Tuesday, April 18, 2023, 06:48, Darwin Ortiz Rosales, TaC, 45220-11, LP-SIS, Done, TaC coating sintering
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Tuesday, April 18, 2023, 06:46
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1830-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02Torr
Tuesday, April 18, 2023, 06:47
IGP1 initial = 3.80e-07 Torr
Start ramp up at 2A min to 230 on both TBHT and TGHT
Tuesday, April 18, 2023, 09:43
Autoramping TGHT to 380 A @4/min (2/A 30s)
Tuesday, April 18, 2023, 10:36
manually ramped to 416A, 6.8 V on TGHT
TBHT = 230 A, 4.0V
Holding here for 4 hours.
OMEGA = 1863 c
Tuesday, April 18, 2023, 11:26
increased current on TGHT to 418 because temperature had slipped below 1850 C
Tuesday, April 18, 2023, 14:52
ramping down @-2A/min TGHT and -1A/min TBHT |
Saturday, August 26, 2023, 09:41, Darwin Ortiz Rosales, TaC, 45447-12, LP-SIS, Done, TaC coating sintering
|
Saturday, August 26, 2023, 09:39
The coated container was wrapped in 4 Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Initial IGP1= 8.7e-07 Torr
Saturday, August 26, 2023, 10:54

IGP1= 1.2e-06 Torr
Start ramp up at 4A/min on both heaters (2A/30s) until TGHT = 400A and TBHT=230A
Saturday, August 26, 2023, 11:32
Paused ramp to allow temperature to stabilize and record data
OMEGA= 1396 C
IGP1= 2.47e-06 Torr

Saturday, August 26, 2023, 11:52
Paused ramp to record data
OMEGA = 1544 C
IGP1=3.4e-06 Torr

Saturday, August 26, 2023, 12:09
Paused ramp to record data
OMEGA = 1653
IGP1 = 4.5e-06 Torr

Saturday, August 26, 2023, 12:33
Omega went up to 1878C. Lowered the current on TGHT to reach OMEGA = 1857 C
Will keep until 430 pm
IGP1- 3.4e-06 Torr

Saturday, August 26, 2023, 16:10

ramping down at -2A/min tght 1A/min tbht
1837 C OMEGA
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Tuesday, August 29, 2023, 12:47, Darwin Ortiz Rosales, TaC, 45220-10, LP-SIS, Done, TaC coating sintering
|
Tuesday, August 29, 2023, 12:46
The coated container was wrapped in 4 Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Tuesday, August 29, 2023, 12:49
Initial heating start
IGP1= 6.0 e-06 Torr
Tuesday, August 29, 2023, 14:31
Paused ramping to take reading

IGP1= 5.98e-06 Torr
OMEGA = 1500 C
Tuesday, August 29, 2023, 15:24
OMEGA 1866 C
IGP1= 6.6e-6 Torr

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Wednesday, September 20, 2023, 14:26, Aaron Schmidt, Ta, 45220-5, LP-SIS, In progress, Conditioning Ta#66
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Ta#66 LP-SIS target description:
Total Ta foils = 470 [6x20 packs + 350 single discs]
Foil Thickness = 0.033mm (0.0013") avg Measured.
Target material batch: Ta 2023-1 Mt'l PO# TR-2022-03028
Target density = 12.446 g/cm3
Target length = 5.0 cm
Total Mass = 62.230 g [Incl foils + Ta wire on 6 packs]
Total mass w/ Target oven= g (w/ end caps)
Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack
Dimpling direction on foils/ Packs. --> Center <--
End caps installed (Not expanded). No Ta foil heat shield added
Desired temperature 1900C
Wednesday, September 20, 2023, 14:18: Roughing.
Wednesday, September 20, 2023, 14:35: TP Started.
Wednesday, September 20, 2023, 14:43: TP on.
Wednesday, September 20, 2023, 14:45: TGHT / TBHT raised to 5 / 5 A & lowered. Quick check ok.
Thursday, September 21, 2023, 07:47: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Vacuum @ 8.30e-07T.
Thursday, September 21, 2023, 09:54: Slope set to 0.98
Thursday, September 21, 2023, 13:42: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1748 C. Vacuum @ 2.47e-06T.
Thursday, September 21, 2023, 14:10: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1843 C. Vacuum @ 3.30e-06T.
Thursday, September 21, 2023, 14:23: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 660 A @ 2 A per min (648 A w/ offset). Temperature @ 1879 C. Vacuum @ 3.77e-06T.
Thursday, September 21, 2023, 14:29: Tapped TGHT to 662. TGHT / TBHT @ 662 / 230 A (649 / 233 A). Temperature @ 1903 C. Vacuum @ 4.08e-06T. Desired Temperature reached.

Thursday, September 21, 2023, 14:33: Auto-cooling started @ 1 A per min.

Monday, September 25, 2023, 08:09: Turbo pump off. |
Thursday, October 05, 2023, 12:47, Aaron Schmidt, Ta, 45220-3, LP-SIS, In progress, Conditioning Ta#68 (Spare)
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Ta#(Spare) LP-SIS target description:
Total Ta foils = 470 [6x20 packs + 350 single discs]
Foil Thickness = 0.033mm (0.0013") avg Measured.
Target material batch: Ta 2023-1 Mt'l PO# TR-2022-03028
Target density = 12.515 g/cm3
Target length = 4.97 cm
Total Mass = 62.202 g [Incl foils + Ta wire on 6 packs]
Total mass w/ Target oven = 461g (w/ end caps)
Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack
Dimpling direction on foils/ Packs. --> Center <--
End caps installed (Not expanded). No Ta foil heat shield added
Was labelled Ta#67 until the Thin foil target 45447-14 became so.
Thursday, October 05, 2023, 12:44: Roughing.
Thursday, October 05, 2023, 13:10; TP1 on.
Thursday, October 05, 2023, 13:11: TGHT / TBHT test. Tap up to 5 / 5 A & back to 0 A. Ok.
Thursday, October 05, 2023, 13:13: Slope Set @ 0.98
Friday, October 06, 2023, 05:54: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min.
Friday, October 06, 2023, 11:50: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1716 C. Vacuum @ 2.76e-06T.
Friday, October 06, 2023, 12:20: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1809 C. Vacuum @ 3.77e-06T.
Friday, October 06, 2023, 12:37: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 665 A @ 2 A per min (650 A w/ offset). Temperature @ 1844 C.
Friday, October 06, 2023, 12:53: Tapped up to TGHT / TBHT @ 670/ 230 A (657 / 233 A). Temperature @ 1880 C. Vacuum @ 4.94e-06T.
Friday, October 06, 2023, 12:57: Tapped TGHT to 675. TGHT / TBHT @ 675 / 230 A (662 / 233 A). Temperature @ 1889 C. Vacuum @ 5.03e-06T.
Friday, October 06, 2023, 13:00: Tapped TGHT to 682. TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1901 C. Vacuum @ 5.46e-06T. Desired Temperature reached.

Friday, October 06, 2023, 13:01: Auto-cooling @ 2 A per min.
Tuesday, October 10, 2023, 08:37: PS & TP off. |
Friday, October 20, 2023, 07:24, Darwin Ortiz Rosales, TaC, 45447-11, LP-SIS, Done, TaC coating sintering
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Friday, October 20, 2023, 07:20
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial = 9.9 e-07 Torr
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Friday, October 20, 2023, 07:24
Starting initial ramp
Vacuum IGP1 initial = 9.9 e-07 Torr
Friday, October 20, 2023, 08:55
After initial pressure bump continued heating at 1A/min to 120A to observe any other possible pressure bump.
Friday, October 20, 2023, 09:05
increased ramp to 4A/min to 400 TGHT and 230 TBHT
Friday, October 20, 2023, 09:35
OMEGA=1280 C
TGHT= 221.5 A, 3.24V
TBHT=228.9, 3.9V
Friday, October 20, 2023, 10:22
OMEGA 1852 C at TGHT = 390A, 6.5 V ; TBHT = 232 A, 4.0 V
Will leave for 4 hours
Friday, October 20, 2023, 14:16
About to start rampdown
TGHT @ -2A/min
TBHT@ -1A/min
Final OMEGA = 1840 C
IGP1 = 1.83e-06 Torr |
Monday, November 06, 2023, 14:07, Darwin Ortiz Rosales, Empty, 45220-4, LP-SIS, Done, TaC coating sintering
|
Monday, November 06, 2023, 09:59
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =3.1 e-07 Torr
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 2A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Monday, November 06, 2023, 14:07
OMEGA =1852 C
IGP1= 3.14e-06 Torr
TGHT= 399A, 6.6V
TBHT= 233A, 4.1V
Tuesday, November 07, 2023, 12:28
Cooled down previous evening and took out today.
rampdown was @-2A/min for TGHT and -1A/min TBHT |
Monday, July 22, 2024, 14:59, Aaron Schmidt, Ta, 45447-14, LP-SIS, In progress, Conditioning Ta#67 Thin foil
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Ta#67 Thin foil LP-SIS target description:
Total Ta foils = 470 loaded into 2 packs of 235 foils each.
Foil Thickness = 0.010mm (0.0004") avg Measured.
Target material batch: https://elog.triumf.ca/TIS/Target+Production/143
Target density = 4.498 g/cm3
Target length = 3.7465 cm
Total Mass = 16.8509 g [Incl foils + Ta wire on 2 packs]
Total mass w/ Target oven = 415g (No end caps)
Discs in target are arranged as follows: 2packs
Dimpling direction on foils/ Packs. --> Center <--
No Ta foil heat shield added
Monday, July 22, 2024, 14:53: Roughing.
Halt roughing. Install heat plates.
Monday, July 22, 2024, 15:06: Roughing.
Monday, July 22, 2024, 15:26: TP On.
Monday, July 22, 2024, 15:34: TP Timeout. Restart.
Monday, July 22, 2024, 15:35: TP at speed (Green)
Monday, July 22, 2024, 15:36: PS On. TGHT / TBHT to 5/5 A manually. OK. Tap down.
Tuesday, July 23, 2024, 07:03: Auto-ramping TGHT / TBHT to 120 / 60 A @ 2 A per min. Desired temperature 1900 C.
Tuesday, July 23, 2024, 08:02: OMEGA IR2C Laser off. Slope set to 0.98.
Tuesday, July 23, 2024, 08:06: Auto-ramping TGHT / TBHT to 300 / 150 A @ 2 A per min.
Tuesday, July 23, 2024, 09:57: Auto-ramping TGHT / TBHT to 500 / 200 A @ 2 A per min. Temperature @ 1022 C.
Tuesday, July 23, 2024, 11:59: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Temperature @ 1538 C.
Tuesday, July 23, 2024, 12:46: TGHT / TBHT @ 580 / 230 A (569 / 233 A). Temperature @ 1710 C. Vacuum @ 7.44e-06T.
Tuesday, July 23, 2024, 14:23: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 620 A @ 2 A per min. Temperature @ 1721 C. Vacuum @ 5.06e-06T.
Tuesday, July 23, 2024, 14:48: TGHT / TBHT @ 620 / 230 A 609 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min. Temperature @ 1799 C. Vacuum @ 6.76e-06T.
Tuesday, July 23, 2024, 14:56: TGHT / TBHT @ 630 / 230 A 618 / 233 A). Temperature @ 1816 C. Vacuum @ 7.14e-06T. Tapping up manually TGHT to get to 1900degC
Tuesday, July 23, 2024, 15:23: TGHT / TBHT @ 670 / 230 A 657 / 233 A). Temperature @ 1890 C. Vacuum @ 9.94e-06T. Stopping and waiting for 5min.

Tuesday, July 23, 2024, 15:39: Target ramp down 2A/min to 0 both TGHT and TBHT.
Wednesday, July 24, 2024, 08:50: TP off.
Wednesday, July 24, 2024, 09:18: Venting.
Wednesday, July 24, 2024, 10:28: Target removed. EVAP2 clear. |
Saturday, September 07, 2024, 09:55, Darwin Ortiz Rosales, TaC, 45447-13, LP-SIS, Done, TaC coating sintering
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Saturday, September 07, 2024, 09:54
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =8.1 e-07 Torr
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating ramp manually to 50A on TGHT and TBHT
Then at 1A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Saturday, September 07, 2024, 17:38
At 400 A set point on TGHT, read back is 392A and OMEGA reads 1840C. TBHT set to 230A reads 233A.
It will be kept at this current for four hours before rampdown. |
Monday, September 09, 2024, 19:08, Darwin Ortiz Rosales, TaC, , LP-SIS, Done, TaC coating sintering LP-SIS with gas line
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Monday, September 09, 2024, 19:06
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =2.6 e-06 Torr
Target temperature on OMEGA= 1800-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 1A/min on TGHT and TBHT until outgassin peak passed
Then at 1A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Monday, September 09, 2024, 19:08
Peak passed around 70A will continue ramp up at 1A/min to 400A on TGHT and 230A TBHT
Tuesday, September 10, 2024, 13:13
Was ramped down at -2 A/min TGHT and -1 A/min TBHT
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Thursday, March 20, 2025, 06:10, Darwin Ortiz Rosales, Empty, 45447-19, LP-SIS, Done, TaC coating sintering
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Wednesday, March 19, 2025, 13:08
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =
Target temperature on OMEGA= 1800-1850 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Thursday, March 20, 2025, 06:10
IGP1 initial = 6.1e-7 Torr
start ramp at 2A/min
Thursday, March 20, 2025, 07:04
paused ramp to prevent pressure spike
Thursday, March 20, 2025, 10:16
OMEGA 1800 C @ TGHT = 402A, 6.8V
Will leave for 4 hours.
Thursday, March 20, 2025, 13:53
Starting rampdown at 2A/min TGHT and 1A/min TBHT |
Tuesday, March 25, 2025, 15:26, Darwin Ortiz Rosales, Empty, 45447-16, LP-SIS, Done, TaC coating sintering
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Tuesday, March 25, 2025, 15:25
The coated container as wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =e-07 Torr
Target temperature on OMEGA= 1800-1850 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Will be left overnight to pump down
Wednesday, March 26, 2025, 09:07
starting ramp up at 2A/min to 230A for both TGHT and TBHT
Wednesday, March 26, 2025, 12:48
1800 C at 400A TGHT, 6.9V TGHT
Leaving for 4 hours |
Friday, March 28, 2025, 10:34, Darwin Ortiz Rosales, Empty, 45447-20, LP-SIS, Done, TaC coating sintering
|
Friday, March 28, 2025, 06:49
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =8.0e-07 Torr
Target temperature on OMEGA= 1800-1850 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Starting ramp at 2A/min
Friday, March 28, 2025, 09:41
At 412A readback on TGHT OMEGA reads 1702 C. Maybe re-use of Ta heatshields resulted in loss of efficiency. Will ramp to 420 A and leave for 4 hours.
Friday, March 28, 2025, 14:25
Started rampdown at -2A/min TGHT and -1A/min TBHT |
Thursday, September 26, 2013, 15:17, John Wong, Empty, 39814-VI-?, LP-IG-LIS, Done, Sintering empty target oven coated with TaC for UCx#8
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Thursday, September 26, 2013, 13:04
The LP-IG-LIS target container is coated with TaC.
Container is wrapped with 3 layers of Ta heat shield and about to go through the sintering process.
A thermocouple is inserted to measure the temperature inside the tube (1st attempt ever).
Click on the link for detailed pictures:
https://www.dropbox.com/sh/6dc5arajg87mws9/6cU5OxjkZg
TGHT will be ramped up to 580A at 0.2A/min
TBHT will be ramped up to 230A at 0.2A/min.
Chamber has been pumped down. HS cooling H2O valves are opened, and no leaks are detected.
Currently IGP1 @ 5.9e-6 Torr.
Thursday, September 26, 2013, 15:44
TGHT stepped up to 30A. TBHT currently @ 0A.
Temp @ 35C, Vac @ 1.4e-5 Torr.
Monday, September 30, 2013, 14:54
The container was heated up to 580A TGHT/ 230A TBHT for a day (see attachment #1 for vac vs cur plot).
The temperature was measure at ~1780C. (see link for details: https://www.dropbox.com/sh/d8d9j2t60qlm3jk/nkMh7dx_R8 )
The target was cooled down and vented.
Proceed complete.
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Thursday, June 04, 2015, 11:10, Laura Lambert, Empty, , LP-IG-LIS, In progress, Sintering TaC coating container for UCx
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Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
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Friday, June 05, 2015, 12:19, John Wong, Empty, , LP-IG-LIS, In progress, Sintering TaC coating container for UCx
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Laura Lambert wrote: |
Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
|
Friday, June 05, 2015, 12:01
TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down
Cooling down process can be initiated after 4 hours.
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Friday, June 05, 2015, 13:22, Laura Lambert, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx 
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John Wong wrote: |
Laura Lambert wrote: |
Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
|
Friday, June 05, 2015, 12:01
TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down
Cooling down process can be initiated after 4 hours.
|
Friday, June 05, 2015, 13:21
OMEGA = 1995C
Increasing TGHT to 470A to achieve desired max temperature of 2000C
Friday, June 05, 2015, 15:59
TGHT sat at max desired temperature of 2000C for ~4hrs.
TGHT = 470A, 7.7V
Initiating auto-cool at 1.0A/min.
Monday, June 08, 2015, 11:31
Vented in air and opened up this morning.
Target container mostly sintered, two tiny patches near both ends not fully sintered.
Will re-install and re-sinter next week as another container with priority needs to be sintered first.
Tuesday, June 09, 2015, 10:45
See attachements for 'not-fully-sintered' photos
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Wednesday, June 10, 2015, 12:15, John Wong, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx
|
Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
|
Friday, June 05, 2015, 12:01
TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down
Cooling down process can be initiated after 4 hours.
|
Friday, June 05, 2015, 13:21
OMEGA = 1995C
Increasing TGHT to 470A to achieve desired max temperature of 2000C
Friday, June 05, 2015, 15:59
TGHT sat at max desired temperature of 2000C for ~4hrs.
TGHT = 470A, 7.7V
Initiating auto-cool at 1.0A/min.
Monday, June 08, 2015, 11:31
Vented in air and opened up this morning.
Target container mostly sintered, two tiny patches near both ends not fully sintered.
Will re-install and re-sinter next week as another container with priority needs to be sintered first.
Tuesday, June 09, 2015, 10:45
See attachements for 'not-fully-sintered' photos
|
Wednesday, June 10, 2015, 12:06
After inspecting the target container, the inner tube surface has "dark" patches, which may not be evenly coated or the coating layer was too think.
See link for photos: https://www.dropbox.com/sh/m94mjuuodwhz5jb/AADEBv_Kha_p_1An40eftWNHa?dl=0
Attempt to re-spray the container and re-sinter.
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Friday, June 12, 2015, 14:59, Laura Lambert, Empty, 40860-1, LP-IG-LIS, In progress, Sintering TaC coating container for UCx
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John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
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Friday, June 05, 2015, 12:01
TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down
Cooling down process can be initiated after 4 hours.
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Friday, June 05, 2015, 13:21
OMEGA = 1995C
Increasing TGHT to 470A to achieve desired max temperature of 2000C
Friday, June 05, 2015, 15:59
TGHT sat at max desired temperature of 2000C for ~4hrs.
TGHT = 470A, 7.7V
Initiating auto-cool at 1.0A/min.
Monday, June 08, 2015, 11:31
Vented in air and opened up this morning.
Target container mostly sintered, two tiny patches near both ends not fully sintered.
Will re-install and re-sinter next week as another container with priority needs to be sintered first.
Tuesday, June 09, 2015, 10:45
See attachements for 'not-fully-sintered' photos
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Wednesday, June 10, 2015, 12:06
After inspecting the target container, the inner tube surface has "dark" patches, which may not be evenly coated or the coating layer was too think.
See link for photos: https://www.dropbox.com/sh/m94mjuuodwhz5jb/AADEBv_Kha_p_1An40eftWNHa?dl=0
Attempt to re-spray the container and re-sinter.
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Friday, June 12, 2015, 14:58
re-sprayed with second layer of TaC spray this morning.
re-loaded into evap2.
HS water valves opened, no leaks detected.
will ramp-up over weekend. |
Friday, June 12, 2015, 16:08, John Wong, Empty, 40860-1, LP-IG-LIS, In progress, Re-Sintering TaC coating container for UCx
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Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
Thursday, June 04, 2015, 9:07
Container was sprayed with TaC and let dry.
Container has 3x Ta heat shields including center block.
Container was loaded into EVAP2 yesterday and pumped down overnight.
HS water valves were opened up this morning, no leaks detected.
IGP1 = 4.6e-7 Torr.
Tapped up manually to 40A.
Waited ~25min, Vacuum stable.
IGP1 = 5.0e-7 Torr.
Initiating auto-ramp.
TGHT will be ramped to reach 2000C
Friday, June 05, 2015, 10:01
IGP1 = 4.5e-7 Torr.
TGHT = 313A, 4.47V
OMEGA = 1444C
Increasing ramping rate to 1.0A/min
Friday, June 05, 2015, 11:31
IGP1 = 1.2e-6 Torr.
Increasing ramping rate to 2.0A/min
|
Friday, June 05, 2015, 12:01
TGHT reached to 465A/7.56V, temp is stable at 2000C. Current vac at 1.2e-6 Torr and coming down
Cooling down process can be initiated after 4 hours.
|
Friday, June 05, 2015, 13:21
OMEGA = 1995C
Increasing TGHT to 470A to achieve desired max temperature of 2000C
Friday, June 05, 2015, 15:59
TGHT sat at max desired temperature of 2000C for ~4hrs.
TGHT = 470A, 7.7V
Initiating auto-cool at 1.0A/min.
Monday, June 08, 2015, 11:31
Vented in air and opened up this morning.
Target container mostly sintered, two tiny patches near both ends not fully sintered.
Will re-install and re-sinter next week as another container with priority needs to be sintered first.
Tuesday, June 09, 2015, 10:45
See attachements for 'not-fully-sintered' photos
|
Wednesday, June 10, 2015, 12:06
After inspecting the target container, the inner tube surface has "dark" patches, which may not be evenly coated or the coating layer was too think.
See link for photos: https://www.dropbox.com/sh/m94mjuuodwhz5jb/AADEBv_Kha_p_1An40eftWNHa?dl=0
Attempt to re-spray the container and re-sinter.
|
Friday, June 12, 2015, 14:58
re-sprayed with second layer of TaC spray this morning.
re-loaded into evap2.
HS water valves opened, no leaks detected.
will ramp-up over weekend.
|
Friday, June 12, 2015, 16:07
Vacuum comes down to 6.1e-6 Torr.
Initiated auto-ramping at 0.2A/min for 300A first.
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