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Entry  Thursday, October 15, 2015, 16:05, John Wong, UC2, 41077-5, LP-SIS, In progress, Conditioning UCx#14 
    Reply  Monday, October 26, 2015, 16:20, Laura Lambert, UC2, 41077-5, LP-SIS, Done, Conditioning UCx#14 
Message ID: 122     Entry time: Monday, October 26, 2015, 16:20     In reply to: 121
Author: Laura Lambert 
Target Material: UC2 
Target Oven W.O#: 41077-5 
Source: LP-SIS 
Status: Done 
Subject: Conditioning UCx#14 

John Wong wrote:

Thursday, October 15, 2015, 15:52

Target container previously sintered with TaC in Evap#2 - Target current at 440A, temp measured at 1900C.  A few tests on the temp measured were done (see Evap#2 elog #251 & 252). 
Note:  This is the new design container with a small back block.

Container is loaded with 245 discs of UC2; measured disc length 7.5 cm

A regular TaC coated endcap is inserted left, wrt the ionizer tube pointing down, so the right is open - discs are held on with Ta wire spring.

3 layers of Ta-heat shield is used. 

Target heater will be ramped up to 440A (according to the achieved temperature from Evap#2). 

Ramping rate at 0.1A/min.

Monitor closely on the vacuum around 400A to see if the carbonization process is complete. 

Chamber is currently being pumped down. 


 Friday, October 16, 2015, 10:33

Chamber has pumped down to 2e-6 Torr. 

Stepping up TGHT to 70A/0.23V. 


 Friday, October 16, 2015, 14:55

TGHT stepped up to 70A, pressure went to max 5.7e-5 Torr and it's coming down.

Initated autoramping.  (good vac at 5e-5 Torr, bad at 6.0e-5 Torr)


 Thursday, October 22, 2015, 12:26

TGHT has reached 440A/4.403V and stablized for about 5 hours. 

Pressure started coming down at around 370A which indicated the ending of the carbonization process. 

Currently vacuum is at 5.6e-6 torr. 

Initiated cooling down process at 2A/min.


 

 Monday, October 26, 2015, 16:18

Target vented in argon, taken out and currently in glove box.

Target looks good, last one of the year! 

Endcaps inserted and need to be expanded, Rh foil still needs to be added.


 

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