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Message ID: 566     Entry time: Wednesday, February 09, 2022, 08:08
Author: Darwin Ortiz Rosales 
Target Material: Nb 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: Done 
Subject: Nb annealing for Phillip 

Wednesday, February 09, 2022, 06:55 

Target boat with a layer of niobium foil on the bottom used to heat up Nb samples to 1100 C for 4 hrs.

OMEGA slope = 0.99

The niobium samples are wrapped in a layer of  Nb foil.

Boat is wrapped with 2 layers of Nb foil.

Good vacuum 3.00e-02 Torr

Bad vacuum 5.00e-02 Torr

Autoramping TGHT at 3A/min to 180A, then monitor until desired temperature (based on eLog 550)

Initial IGP1=9.9e-07 Torr


Wednesday, February 09, 2022, 08:00

TGHT = 225 A, 3.2V

IGP1=  1.17e-06 Torr

OMEGA= 1100C +/- 12C fluctuations 


Wednesday, February 09, 2022, 11:55

TGHT=  225 A, 3.3 V

IGP1= 9.7e-07 Torr

OMEGA=1100C +/- 10C fluctuations


Wednesday, February 09, 2022, 11:56

Start cooling @-2A/min 

ELOG V2.9.2-2455