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Message ID: 138     Entry time: Wednesday, October 19, 2016, 16:52
Author: Laura Lambert 
Target Material: UC2 
Target Oven W.O#: 41790-6 
Source: LP-SIS 
Status: Done 
Subject: Conditioning UCx#18 

 Wednesday, October 19, 2016, 16:47

Target container was previously coated with TaC spray and sintered.

Container is wrapped with 3 layers of Ta-heat shield, including the center block using one single foil/ layer

The target consists of 165 discs of UCx with 5.4cm in length

Materials: 4 packs of 5 {all made with 'modified' UC2cast} + 145 single discs{20 from 'modified cast'}

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down.

The right side is open with a TaC coated spring to help hold materials in.

The chamber is currently pumping down.

TGHT will be ramped up to 430A at 0.1A/min [same current used to reach 1900C in evap2 when sintering TaC coating - elog327 evap2]

Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac.


Thursday, October 20, 2016, 10:11

Tapped up manually to 40A

Vacuum stable.

IG1 = 4.45e-6 Torr.

Initiating auto-ramp.


 Monday, October 24, 2016, 11:19

TGHT = 254A, 2.46V

Still ramping up...~half way to final setpoint

Vacuum dropped, looks good, IG1 = 6.77e-6 Torr


 Wednesday, October 26, 2016, 09:38

Target has remained at max setpoints for ~16hrs.

TGHT = 430A, 4.25V

IG1 = 2.3e-6 Torr

Conditioning/ re-carbonization process is now complete.

Initiating auto-cool at 1.0A/min


 Thursday, October 27, 2016, 15:35

UCx done.

Vented in Ar and transferred to glove box.

Looked inside before inserting 2nd endcap - clean view all the way through the materials to the endcap/ no visible shifting.

Ta coated spring helped hold materials in place, materials expanded minimally ~0.5cm

Pushed materials back to desired length.

Successfully removed a single disc for further analysis.

Second endcap now in with 2x graphite foils.

Both endcaps need expanding.

Ready for assembly.

Requires Rh foil - to be inserted during assembly.


 

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