Saturday, April 28, 2018, 16:09
Container is coated with TaC and wrapped with TaC heatshield.
Will be used for carbonizing nanoSiC target materials.
Chamber is pumping down...
Sintering temp 1800C, est TGHT ~550A
Saturday, April 28, 2018, 18:08
Pressure at 5.e-6 Torr.
Initial auto-ramp at 1.0A/min reaching TGHT 500A. Monitoring temp.
Sunday, April 29, 2018, 23:37
Target temp stabilizes at 1800C with TGHT holding at 400A/7.02V for 24 hours. Pressure at 4.4 e-7 Torr.
Lower TGHT to 338A/5.51V to reach 1600C - This will temp/current will be used for carbonizing the nanoSiC fibers.
Holding TGHT overnight to determine temp stability.
Monday, April 30, 2018, 18:04
Temp is holding at 1600C, TGHT 338A/5.5V. Pressure at 3.0 e-7 Torr.
Initiated cooling down at 2A/min.
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