Wednesday, October 31, 2018, 19:35
Container is coated with TaC and wrapped with Ta heat-shield (3 layers)
Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).
Chamber is currently being pumped down
Thursday, November 01, 2018, 10:31
Pressure at IGP1 9.44e-7 Torr.
Tapped up TGHT and TBHT manually to 40 A
Thursday, November 01, 2018, 12:32
Waited ~1 hr for vacuum to stabilize.
IGP1 = 1.42e-6 Torr
Good vac at 3.00-5 Torr
Bad vac at 5.0e-5 Torr.
Initiating auto ramp for TGHT @ 1 A/min to a max setpoint of 350 A
Initiating auto ramp for TBHT @ 0.5 A/min to a max setpoint of 230 A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900 C
Tapped manually to 445 A, Temperature 1896 C.
Friday, November 02, 2018, 07:35
TGHT 7.86 V 445.6 A
TBHT 3.22 V 233.3 A
IGP1 1e-6 Torr
Ramping down TGHT and TBHT to 0 A @ 2 A/min.
Friday, November 02, 2018, 17:28
Monday, October 29, 2018, 12:39
Venting EVAP2, TaC coat sintering completed. |