Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2, Page 33 of 35  Not logged in ELOG logo
Entry  Friday, October 16, 2020, 16:31, Luca Egoriti, Empty, , TARGET BOAT, In progress, HPOG annealing 

Friday, October 16, 2020, 11:30

 Target mounted in EVAP2. Pump down started

Friday, October 16, 2020, 12:05

Pressure goes up. Checked with Ferran and he says that the valve IEVAP2:RV1 automatically closes sometimes. WEIRD, to be chacked.

Friday, October 16, 2020, 15:20

IGP2 bottoms at 0.2T, and doesn't increase recover if I close RV1 while it shouldn't (as shown before). --> Vented to restart from scratch

 

Friday, October 16, 2020, 15:45

 

Pumped down again, vacuum went down to 0.16 and then started raising until ~0.18. This time the valve was open indeed! opening and closing the valve had no effect on the vacuum as if the  booster pump was not effective

 

 

Friday, October 16, 2020, 16:27

Tried a THIRD time, this time effectively, to turn the turbo ON. I managed to, but the turbo makes weird spinning sounds every ~30 sec. Moreover, its pumping down plot seems quite weird  - see spike UP while pumping. Could it be related to a dysfunction of the backing pump?

 

Entry  Tuesday, November 24, 2020, 08:13, Aaron Schmidt, , , , , Flex - line HS installed 

Monday, November 23, 2020, 17:01: Flex-line HS installed.


Tuesday, November 24, 2020, 08:03: Vacuum @ 9.55e-07T.

Tuesday, November 24, 2020, 08:08: Vacuum Ok

Tuesday, November 24, 2020, 08:09: Modify Controls dialogue on IEVAP2:IGP1:RDVAC

Max value from 0.1 to 0.0001 to better view curve on the strip tool and monitor for vacuum spikes.

Tuesday, November 24, 2020, 08:13: TGHT / TBHT PS on. 

 

Entry  Monday, March 01, 2021, 13:58, Aaron Schmidt, , , , , Flex - line HS installed 

Flex-Line HS had been fully scrubbed out earlier. All gaskets replaced.

Empty. Quick check for leaks.

Monday, March 01, 2021, 13:57: Roughing.

Monday, March 01, 2021, 14:13: TP1 on. 

Monday, March 01, 2021, 15:18: Vacuum @ 1.01e-05T. Open HS waterline. 

Monday, March 01, 2021, 15:24: Vacuum @ 9.30e-06T & dropping. Waterline ok. 

Monday, March 01, 2021, 15:25: Turbo pump off. Vent when ready. 

Entry  Tuesday, March 16, 2021, 08:29, Darwin Ortiz Rosales, TaC, , TARGET BOAT, Done, sintering of TaC on Caps and springs 

 Tuesday, March 16, 2021, 08:28 

Each endcap is separated with a disc of graphite foil and rolled into packs of 5 within a foil envelope in a target boat.

There are also 4 coated springs, one in between endcaps and three on the ends

The boat is wrapped with 3-layers of Ta heatshields.

Chamber pumping down

OMEGA slope = 0.99

Will ramp TGHT up to 40 A then autoramp to 400A at 1A/min.

Final desired temperature on OMEGA (tap)= 1800C


Tuesday, March 16, 2021, 11:22

 IGP1= 3.5e-06 Torr

TGHT = 40A, 0.4V

Will ramp up at 1A/min to 400 A


Wednesday, March 17, 2021, 08:06

IGP1=  2.98 e-07 Torr

TGHT = 400 A, 4.3V

OMEGA shows no temperature reading.  Will ramp up to 450A at 1A/min

 


Wednesday, March 17, 2021, 08:58

OMEGA still shows no reading

IGP1= 4.2e-07 Torr

ramping to 470A @ 1A/min 


Wednesday, March 17, 2021, 09:21

OMEGA no reading

IGP1 = 4.4 e-07 Torr

TGHT = 470 A, 5V

ramp up to 490 A at 1A/min


Wednesday, March 17, 2021, 11:05 

TGHT at 490 A, 5.2 V since 10 am.  Will start cooling at 2 pm.  


Wednesday, March 17, 2021, 13:47

TGHT = 493A, 5.3V

IGP1= 3.2e-07 Torr and stable

Start ramp down at -2A/min


Thursday, March 18, 2021, 11:20 

The boat was dismounted but the materials had not sintered properly.  The boat looked very twisted.  Everything was transferred to a new boat with uncoated Ta caps at either end.  

It was left overnight to establish vacuum.


Friday, March 19, 2021, 08:23

IGP1= 2.2 e-07 Torr

initiate heating at 1A/min on TGHT to 60 A


Friday, March 19, 2021, 10:04

IGP1= 3.6 e-07 Torr

TGHT = 60 A, .73 V

Ramp up to 450 A @ 2A/min

 


Friday, March 19, 2021, 14:26

OMEGA 1895 at 455A, 8.4 V

manually ramp down to 1800C

OMEGA 1800C at 416A, 7.6V

will leave like that for 3 hours more


Friday, March 19, 2021, 17:12

OMEGA 1795 C

 TGHT = 415A, 7.6V

IGP1= 6.8e-07 Torr

Start ramp down at -2A/min


Monday, March 22, 2021, 23:07 

Marla removed from Evap 2.  Sintering vwas very good.  The container with Ta caps is better for sintering these pieces.

 

Entry  Tuesday, March 23, 2021, 08:07, Aaron Schmidt, , , , , Re - Ta test. Leak check. 

 Modified HS installed with new brackets as per Marla.

Tuesday, March 23, 2021, 08:02: Vacuum @ 3.64e-07T. Waterlines opened.

Tuesday, March 23, 2021, 08:06: Vacuum @ 3.60e-07T. Stable.

Entry  Thursday, March 25, 2021, 07:57, Aaron Schmidt, , , , , Re - Ta test. Leak check. 

Thursday, March 25, 2021, 07:55: Vacuum @ 5.12e-07T. Waterlines opened.

Thursday, March 25, 2021, 07:55: Vacuum @ 5.09e-07T. Stable.

Entry  Friday, June 11, 2021, 08:41, Darwin Ortiz Rosales, Nb, , TARGET BOAT, Done, Nb treatment for Norman 

 Friday, June 11, 2021, 08:05

Target boat with a layer of niobium foil on the bottom is used to heat up Nb samples to 1100 C for 4 hrs.

OMEGA slope = 0.99

The niobium samples are wrapped in a layer of  Nb foil.

Boat is wrapped with 2 layers of Nb foil.

Good vacuum 3.00e-02 Torr

Bad vacuum 5.00e-02 Torr

Autoramping TGHT at 2A/min to 50A then to 100A, then monitor until desired temperature

Initial IGP1= 9.4e-07 Torr


Friday, June 11, 2021, 09:59

TGHT = 200 A, 2.7V

IGP1=  9.8e-07 Torr

Tap to 1100C


Friday, June 11, 2021, 10:09 

Temperature reached at 10:05 am.

TGHT = 224A, 3.1V

IGP1= 1.0e-06 Torr

OMEGA= 1100C +/- 10C fluctuations


Friday, June 11, 2021, 14:10

TGHT = 224A, 3.1V

IGP1= 9.2e-.07 Torr

OMEGA = 1100C +/-  10C fluctuations

Started rampdown at -3A/min

 

Entry  Wednesday, July 21, 2021, 16:45, Ferran Boix Pamies, Empty, , TARGET BOAT, Done, parasitic target thermal tests v2, foil measurement. 

 2021-07-21 4:44pm Vacumm at 1e-5Torr. Water cooling leak check ok.

 2021-07-21 4:54pm ramping up TGHT to 200A 1A/10s.

2021-07-21 5:31pm 200A TGHT, TC 94degC pyro 1100degC. TC very low, ramping down and venting.

2021-07-22 5:00pm Parasitic prototype target installed, Vacuum 3e-5T, leak check ok. Power on HE of parasitic target.

2021-07-22 5:14pm vacuum 2e-5T. Ramping up container to 100A , 1A/10s.

2021-07-22 5:33pm vacuum 1e-5T. All good at 100A. Ramping up container to 200A , 1A/10s.

2021-07-22 5:54pm vacuum 8.2e-6T. All good at 200A pyro at 1100degC. Ramping up container to 300A , 1A/10s.

2021-07-22 6:15pm vacuum 7.6e-6T. All good at 300A pyro at 1420degC. Ramping up container to 400A , 1A/10s.

2021-07-22 6:36pm vacuum 8e-6T. All good at 400A pyro at 1700degC. Ramping up container to 500A , 1A/10s.

2021-07-22 6:57pm vacuum 1e-5T. All good at 500A pyro at 1960degC. Ramping up container to 553A , 1A/10s.

2021-07-22 7:13pm vacuum 1e-5T. All good at 553A pyro at 2100degC.

2021-07-22 7:36pm Ramping down 1A/10s.

2021-07-23 10:00am Venting.

Entry  Wednesday, October 13, 2021, 08:35, Aaron Schmidt, , , , Problems, Troubleshoot - Pump down issues. 

Swapped out the Cu gaskets for SS gaskets in the HS top lines. (x2)

Wednesday, October 13, 2021, 08:35: Roughing.

Wednesday, October 13, 2021, 08:50: Turbo pump on. TP Current 6.06-6.10A.

Wednesday, October 13, 2021, 08:59: TP maxed out at 3-4 KRPM, yet went "Green/On".

Wednesday, October 13, 2021, 09:00: Change FULL to Low setting. Restart. TP Current 6.15A.

Wednesday, October 13, 2021, 09:08: Timed out. Restarted from 5 KRPM. 

Wednesday, October 13, 2021, 09:14: Stalling @ 5 KRPM. Stop TP. Contact vacuum group.


Monday, October 18, 2021, 09:03: Roughing. Reboot TP controller. 

Monday, October 18, 2021, 09:25: Walkthrough soft start w/ vacuum group. TP timed out. Soft start failed. 

Monday, October 18, 2021, 09:31: EVAP 2 vented. TP to be disconnected & removed.

Monday, October 18, 2021, 09:55: TP removed. Quick check, barely spins when spin by hand gently. Replacement or refurbishment needed. 


500 lpm turbo pumps installed. TV551 Varian. SN: 202311 (Slightly active from BL1A - will not cross contaminate. Field only - Tagged) 

Wednesday, October 20, 2021, 11:35: Roughing. 

Wednesday, October 20, 2021, 11:52: TP on. 

Wednesday, October 20, 2021, 11:59: TP at speed. 

Wednesday, October 20, 2021, 12:02: Vacuum @ 6.13e-05T. Open HS waterline.

Wednesday, October 20, 2021, 12:03: Vacuum @ 5.63e-05T & dropping.

Wednesday, October 20, 2021, 12:04: Vacuum @ 5.32e-05T. TGHT PS on. 

Entry  Thursday, October 21, 2021, 09:58, Darwin Ortiz Rosales, TaC, , TARGET BOAT, Done, Coating of Ta caps and Ta springs (10 caps and 2 springs) 

 

Thursday, October 21, 2021, 10:02

10 TaC coated Ta caps, wrapped in graphite foil.

2 TaC coated Ta springs .

All mounted inside a target boat with enclosed ends.

Good vacuum = 3.0 e-3 Torr

Bad vacuum = 5.0 e-2 Torr

Will heat up to 1800-1900 C and keep at Temp for four hours

OMEGA slope = 0.990

*Note that the turbo pump has been replaced and this is the first EVAP2 operation after replacement*

 


Thursday, October 21, 2021, 10:03

IGP1= 1.6 e-06 Torr

starting ramp up at  2 amp/min to 30 A on TGHT


Thursday, October 21, 2021, 10:46

Ramping to 40 A at 2A/min and will keep there for 20 minutes. 


Thursday, October 21, 2021, 11:19

 IGP1= 1.2e-05 Torr and dropping

Start ramp up to 400 A at 0.5A/min


Thursday, October 21, 2021, 18:58

Started ramping at 3A/min to 468A on TGHT

 


Thursday, October 21, 2021, 20:15

Current at 468.  Will keep there until pressure low enough.


Friday, October 22, 2021, 05:50

IGP1= 8.9 e-06 Torr

Start ramp down at -2A/min


 Monday, October 25, 2021, 11:47

Upon examination the caps and springs did not appeared coated.  The camera was not online so the current used was based on previous elogs.  It may have evaporated TaC due to over temperature.

The materials will be cleaned, recoated and resintered.

Entry  Monday, November 08, 2021, 09:36, Darwin Ortiz Rosales, Endcaps, , TARGET BOAT, Done, Coating of Ta caps and Ta springs (8 caps and 2 springs) 

Monday, November 08, 2021, 09:35

Two groups of 4 caps wrapped in graphite with graphite discs in between. 

Two TaC coated springs at either end of the boat.

Target temperature = 1800 C

Expected around 430 TGHT

Good Vacuum 3e-03 Torr

Bad Vacuum 5e-02 Torr

Evap two was left pressuring down over weekend.


Monday, November 08, 2021, 09:35

Starting autoramp to 40 A at 1A/min

TGHT = 2.5e-07 Torr

 


Monday, November 08, 2021, 10:57

IGP1 = 8.5e -06 Torr and dropping

set autoramp to 50A at 1A/min


IGP1 1.0e-05 Torr and dropping

Set TGHT to autoramp to 90 A @ 1A/min and leave until pressure below 9e-06 Torr


Monday, November 08, 2021, 15:09

IGP1= 9.6e-06 Torr

Start autoramp to 400A at 2A/min 


Monday, November 08, 2021, 17:37

TGHT = 377 A, 6.1V

OMEGA= 1234 C

 


Monday, November 08, 2021, 17:58

OMEGA = 1292 (cannot trust )

400A, 6.3 V

1.4 e-05 Torr

 Autoramp @ 1A/min to 425A

Will heat to 425A and keep there for four hours


Monday, November 08, 2021, 22:02

TGHT=420A, 6.7V

IGP1= 7.0e-06 Torr

Start ramp down at -2A/min 

 

Entry  Thursday, November 25, 2021, 14:00, Aaron Schmidt, , , , , Lower insulator replaced 

 The Helicoil had mostly pulled out of the old one.

Thursday, November 25, 2021, 13:58: Insulator replaced. EVAP 2 is ready for use with ISAC targets.

Entry  Wednesday, February 09, 2022, 08:08, Darwin Ortiz Rosales, Nb, , TARGET BOAT, Done, Nb annealing for Phillip 

Wednesday, February 09, 2022, 06:55 

Target boat with a layer of niobium foil on the bottom used to heat up Nb samples to 1100 C for 4 hrs.

OMEGA slope = 0.99

The niobium samples are wrapped in a layer of  Nb foil.

Boat is wrapped with 2 layers of Nb foil.

Good vacuum 3.00e-02 Torr

Bad vacuum 5.00e-02 Torr

Autoramping TGHT at 3A/min to 180A, then monitor until desired temperature (based on eLog 550)

Initial IGP1=9.9e-07 Torr


Wednesday, February 09, 2022, 08:00

TGHT = 225 A, 3.2V

IGP1=  1.17e-06 Torr

OMEGA= 1100C +/- 12C fluctuations 


Wednesday, February 09, 2022, 11:55

TGHT=  225 A, 3.3 V

IGP1= 9.7e-07 Torr

OMEGA=1100C +/- 10C fluctuations


Wednesday, February 09, 2022, 11:56

Start cooling @-2A/min 

Entry  Thursday, February 10, 2022, 08:58, Darwin Ortiz Rosales, SiC, , HP-FEBIAD, Done,  

Thursday, February 10, 2022, 08:52 

Total number of foils: 528 ( including 10 analysis discs)

Weight without springs = 1521.9 g (includes heatshields and T bar)

Total length packed 18.1 cm (including 10 analysis discs that will be removed)

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Ta coated spring at  ends

Initially to ramp TGHT and TBHT to 50A at0.5 A/min

Then heat automatically heat to OMEGA ~1400 C , then continue to max 530A on TGHT and 230A on TBHT (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -4 Torr

Bad vac at 5.00 e-2 Torr

 IGP1= 1.0 e-06 Torr at start of initial ramp


IGP1 = 5.7 e-06 Torr

TGHT = 50.0 A, 0.6 V

TBHT = 50.0A, 0.5 V

continue to ramp up at 0.5A/min to 200A


Friday, February 11, 2022, 07:59 

IGP1=3.0e-07 Torr and stable

TGHT= 201A, 2.8V

TBHT = 201A, 2.6V

continue autoramp at 1A/min to 230A on TBHT and 450A on TGHT


Friday, February 11, 2022, 12:41

IGP1= 6.6e-05 Torr

TGHT= 450A, 6.5V

TBHT= 232A, 3.1V

OMEGA = 1258C

Allowing pressure to drop.  Will continue ramp up when [pressure around 9-e-6 Torr


Friday, February 11, 2022, 13:59

IGP1= 2.4e-05 Torr

Will ramp up at 1A/min to 550A on TGHT


Friday, February 11, 2022, 15:54  

IGP1= 2.4e-05 Torr

TGHT= 551.0A, 8.3V

TBHT=232A, 3.2V

OMEGA= 1426 C

ramp to 600 A @ 2A/min


Friday, February 11, 2022, 16:23

TGHT= 600.1A, 9.3V

TBHT= 232A, 3.2V

OMEGA = 1612C

ramp to 689 @2A/min to 1800 C as projected in regression plot attached 


Friday, February 11, 2022, 21:20 

Evap has been at 1800 +/- 20 C for 4 hours and 10 minutes

OMEGA 1802 C

TGHT = 689 A, 11.0V

TBHT=232.8 A, 3.26V

IGP1= 1.3e-05 Torr and stabilizing.  

will start cool down at -2A/min TGHT and -1A/min TBHT

 

 

Entry  Tuesday, February 15, 2022, 12:37, Darwin Ortiz Rosales, Nb, , TARGET BOAT, Done, Nb annealing for Phillip 

Wednesday, February 09, 2022, 06:55 

Target boat with a layer of niobium foil on the bottom used to heat up Nb samples to 1400 C for 4 hrs.

OMEGA slope = 0.99

The niobium samples are wrapped in a layer of  Nb foil.

Boat is wrapped with 2 layers of Nb foil.

Good vacuum 3.00e-02 Torr

Bad vacuum 5.00e-02 Torr

Autoramping TGHT at 2A/min to 200A, then monitor until desired temperature

Initial IGP1=6.0e-06 Torr


Tuesday, February 15, 2022, 12:44

Increasing ramp up to 3A/min to 220 A as pressure very stable


Tuesday, February 15, 2022, 14:04

ramped up manually to 1400C

IGP1 =3.9 e-06 Torr

TGHT = 340A, 5.5V

OMEGA = 1400 C


Tuesday, February 15, 2022, 14:21

Temperature on OMEGA up to 1413 C

Lowering current to 332A , OMEGA = 1400 +/- 5C


Wednesday, February 16, 2022, 11:43

On Tuesday February15, 2020 @18:04 started ramp down @-3A/min


 

Entry  Tuesday, April 12, 2022, 13:41, Aaron Schmidt, , , , Maintenance, New Flex - line HS installed 

Old HS sprang a leak in the copper tubing.  

HS#44378-15

Tuesday, April 12, 2022, 13:35: Roughing. 

Tuesday, April 12, 2022, 13:49: TP1 switched on. 

Tuesday, April 12, 2022, 13:57: TP1 stable (green).

Tuesday, April 12, 2022, 14:10: Vacuum @ 3.71e-05T & dropping.

Tuesday, April 12, 2022, 14:11: HS waterline opened. 

Tuesday, April 12, 2022, 14:12: Vacuum @ 3.32e-05T.

Tuesday, April 12, 2022, 14:22: Vacuum @ 2.19e-05T (Stable).

Entry  Tuesday, May 10, 2022, 14:43, Aaron Schmidt, , , , Maintenance, Active TP removed / Swap / Slow start TP 

 Tuesday, May 10, 2022, 14:42: TV551 Varian. SN: 202311 (Slightly active from BL1A - will not cross contaminate. Field only - Tagged) was removed as it was meant to be a temporary fix. Replacement (Refurbished) pump is to be installed. (Tomorrow - Use slow start function as per vacuum group) 


Thursday, May 12, 2022, 13:30: Agilent TP & hardware installed.

SN: IT21381010 

Thursday, May 12, 2022, 13:41: Roughing.

Thursday, May 12, 2022, 13:46: Halt. 


Friday, May 13, 2022, 07:05: Roughing. 

Friday, May 13, 2022, 07:18: TP1 on.

Friday, May 13, 2022, 07:23: Up to 14 KRPM. Pause/Halted startup (Whining?). Slow start w/ vacuum group.

Process to perform a TP slow start:

- Hold both top buttons on the controller for about 3 seconds

- Right Yes/No left to continue. 

- Advance to soft start - 20 min. 

- Back to remote start & go.

Friday, May 13, 2022, 08:26: TP1 on w/ slow start.

Friday, May 13, 2022, 08:39: 13 KRPM & climbing.

Friday, May 13, 2022, 09:10: TP at full speed. 38 KRPM. 0.5A 9w. This pump whines, but is operating fine. Likely will switch again when another is available. (It appears to have been dropped, Noted by Edi. Likely when shipped) 

Friday, May 13, 2022, 09:14: TP off. Slow start function off. Back to normal function. 

Entry  Thursday, June 09, 2022, 09:09, Darwin Ortiz Rosales, Ta, , HP-FEBIAD, Done, Troubleshooting MicrosoftTeams-image_(3).pngMicrosoftTeams-image_(4).pngMicrosoftTeams-image_(5).png

Thursday, June 09, 2022, 09:07

Yesterday, Wednesday June 08, 2022 @ ~3.00 pm a "dummy" target container was installed in EVAP 2 after the heatshield assembly had been swapped.

The purpose is to test correct functioning of the system.  Melting and evaporation on one of the bolts of the previous target container (eLog578) prompted the change in heatshield assembly and current testing.

TGHT was ramped up to 740A @ 4A/min, left to run at the final current for ~4.5 hours and then ramped down @-2A/min to 0A.

Will dismount dummy container this morning.

IGP1=2.5e-07 Torr


Thursday, June 09, 2022, 11:16

The target appears in good shape.  No abnormal behaviour. 

Picture attached are of the previous failed target eLog 578

 

Entry  Monday, June 20, 2022, 14:52, Darwin Ortiz Rosales, Empty, , , Done, softstart of new TP 

Monday, June 20, 2022, 14:50

A new Turbo pump was installed this morning and it was soft started.  It has operated correctly and it is ready for use.  Derek O.  installed it.

Previous pump had issues at start-up and was diagnosed as finished by Edi/

 

Entry  Thursday, August 04, 2022, 09:31, Ferran Boix Pamies, Empty, , TARGET BOAT, In progress, TC on Ta boat test. 

 11am: Setting up new target tube thermocouple test

Thursday, August 04, 2022, 09:31 Test finished August 3rd afternoon. Venting now.  

 

 

ELOG V2.9.2-2455