up manually to 85A, 0.65V

IG1 = 3.6e-6 Torr.

Initiating auto-ramp.

 Friday, July 03, 2015, 14:47

All water valves look good, flow is good.

WV turned back on, TGHT turned back on. 

Tapped back up manually to 20A.

IG1 = 2.3e-6 Torr

Initiating auto-ramp at 0.1A/min with a max setpoint of 150A over the weekend.

Will continue to ramp up monday.

Approved by Peter Kunz.

Laura Lambert wrote:

Tuesday, June 30, 2015, 13:28 Target container was previously coated with TaC spray and sintered. It's is wrapped with 3 layers of Ta-heat shield, including the center block. The target consists of 221 discs of UCx with 7.3cm in length. A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring. The chamber is currently pumping down. TGHT will be ramped up to 520A at 0.1A/min Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.  Tuesday, June 30, 2015, 14:43 IG1 = 1.8e-5 Torr. Tapped up manually to 30A. Vacuum stable; IG1 = 1.2e-5 Torr. Initiating auto-ramp.  Thursday, July 02, 2015, 08:41 EVAP1 was tripped off due to backflow preventer test this morning. IG1 - 4.2e-6 Torr. Tapping back-up manually before re-initiating auto-ramp.  Thursday, July 02, 2015, 11:49 Tapped up manually to 85A, 0.65V IG1 = 3.6e-6 Torr. Initiating auto-ramp.

 Thursday, July 02, 2015, 12:58

NOTE:  Before venting the EVAP1 chamber, the Ar line must disconnect from Peter's sampling chamber (inside the fumehood) and connect back to the EVAP. 

John Wong wrote:

Laura Lambert wrote:  Tuesday, June 30, 2015, 13:28 Target container was previously coated with TaC spray and sintered. It's is wrapped with 3 layers of Ta-heat shield, including the center block. The target consists of 221 discs of UCx with 7.3cm in length. A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring. The chamber is currently pumping down. TGHT will be ramped up to 520A at 0.1A/min Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.  Tuesday, June 30, 2015, 14:43 IG1 = 1.8e-5 Torr. Tapped up manually to 30A. Vacuum stable; IG1 = 1.2e-5 Torr. Initiating auto-ramp.  Thursday, July 02, 2015, 08:41 EVAP1 was tripped off due to backflow preventer test this morning. IG1 - 4.2e-6 Torr. Tapping back-up manually before re-initiating auto-ramp.  Thursday, July 02, 2015, 11:49 Tapped up manually to 85A, 0.65V IG1 = 3.6e-6 Torr. Initiating auto-ramp.    Thursday, July 02, 2015, 12:58 NOTE:  Before venting the EVAP1 chamber, the Ar line must disconnect from Peter's sampling chamber (inside the fumehood) and connect back to the EVAP.

 Friday, July 03, 2015, 13:42

water valve tripped off at ~1pm, which subsequently tripped off the TGHT [see photo]

currently trying to figure out what caused this to occur before re-starting....

 Friday, July 03, 2015, 14:47

All water valves look good, flow is good.

WV turned back on, TGHT turned back on. 

Tapped back up manually to 20A.

IG1 = 2.3e-6 Torr

Initiating auto-ramp at 0.1A/min with a max setpoint of 150A over the weekend.

Will continue to ramp up monday.

Approved by Peter Kunz.

 Monday, July 06, 2015, 09:29

TGHT reached 150A 1.5hrs ago.

Vacuum stable.

IG1 = 2.7e-5 Torr.

Re-starting auto-ramp at 0.1A/min with a max setpoint of 520A.

Laura Lambert wrote:

John Wong wrote: Laura Lambert wrote:  Tuesday, June 30, 2015, 13:28 Target container was previously coated with TaC spray and sintered. It's is wrapped with 3 layers of Ta-heat shield, including the center block. The target consists of 221 discs of UCx with 7.5cm in length. A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring. The chamber is currently pumping down. TGHT will be ramped up to 520A at 0.1A/min Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.  Tuesday, June 30, 2015, 14:43 IG1 = 1.8e-5 Torr. Tapped up manually to 30A. Vacuum stable; IG1 = 1.2e-5 Torr. Initiating auto-ramp.  Thursday, July 02, 2015, 08:41 EVAP1 was tripped off due to backflow preventer test this morning. IG1 - 4.2e-6 Torr. Tapping back-up manually before re-initiating auto-ramp.  Thursday, July 02, 2015, 11:49 Tapped up manually to 85A, 0.65V IG1 = 3.6e-6 Torr. Initiating auto-ramp.    Thursday, July 02, 2015, 12:58 NOTE:  Before venting the EVAP1 chamber, the Ar line must disconnect from Peter's sampling chamber (inside the fumehood) and connect back to the EVAP.     Friday, July 03, 2015, 13:42 water valve tripped off at ~1pm, which subsequently tripped off the TGHT [see photo] currently trying to figure out what caused this to occur before re-starting....  Friday, July 03, 2015, 14:47 All water valves look good, flow is good. WV turned back on, TGHT turned back on.  Tapped back up manually to 20A. IG1 = 2.3e-6 Torr Initiating auto-ramp at 0.1A/min with a max setpoint of 150A over the weekend. Will continue to ramp up monday.   Approved by Peter Kunz.  Monday, July 06, 2015, 09:29 TGHT reached 150A 1.5hrs ago. Vacuum stable. IG1 = 2.7e-5 Torr. Re-starting auto-ramp at 0.1A/min with a max setpoint of 520A.

 Wednesday, July 08, 2015, 10:44

The carbonization process is complete; chamber vacuum is stabilizing at 9.5e-6 Torr. 

Currently TGHT is at 430A.  Increased TGHT ramping rate to 1A/min.  Target should be at max current (520A) in 1.5 hours, so TGHT can be ramped down around 4:30pm today. 

 Wednesday, July 08, 2015, 16:36

TGHT at 520A/5.884V for over 4 hours.  Pressure coming down, currently at 1.42e-5 Torr. 

Initiated cooling at -2A/min. 

Chamber can be vented in Ar tomorrow and the target will be inspected.

Thursday, July 09, 2015, 17:08  

The target was taken out from the evaporator and inspected. 

Some "burnt" marks on the ionization legs can be observed and also the centre support leg is bent.  (see photos#1)

Not sure if the centre leg came in bent after machining or it happened during the carbonization process??  Do not have photos of the container before the process to compare.  

A few things to note…  During the process, the power supply did tripped off twice due to the cooling water valve shut off. (see photo#2).  An assumption is that sudden cool down of the hot target might have caused the quenching effect. 

No other visible damage.  

End caps are inserted and ready for assembly.

Link to photos:  https://www.dropbox.com/sh/c1ake0fu4x7lckc/AAD0F8TVRrpCbbHquEvSkyYIa?dl=0

Friday, March 20, 2015, 15:17 

Target container was previously coated with TaC spray and sintered.

It's is wrapped with 3 layers of Ta-heat shield, including the center block.

The target consists of 225 discs of UCx with 9.2cm in length.

Packing step was skipped for first time, loaded singular discs into target container, no binder holding discs together.

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open.

The chamber is currently pumping down.

TGHT will be ramped up to 520A - keep heating the current for 4-5 hours.

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

Auto ramp at 0.1A/min.

 Monday, March 23, 2015, 09:09

IOC has been rebooted.

Ion gauge won't turn on - goes into drive, then times out...

 Monday, March 23, 2015, 15:06

Both filaments in IG1 are burnt out.

EVAP1 will be vented tomorrow morning.

UCx will be placed in the pelican case under argon while the filaments are being replaced in the morning.

 Tuesday, March 24, 2015, 11:27

Vented in argon and placed target in pelican case.

Ion gauge replaced this morning.

Continued purging evap1 and re-installed UCx back into evap1.

Currently pumping back down.

 Wednesday, March 25, 2015, 09:38

IG1 = 8.65e-7 Torr

Tapped up evap1 manually to 40A.

Waited ~20min.

Vaccuum stable.

IGP1 = 7.75e-7 Torr.

Initiating auto-ramp.

 Wednesday, April 01, 2015, 15:07

TGHT has reached 520A, 5.82V - YAY!

Will continue to heat overnight and initiate ramp-down/ cooling tomorrow morning.

Slightly shorter time frame to reach max setpoints than normal - possibly due to lack of binder/ skipping packing process.

Great timing before the long weekend 

 Thursday, April 02, 2015, 09:20

Target has been conditioned at max setpoints for 20hours.

Auto-cooling ramp down initiated at 2.0A/min.

 Thursday, April 09, 2015, 16:02

Vented in argon and removed from evap1 tuesday.

Appears as though some discs may be slightly displaced, pictures to follow...

 Friday, October 17, 2014, 11:47

Target container was previously coated with TaC spray and sintered.

It's is wrapped with 3 layers of Ta-heat shield, including the center block.

The target consists of 255 discs of UCx with 10.5cm in length.

A regular TaC coated endcap is inserted right, wrt the ionizer tube pointing down, so the left is open with a removable half-cap to allow out-gassing.

The chamber was pumped down overnight.

TGHT will be ramped up to 520A - keep heating the current for 4-5 hours.

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.

Auto ramp at 0.1A/min.

 Friday, October 17, 2014, 13:25

IG1 = 2.6e-6 Torr

Manually stepped up to 35A

Waited ~1hr15

IG1 = 4.2e-6 Torr

Initiating auto-ramp.

Laura Lambert wrote:

Friday, October 17, 2014, 11:47 Target container was previously coated with TaC spray and sintered. It's is wrapped with 3 layers of Ta-heat shield, including the center block. The target consists of 255 discs of UCx with 10.5cm in length. A regular TaC coated endcap is inserted right, wrt the ionizer tube pointing down, so the left is open with a removable half-cap to allow out-gassing. The chamber was pumped down overnight. TGHT will be ramped up to 520A - keep heating the current for 4-5 hours. Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac. Auto ramp at 0.1A/min.  Friday, October 17, 2014, 13:25 IG1 = 2.6e-6 Torr Manually stepped up to 35A Waited ~1hr15 IG1 = 4.2e-6 Torr Initiating auto-ramp.

 Monday, October 20, 2014, 14:10

There were two big power bumps occurred on Saturday Oct 18 and wiped all the IOC/PLC on the Evaporators.   All the system, including TGHT/pumps/EPICS/Alarm handlers were found off.  The ion gauge was turned on this morning and showed the pressure was around 16mTorr. (see attachment).

The pump has been turned back on; pressure is currently at 3.5e-6 Torr.

Ramping up TGHT...

 Monday, November 03, 2014, 12:05

TGHT has reached to 580A and the target has conditioned at that current for about 3 days. 

Cooling down at 2A/min.

 Wednesday, November 05, 2014, 16:40

UCx conditioning complete.

Target is now in the Ar-glove box.  End caps are inserted but need to be expanded.

Need to insert Re foil prior to assembly.