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    Reply  Friday, June 16, 2017, 15:14, Laura Lambert, SiC, 40282-4, TARGET BOAT, Done, Sintering SiC pellets 20170619_111816.jpg20170619_111848.jpg


    
        
            Marla Cervantes wrote:
        
        
            
            
            
Entry  Monday, August 21, 2017, 17:32, John Wong, SiC, , TARGET BOAT, Done, Carbonization of sol-gel SiO2+CNT 
Monday, August 21, 2017, 17:09
Two pellets of sol-gel SiO2+CNT were produced.  See lab book pg 44-46 for details. 
Samples were loaded in Ta boat, wrapped with heat shield (1 layer)
Entry  Monday, June 24, 2019, 08:42, Darwin Ortiz Rosales, SiC, 42464-4, HP-FEBIAD, Done, Conditioning of BSiC discs 

Monday, June 24, 2019, 08:24
Total number of foils: 484
Total mass in  including container = 1495 grams
Entry  Tuesday, October 08, 2019, 14:16, Aaron Schmidt, SiC, , HP-FEBIAD, In progress, Temp measurements. 
Tuesday, October 08, 2019, 14:14: Remove Flex line HS. 
HS: 42752-1
Waterlines not open yet.
Entry  Friday, November 15, 2019, 13:26, Aaron Schmidt, SiC, , HP-FEBIAD, Problems resolved, Temp map testing - 1. (Leak issue) Test_FEBIAD_2019_-_Nov_-_Leak.docxEvap_2_cooling_-_1.jpgTest_FEBIAD_Left_HS_cooling_line_-_1.jpgTest_FEBIAD_Left_HS_cooling_line_-_2.jpg
 HS 42752-5 - Setup for Temperature mapping.
Friday, November 15, 2019, 13:26: Roughing. 
Friday, November 15, 2019, 13:36: Turbo pump on. 
Entry  Thursday, November 21, 2019, 08:10, Aaron Schmidt, SiC, , HP-FEBIAD, In progress, Temperature mapping. 
 Thursday, November 21, 2019, 08:09: PS on. Leak issue resolved (Evap 2 Elog 466). Vacuum @ 4.10e-07T.
Thursday, November 21, 2019, 08:15: Auto-ramping TGHT / TBHT @ 2 A per min to 300 / 150 A. 
Entry  Tuesday, November 26, 2019, 15:21, Darwin Ortiz Rosales, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH) HPFIBIAD20191124-SinteringTaC.PNG
Tuesday, November 26, 2019, 14:53
Total number of foils: 504
Total length packed 17.4 cm
Entry  Tuesday, November 26, 2019, 15:43, Anders Mjos, SiC, 42464-3, HP-FEBIAD, Problems resolved, Water to vacuum leak on heat shield line 
This morning, the vacuum responded to shutting of the water of the heat shield circuit (leak rate without pumping leveling out). The vacuum chamber was
vented and the heat shield with flexible lines was replaced with another heat shield with fixed lines. The chamber was again pumped down and water opened
at ~150 mTorr to test the leak up rate without pumping. No leaks apparent, so continued pumping down with turbo pump. At a vacuum of about 1E-6 Torr the
    Reply  Wednesday, November 27, 2019, 17:45, John Wong, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH) SiC_42464-3_RUSH_400A.JPG


    
        
            Darwin Ortiz Rosales wrote:
        
        
            
            Tuesday, November 26, 2019, 14:53
Entry  Friday, March 13, 2020, 14:21, Darwin Ortiz Rosales, SiC, 42218-8 , HP-SIS, Done, Conditioning of SiC discs (sintering) (RUSH)  
Friday, March 13, 2020, 13:52
Total number of foils: 493
Total length packed 17.4 cm
Entry  Thursday, July 16, 2020, 11:15, Darwin Ortiz Rosales, SiC, 44139-11, LP-SIS, Done, SiC sintering for Luca 1 of 2 
 Thursday, July 16, 2020, 11:15
Coated Ta tube cotaining 233 SiC disks wrapped with Ta heat-shields (3 layers)
Desired temperature= 1800C (expected TGHT 410 A), TBHT will be set fixed at 230A (max).
Entry  Monday, July 20, 2020, 19:25, Darwin Ortiz Rosales, SiC, 44139-11, LP-SIS, Done, SiC sintering for Luca 2 of 2 
Monday, July 20, 2020, 19:27 
Coated Ta tube cotaining 355 SiC disks wrapped with Ta heat-shields (3 layers)
Desired temperature= 1800C (expected TGHT 410 A), TBHT will be set fixed at 230A (max).
Entry  Monday, February 01, 2021, 13:57, Darwin Ortiz Rosales, SiC, 40282-4, TARGET BOAT, Done, Sintering of SiC discs for SEM 
Monday, February 01, 2021, 13:52  
Ta boat loaded with 20 Disc on either end capped with Ta springs to prevent overexpansion. 
 discs wrapped Graphite foil and boat wrapped in Ta heat-shields (3 layers).
Entry  Saturday, February 13, 2021, 08:14, Darwin Ortiz Rosales, SiC, 41992-1, TARGET BOAT, Done, Sintering of SiC discs for SEM  Screenshot_2021-02-14_114713.png
Saturday, February 13, 2021, 08:10
Ta boat loaded with 80 discs enclosed in graphite foil in pockets of 20.  Sample A at both
ends and sample B in the middle spaced out. Boat wrapped in Ta heat-shields (3  layers).
Entry  Wednesday, April 28, 2021, 11:57, Darwin Ortiz Rosales, SiC, 42218-7, HP-SIS, Done, sintering discs for SiC#41 (or back-up for #40) 
Wednesday, April 28, 2021, 11:54
Total number of foils: 449 (not including analysis discs)
Total length packed 16.7 cm
Entry  Thursday, August 05, 2021, 11:18, Darwin Ortiz Rosales, SiC, 44691-2, LP-SIS, Done, Dr blade and non-Dr blade Material Experiment (sintering) image_2021-08-09_221014.png
Thursday, August 05, 2021, 11:10
Total number of foils: 380
Total length packed 13.5 cm
Entry  Thursday, February 10, 2022, 08:58, Darwin Ortiz Rosales, SiC, , HP-FEBIAD, Done,  
Thursday, February 10, 2022, 08:52 
Total number of foils: 528 ( including 10 analysis discs)
Weight without springs = 1521.9 g (includes heatshields and T bar)
Entry  Wednesday, May 18, 2022, 09:59, Darwin Ortiz Rosales, SiC, 44692-9, HP-FEBIAD, Done, T-220516 Sintering SiC 
 Wednesday, May 18, 2022, 09:46
Total number of foils: 415 ( including 10 analysis discs on the right side of the container)
Total weight = 1580 g (includes heatshields and T bar)
Entry  Tuesday, June 07, 2022, 07:31, Darwin Ortiz Rosales, SiC, 42464-2, HP-FEBIAD, Done, T-220524 Sintering SiC 
Tuesday, June 07, 2022, 07:19
Total number of foils: 403 ( including 5 analysis discs on the right side of the container)
Total weight = 1535.3 g (includes heatshields, spring and T bar)
Entry  Tuesday, June 21, 2022, 09:48, Darwin Ortiz Rosales, SiC, 37978-1, HP-FEBIAD, Done, T-220617 sintering 
Tuesday, June 21, 2022, 09:43
Total number of foils: 377 ( including 6 analysis discs on the right side of the container)
Total weight = 1454 g (includes heatshields, spring and T bar)
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