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Message ID: 421     Entry time: Wednesday, October 31, 2018, 19:35
Author: Marla Cervantes 
Target Material: TaC 
Target Oven W.O#: 39530-1 
Source: LP-FEBIAD 
Status: Done 
Subject: TaC coating/sintering for graphite insert test 

 Wednesday, October 31, 2018, 19:35

Container is coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Chamber is currently being pumped down


 Thursday, November 01, 2018, 10:31

Pressure at IGP1 9.44e-7 Torr. 

Tapped up TGHT and TBHT manually to 40 A


Thursday, November 01, 2018, 12:32

Waited ~1 hr for vacuum to stabilize.

IGP1 = 1.42e-6 Torr

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.

Initiating auto ramp for TGHT @ 1 A/min to a max setpoint of 350 A

Initiating auto ramp for TBHT @ 0.5 A/min to a max setpoint of 230 A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900 C


 Tapped manually to 445 A, Temperature 1896 C.


Friday, November 02, 2018, 07:35

TGHT 7.86 V 445.6 A

TBHT 3.22 V 233.3 A

IGP1 1e-6 Torr

Ramping down TGHT and TBHT to 0 A @ 2 A/min.  


Friday, November 02, 2018, 17:28

Monday, October 29, 2018, 12:39

Venting EVAP2, TaC coat sintering completed. 

Attachment 1: Capture.JPG  105 kB  Uploaded Friday, November 02, 2018, 18:28  | Show | Hide all
Attachment 2: Coating.jpg  131 kB  Uploaded Friday, November 02, 2018, 18:30  | Show | Hide all
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