Saturday, February 13, 2021, 08:10
Ta boat loaded with 80 discs enclosed in graphite foil in pockets of 20. Sample A at both ends and sample B in the middle spaced out. Boat wrapped in Ta heat-shields (3 layers).
(A B B A)
Desired temperature= 1800C (expected TGHT approx 410 A).
good vacuum = 3.00 e-05 Torr
bad vacuum = 5.00 e-05 Torr
Evap2 left to pump down over previous night.
IGP1= 5.4e-7 Torr and stable
Initiating TGHT ramp up at 1 A/ min to 30 A
Saturday, February 13, 2021, 12:19
IGP1= 6.9e-06 Torr
Ramp to 50 A 1A/min
Saturday, February 13, 2021, 14:35
IGP1 = 6.4e-6 Torr
Pressure trending down.
Saturday, February 13, 2021, 14:56
IGP1= 4.9 e-6 Torr
Initiate Ramp up @ 1 A/min to 400 A
Changed ramp up to 0.5 A/min at around 11:30 pm
Sunday, February 14, 2021, 11:43
The current will be ramped up to 420 A according to the trendline approximation (see attachement 1)
Sunday, February 14, 2021, 12:26
IGP1 = 8.9 e-06 Torr and trending down
TGHT = 420 A, 7.5 V
OMEGA = 1730 C
Will ramp up to 428 A manually
Sunday, February 14, 2021, 12:30
Reached 428 A on TGHT.
OMEGA = 1760 C
Will bump to 430 A and hold for 4 hours
OMEGA= 1765 C
Sunday, February 14, 2021, 18:00
OMEGA = 1789 C
IGP1= 7.5 e -7 Torr
TGHT = 430.5 A , 7.8 V
Start ramping down at -1A/min to zero A
|