Aurelia Laxdal wrote:

Temperature measurements in progress this week for Ta HP-SIS.

 Friday, January 08, 2016, 10:49

Rh foil added.

endcaps inserted and expanded.

total length of target with end caps = 3.45cm

spot weld one thermocouple onto center block and one thermocouple onto target leg [left side wrt ionizer tube into page].

 see elog id# 268 for more info regarding measurements taken and state of TBHT power supply...

 Thursday, November 21, 2019, 08:09: PS on. Leak issue resolved (Evap 2 Elog 466). Vacuum @ 4.10e-07T.

Thursday, November 21, 2019, 08:15: Auto-ramping TGHT / TBHT @ 2 A per min to 300 / 150 A. 

Tuesday, December 03, 2019, 08:15: Waterlines opened. Vacuum ok @ 4.06e-07T

Tuesday, December 03, 2019, 08:23: Unable to start due to flow trip? PS off. 

Tuesday, December 03, 2019, 08:25: Turbo & Vac off. 

Tuesday, December 03, 2019, 08:51: Vented. Investigate. Install outer shields. Loose wire found on exterior paddle. Trip gone. Roughing. 

Tuesday, December 03, 2019, 09:03: Turbo pump on. 

Tuesday, December 03, 2019, 09:12: PS on. Vacuum @ 4.46e-05T and dropping. 

Wednesday, December 04, 2019, 10:21: Manually tapped up the TGHT / TBHT to 35 / 10 A.

Wednesday, December 04, 2019, 10:22: Auto-ramping TGHT / TBHT to 300 / 150 A @ 2 A per min. 

FM

Wednesday, December 04, 2019, 13:48:  Auto-ramping TGHT / TBHT to 350 / 175 A @ 2 A per min. 

Wednesday, December 04, 2019, 14:20: Auto-ramping TGHT / TBHT to 400/ 190 A @ 2 A per min.  

Thursday, December 05, 2019, 10:58: Checking the striptool, approximately 30 minutes ago there was an oscillatory behaviour on the TGHT power. It went down to 0 in a very short time.

Temperature measurements were recorded and indicate a 70C difference from before the event.

 Thursday, December 05, 2019, 15:08: Auto-ramping TGHT / TBHT to 450/ 230A @ 2 A per min.  

Thursday, December 05, 2019, 19:05: Checking the striptool, at around 6 pm the TGHT power supply trip and didn't come back.

Thursday, December 05, 2019, 19:06: Drop in temperature indicates the target stop glowing.

Thursday, December 05, 2019, 19:07> Turning off power supply on EPICS and setting the slider to 0A.

I will ramp up TGHT in the morning while in the lab. 

Friday, December 06, 2019, 14:55: Ramping down TBHT to 0A @ 2A/min 

Tuesday, December 10, 2019, 09:11: Manually tapped up the TGHT / TBHT to 35 / 10 A 

Tuesday, December 10, 2019, 09:12:  Auto-ramping TGHT / TBHT to 400/ 230A @ 2 A per min.  

Aborted

Wednesday, May 11, 2016, 17:15

Nanofiber SiC (~50nm grain size)/PAN was prepared at UBC. 

SiC 0.50g, DMF 9.0g, PAN 1.0g, tiny bit of SDS.

The fiber mat was stabilized in air at 250C and then cut into discs, initial mass = 0.1072g

Discs were then bounded with PVA on 9 pieces of rounded graphite foil  (green mass gained to 0.6031g)

The stack of naofiber SiC/PAN was loaded on to Ta boated (coated) and wrapped with Ta heat shield. 

Chamber is currently being pumped down.

 Friday, May 13, 2016, 15:00

TGHT at 390A/6.966V.  Temp measured at 1615C. 

Will keep at that temperature for a few days.

 Monday, May 16, 2016, 15:44

Sample has been heated at ~1600C for 4 days.  TGHT at 400A/7.02V. 

Cooling down at 2A/min

 Tuesday, May 17, 2016, 11:18

Chamber vented.  Inspecting samples.

Tuesday, October 08, 2019, 14:14: Remove Flex line HS. 

HS: 42752-1

Waterlines not open yet.

Tuesday, October 08, 2019, 14:15: roughing.

Tuesday, October 08, 2019, 14:24: Turbo pump on. 

Tuesday, October 08, 2019, 14:32: TP @ speed. 

Wednesday, October 09, 2019, 13:24 

The initial pressure was 3.25e-7 Torr

The current was manually increased to 25 A on both TBHT and TGHT  at a rate of 1 A each 30 s for both heaters.

Wednesday, October 09, 2019, 13:33

At 1 pm an additional ram was made to TGHT 350 A and TBHT 200 at same rate.

 HS 42752-5 - Setup for Temperature mapping.

Friday, November 15, 2019, 13:26: Roughing. 

Friday, November 15, 2019, 13:36: Turbo pump on. 

Monday, November 18, 2019, 07:46: Waterlines opened. Vacuum ok @ 3.56e-07T.

Monday, November 18, 2019, 07:48: PS on.

Monday, November 18, 2019, 09:21: PS off. Vacuum slowly spiked to 1.23e-06T. Indicative of a small water leak. 

Monday, November 18, 2019, 09:24: HS waterlines purged. vacuum dropped to 5.54e-07T. 

Monday, November 18, 2019, 09:27: Valves closed. TP off. BP off.

Monday, November 18, 2019, 10:27: Venting.

Monday, November 18, 2019, 11:06: Gaskets checked / replaced. Roughing. 

Monday, November 18, 2019, 11:14: turbo pump on. 

Monday, November 18, 2019, 14:19: Waterlines opened. 

Monday, November 18, 2019, 14:23: Response on vacuum. Leak is still present & a higher rate (Has an immediate response). Turbos off. 

Monday, November 18, 2019, 14:28: Venting. 

Monday, November 18, 2019, 14:49: turbo pump on. 

Tuesday, November 19, 2019, 07:07: Waterlines opened. Leak is present.  Turbo pump off. 

Tuesday, November 19, 2019, 11:24: After venting, changed 1 gasket. Setup LD & completed a leak check with the lines pressurized to 75 PSI of He. 

Tuesday, November 19, 2019, 11:25: Roughing. 

Tuesday, November 19, 2019, 11:33: Turbo pump on. 

Wednesday, November 20, 2019, 08:59: Waterlines opened. Leak is present.  Turbo pump off.  

Wednesday, November 20, 2019, 11:26: FEBIAD Removed. U-Line installed to check Evap 2 Connection. FEBIAD examined outside. 

Wednesday, November 20, 2019, 11:34: Turbo pump on. 

Wednesday, November 20, 2019, 13:05: HPA off (Was running through HS line still. Vac @ 5.54e-06T).  

Wednesday, November 20, 2019, 13:07: Open waterline. Vacuum @ 3.88e-06T & dropping steadily.  

Wednesday, November 20, 2019, 13:12: Vacuum @ 3.69e-06T & dropping. No leak detected via Vac. 

Wednesday, November 20, 2019, 13:14: Waterline Closed / purged. Turbo pumps off. 

Wednesday, November 20, 2019, 13:58: Turbo pump on. 

Wednesday, November 20, 2019, 13:50: Cleaned seal / FEBIAD re-installed. Roughing.

Thursday, November 21, 2019, 08:06: Waterlines opened. Vacuum ok @ 4.10e-07T. 

Notes:

1) The FEBIAD left cooling line was the culprit for the leaks. A fine copper build up was noted on the gasket /  sealing face. Images included. 

2) Evap 2 was leak checked separately as well & is OK.

Monday, June 17, 2019, 17:04

A LP-SIS target container  was wrapped with 3 heat shielding layers,

and an empty graphite insert of 17.4 g was introduce in it.

The system was loaded in the EVAP2 and the chamber is currently being evacuated.

The container will be heated to 2000 C in order to correlate the temperature, current and voltage,

as well as to condition the container.

 Tuesday, June 18, 2019, 07:28

The TGHT and TBHT current will be tapped to 40 A manually

Autoramp will be set to TGHT 1A/min to 500 A

and TBHT 0.5A/min to 230 A.

Tuesday, June 18, 2019, 20:51

After 2 hours at ~1800 C the container was cooled,

IGP1 = 1.2e-6 Torr

TGHT = 7.16 V, 447.094 A

TBHT = 4.19 V, 233.43 A

Temperature 1793 C

 Auto ramp TGHT = -2 A/min, TBHT = -1A/min 

Thursday, December 20, 2018, 10:24

A tantalum tube was loaded in evaporator 2 on Wednesday 19/Dec/2018.

It is going to be heated to 2000 C during 3 weeks 

Pressure IGP1 =  4.88e-7 Torr

TGHT manually tapped to 40 A

Autoramp set to 2 A/min on TGHT to 400 A aiming for 1800 C

The system tripped due to a power outage.

the current went from 57 to 0 A.

The tube did not show damage signs.

Saturday, April 28, 2018, 16:09

Container is coated with TaC and wrapped with TaC heatshield. 

Will be used for carbonizing nanoSiC target materials.

Chamber is pumping down...

Sintering temp 1800C, est TGHT ~550A

 Saturday, April 28, 2018, 18:08

Pressure at 5.e-6 Torr. 

Initial auto-ramp at 1.0A/min reaching TGHT 500A.  Monitoring temp.

 Sunday, April 29, 2018, 23:37

Target temp stabilizes at 1800C with TGHT holding at 400A/7.02V for 24 hours.  Pressure at 4.4 e-7 Torr.

Lower TGHT to 338A/5.51V to reach 1600C - This will temp/current will be used for carbonizing the nanoSiC fibers.

Holding TGHT overnight to determine temp stability.

 Monday, April 30, 2018, 18:04

Temp is holding at 1600C, TGHT 338A/5.5V.  Pressure at 3.0 e-7 Torr. 

Initiated cooling down at 2A/min.

 Thursday, October 25, 2018, 10:36

Container is coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Chamber is currently being pumped down

 Friday, October 26, 2018, 08:40

Pressure at IGP1 1.06e-6 Torr. 

Tapped up TGHT and TBHT manually to 40 A

Waited 1 hr for vacuum to stabilize.

IGP1 = 8.9e-6 Torr

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Initiating auto ramp for TGHT @ 1 A/min to a max setpoint of 350 A

Initiating auto ramp for TBHT @ 0.5 A/min to a max setpoint of 230 A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900 C

 Friday, October 26, 2018, 10:46

At 62 A, the vacuum overpassed the "Bad vacuum " limit and the current reduced to 54 A.

when the pressure returned to the "Good vac" limit the ramping started automatically.

Friday, October 26, 2018, 16:59

TGHT= 450 A, Temperature = 1878 C

Ramping rate increased to 1A/min for the TBHT.

Tapped manually to 454 A, Temperature 1880 C.

Saturday, October 27 2018, 10:00 

Ramping down to 0 A @ 2 A/min.

Monday, October 29, 2018, 12:39

 Venting EVAP2, TaC coat sintering completed.

 Wednesday, October 31, 2018, 19:35

Container is coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Chamber is currently being pumped down

 Thursday, November 01, 2018, 10:31

Pressure at IGP1 9.44e-7 Torr. 

Tapped up TGHT and TBHT manually to 40 A

Thursday, November 01, 2018, 12:32

Waited ~1 hr for vacuum to stabilize.

IGP1 = 1.42e-6 Torr

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Initiating auto ramp for TGHT @ 1 A/min to a max setpoint of 350 A

Initiating auto ramp for TBHT @ 0.5 A/min to a max setpoint of 230 A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900 C

 Tapped manually to 445 A, Temperature 1896 C.

Friday, November 02, 2018, 07:35

TGHT 7.86 V 445.6 A

TBHT 3.22 V 233.3 A

IGP1 1e-6 Torr

Ramping down TGHT and TBHT to 0 A @ 2 A/min.  

Friday, November 02, 2018, 17:28

Monday, October 29, 2018, 12:39

Venting EVAP2, TaC coat sintering completed. 

 Monday, November 19, 2018, 08:57

Tantalum tube was coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Pressure at IGP1 2.61-7 Torr. 

Tapped up TGHT and TBHT manually to 40 A

Waited ~1 hr for vacuum to stabilize.

IGP1 = 4.27e-7 Torr

Good vac at 3.00e-5 Torr

Bad vac at 5.00e-5 Torr.

Initiating auto ramp for TGHT @ 1 A/min to a max setpoint of 350 A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900 C

Monday, November 19, 2018, 18:14

Temperature was 1755 C at 350 A

IGP1 = 9.28e-7 Torr

Tapped manually to 393 A (6.83 V)

IGP1 = 1.4e-6 Torr

Temperature 1904 C

The tube will stay at max current point overnight.

Tuesday, November 20, 2018, 08:17

 IGP1 = 9.28e-7 Torr

TGHT = 395 A, 6.98 V

Temperature 1903 C

Auto-ramp set to TGHT 0 A @ -2 A/min. 

 Tuesday, January 15, 2018, 17:30

Tantalum tube was coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

EVAP2 currently pumping down.

 Pressure at IGP1 4.71 -7 Torr. 

Tapped up TGHT manually to 40 A

Waited ~1 hr for vacuum to stabilize.

IGP1 = 9.96-7 Torr

Good vac at 3.00e-5 Torr

Bad vac at 5.00e-5 Torr.

Initiating auto ramp for TGHT @ 1 A/min to a max set point of 350 A

Once max set points achieved, will tap up manually to final desired temperature of 1900 C

 Thursday, January 17, 2019, 15:31

The tube remained at ~1900 C for 6 hours.

IGP1=5.8e-7 Torr

TGHT = 427 A, 7.23 V

Min Temperature = 1890 C

Thursday, January 17, 2019, 15:33

 Auto-ramp set to TGHT 0 A @ -2 A/min. 

 Wednesday, April 03, 2019, 16:57

Tantalum tube was coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V).

EVAP2 currently pumping down.

 Thursday, April 04, 2019, 05:12

IGP1 = 4.5e-7 Torr

The current is tapped manually to 40 A

After1 hour IGP1 = 1.18e-6 Torr, the autoramp was set to 1 A/min to 400 A

Thursday, April 04, 2019, 18:58

After 4 hours at ~1900 C:

IGP1 = 6.13e-7 Torr 

TGHT = 6.74 V, 416.06 A

 Friday, May 10, 2019, 16:54

A tantalum tube was coated with TaC,and wrapped with three tantalum sheets,

the tube was set in the EVAP2 to sinter the TaC coating.

EVAP2 is currently pumping down. 

 Sunday, May 12, 2019, 18:40

IGP1 = 3.01e-7 Torr

Manually tapped current TGHT to 40 A

IGP1 = 4.89e-Torr

at the IGP1 = 1.961e-6 Torr the autoramp was set to 1 A/min to 380 A

IGP1 = 6.91e-7 Torr

TGHT = 6.133 V, 386.8 A, temperature 1682  C

IGP1 = 7.77e-7

TGHT=6.36V, 399A 1730 C

After 4 hours at 1895 C TGHT = 7.435 V and 445.781 A

TGHT was set -2 A/min to 0 A

The EVAP2 was vented with air and the tube was removed

Wednesday, July 25, 2018, 17:32

Container is coated with TaC and wrapped with 3 layers of Ta heat-shields.

Desired sintering temperature ~1900 C, TGHT is estimated to be ~ 445A (3.3 kW), TBHT set to 230A (as usual).

OMEGA slope set to 0.99

Good vac = 3.0 e-5 Torr, Bad vac = 5.0 e-5 Torr.

Chamber is currently being pumped down.

 Friday, July 27, 2018, 10:32

Vacuum at 9.9 e-7 Torr. 

Autoramp TGHT at 1A/min to 300A and TBHT at 1A/min to 230A. Will monitor temp and adjust TGHT to reach the desire temp.

 Friday, July 27, 2018, 16:31

TGHT reached to 1500 C, and TBHT at 230A, Temp at 1480 C, pressure at 2.e-6 Torr.

Autoramp TGHt at 1A/min to 400A.  Continue monitoring temp.

 Saturday, July 28, 2018, 12:41

TGHT at 400A/6.2V. Temp at 1730 C.  Pressure 7.4 e-7 Torr.

Tapped up TGHT to 450A/7.2V, temp at 1891 C. Holding at this current... Pressure coming down from 1.2e-6 Torr.

 Monday, July 30, 2018, 22:40

Target temp has been held at 1880 C, TGHT at 450A/7.57V, TBHT 230/4.18V, vaccum at 3.8 e-7 Torr. 

Cooling TGHT and TBHT at 2A/min and 1A/min, respectively. 

 Tuesday, July 31, 2018, 10:23

TGHT/TBHT at 0A.  Pressure at 1.5e-7 Torr. 

Process completed. 

Venting chamber.

Target containers looks good.  Transferred to Ar glovebox.

 Monday, September 10, 2018, 15:09

Container is coated with TaC and wrapped with Ta heat-shield ( 3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Chamber is currently being pumped down

 Tuesday, September 11, 2018, 09:27

Pressure at IGP1 8.61e-7 Torr. 

Auto ramping TGHT at 1A/min to reach 400A, and TBHT at 1A/min to reach 230A.

 Tuesday, September 11, 2018, 12:05

Pressure increased to 6.9e-e5 Torr and auto-ramp reduced the current:

TGHT from 94.6 A to 84.86 A

TBHT from 87.8 A to 78.87 A

(see figure EVAP2-_01)

EPICS automatically started ramping up TBHT and TGHT current when the pressure was between the good limit.

 Tuesday, September 11, 2018, 14:29

TBHT current reached ~230 A and EPICS stopped inputting current automatically. 

TBHT current reading on:

EPICS 232.8 A

Power supply: 235 A

 Tuesday, September 11, 2018, 16:53

TGHT reached 400 A, EPICS stopped auto-ramping automatically. (Fig. Heater-ramp and Plot_400A-230A)

Temperature read by OMEGA 1837 C (Fig. Tempeature-at-400A)

 Tuesday, September 11, 2018, 17:40

TGHT current was increased manually to 419 A (power supply current 422 A, EPICS plot 421.6 A) in steps of ~5A/2min

The temperature after ~30 min of being at 419 A is 1898 C.

The container will stay 5 hours at 1898 C 

Wednesday, September 12, 2018, 09:05 

EVAP2 remained at max setpoints for 5hrs

Auto-cool was set to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

The automatic ramp decreased the TBHT current to 0A, but not so for TGHT, 

TGHT only reduced to 22 A, the TGHT was manually tapped to 0A

 Wednesday, September 12, 2018, 18:30

Process completed (fig. TaC-coating). 

Chamber was vented.

Tuesday, September 04, 2018, 16:58

Container is coated with TaC and wrapped with Ta heat-shield ( 3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Chamber is currently being pumped down

 Wednesday, September 05, 2018, 10:53

Pressure at 9.5-7 Torr. 

Auto ramping TGHT at 1A/min to reach 400A, and TBHT at 1A/min to reach 230A.

 Wednesday, September 05, 2018, 17:52

Problem with TGHT readback vs setpoint.  TGHT ramped up to 400A, temp measured at 1830C.  However, the setup remained at 228A (see attachment).  The autoramping program only sees the readback; in this case, the TGHT would continue to keep ramping up until the target breaks.  The autoramping program has stopped just in time. 

TGHT stepped down to 400A (setpoint), readback at 206A/6.59V.  TGHT at 230A/4.16V.  Temperature holding at 1783C. 

Control has been informed.

 Thursday, September 06, 2018, 10:54

Target temp holding at 1773C.  Pressure at 8.5e-7 Torr. 

Ramping down TGHT and TBHT, and inspect the container later. 

Problem with the TGHT readback/setpoint will need to be investigated.

 Friday, September 07, 2018, 16:03

Target container is nicely sintered.

Awaiting for Control group to investigate with the problem on TGHT readback/setpoint. 

Friday, January 18, 2019, 15:00

Container was coated with TaC and wrapped with 3 Ta heat shields.

Desired temp = 1900 C, Omega slope set = 0.990, Auto ramping TGHT at 1A/min to reach 400A, TGHT will be tapped up accordingly to reach desired Temp.

TBHT will be set fixed at 230A (max). TBHT at 1A/min to reach 230A.

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Chamber is currently being pumped down.  Sintering will proceed next week.

 Monday, January 21, 2019, 10:17

Current pressure at IGP1 = 1.31e-7 Torr

Manual tapping to 50A on TBHT and TGHT

TBHT 38.75A, 0.41V

TGHT 37.5A, 0.07V

waiting for pressure to stabilize.

pressure  IGP1 8.0 e-7 Torr

Auto ramping TGHT at 1A/min to reach 400A, and TBHT at 1A/min to reach 230A.

 Tuesday, January 22, 2019, 09:34

TGHT reached 400A , 1800 C, however temperature dropped to 1785 C.

TGHT increased to 444A manually.  Temperature stabilized at 1880 C.  

After 10 hours, TGHT was ramped down @ 2A/min and TBHT @1A/min

Tuesday, January 22, 2019, 14:36: Evap 2 PS off. Turbo off (Around 14:10) Vented Evap 2 and removed the target container with Darwin. - AS.  

 Sunday, May 24, 2020, 06:54

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature= 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down

Good vacuum= 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Ramped TGHT and TBHT to 40A at 0.5A/min

Initial IGP1 = 2.5e-7 Torr

Sunday, May 24, 2020, 08:24

Autoramp deliver 40 A

TGHT = 0.58 V, 39.6 A

TBHT = 0.46 V, 39.81 A

IGP1 = 2.9 e-7 Torr and increasing

Heater conditions will be hold for 15 min to account for pressure changes.

 Sunday, May 24, 2020, 08:39

IGP1 = 2.7e-7 Torr and decreasing

Autoramp TGHT and TBHT at 1A/min to 400A and 230A respectively.

 Sunday, May 24, 2020, 14:57

After 15 min the autoramp stopped

TGHT = 6.8 V, 394.65 A

TBHT =4 V, 232.9 A

IGP1 = 2.2e-6 Torr and going down

Omega = 1747 degC

Autoramp set to TGHT 1A/min to 450A

Sunday, May 24, 2020, 16:07

After 15 min the autoramp stopped

TGHT = 7.7 V, 448 A

IGP1 = 2.88e-6 Torr

Omega = 1886 degC

The current will be increased manually to reach 1900 deg C

Final TGHT = 7.9 V, 453.15 A (455 A input)

Omega = 1899 degC

The TGHT and TBHT will leave at current conditions until pressure reduce (approx 4 hours)

Sunday, May 24, 2020, 20:01

TGHT = 7.9 V, 456 A

TBHT = 4 V, 232.9 A

IGP1 = 1.8e-6 Torr

Omega = 1893 degC

Initiating auto-cool at -2.0A/min and -1.0A/min for the TGHT and TBHT respectively.