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Message ID: 676     Entry time: Monday, September 09, 2024, 19:08
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#:  
Source: LP-SIS 
Status: Done 
Subject: TaC coating sintering LP-SIS with gas line 

Monday, September 09, 2024, 19:06

The coated container was wrapped in 4 Ta foil heatshields.

Vacuum IGP1 initial =2.6 e-06 Torr

Target temperature on OMEGA= 1800-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230 A

Final TGHT current= ~400A (adjustable)

Heating autoramp starged at 1A/min on  TGHT   and TBHT until outgassin peak passed

Then at 1A/min  to =400 A TGHT and 230A TBHT

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


Monday, September 09, 2024, 19:08

Peak passed around 70A will continue ramp up at 1A/min to 400A on TGHT and 230A TBHT


Tuesday, September 10, 2024, 13:13

Was ramped down at -2 A/min TGHT and -1 A/min TBHT

 

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