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Entry  Tuesday, November 26, 2019, 15:21, Darwin Ortiz Rosales, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH) HPFIBIAD20191124-SinteringTaC.PNG
    Reply  Wednesday, November 27, 2019, 17:45, John Wong, SiC, 42464-3, HP-FEBIAD, Done, Conditioning of SiC discs (sintering) (RUSH) SiC_42464-3_RUSH_400A.JPG
Message ID: 471     Entry time: Tuesday, November 26, 2019, 15:21     Reply to this: 473
Author: Darwin Ortiz Rosales 
Target Material: SiC 
Target Oven W.O#: 42464-3 
Source: HP-FEBIAD 
Status: Done 
Subject: Conditioning of SiC discs (sintering) (RUSH) 

Tuesday, November 26, 2019, 14:53

Total number of foils: 504

Total length packed 17.4 cm

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Two TaC coated Ta wire springs inserted at either end.

Initially to ramp TGHT and TBHT to 50A at 1A/min

Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically  to reach 530A A (Omega slope set = 0.990)

Then temperature= (Correected to 1800C) 1900 C, Omega Slope set = 0.990, manually and automatically ramp to 700A, TGHT will be tapped up accordingly to reach desired Temp.

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -5 Torr

Bad vac at 5.00 e-5 Torr

System experienced some vacuum issues due to cooling water leak in a heatshield line. 

Evaluation discs not included because no space.

Total Green disc mass measured = 58.250 g

 


Tuesday, November 26, 2019, 15:00

IGP1= 7.4e-06 Torr.  No leak issues found after last fix (Anders will add details).


Tuesday, November 26, 2019, 15:33

TGHT= 52.7A, .22V   TBHT= 49.3A, .52V

IGP1= 7.202 e-06 Torr (trending up so will allow to stabilize).


Wednesday, November 27, 2019, 06:09

left with autoramp waiting for vac to drop but no advance overnight.

Pressure did not seem to drop back below 3e-5 Torr magnitude, therefore not much advance in current ramp.


Thursday, November 28, 2019, 11:15

Continued ramping manually 

OMEGA = 1429 C  (0.99 slope), TGHT = 542A, 7.8V

With slope = 1.08 OMEGA = 1724 C, therefore staying at 0.99 slope

TaC coating sintering  plot suggests 753A to reach 1800C (See attachment 1)

Windows a little bit coated but not enough to disturb laser. 


Thursday, November 28, 2019, 12:17

TGHT =753A, 11.8V since 12:00 noon. 

TBHT= 233.4A, 3.3V

OMEGA= 1735 C (0.99 slope)


 Thursday, November 28, 2019, 13:01

OMEGA = 1860C (1.08 slope)


 Thursday, November 28, 2019, 14:38

OMEGA temperature began to creep up to ~1880.  Tapped TGHT current down to 733.5A, 11.4V


Thursday, November 28, 2019, 15:12

Checked windows and no significant additional buildup of obstructive material.

Temperature creeping up again.  Tap down TGHT current to 729 A, 11.2 V

OMEGA = 1870C at slope 1.08


 Thursday, November 28, 2019, 16:03

Temperature increase to 1880C

Tap down TGHT current to 715A, 10.9V

OMEGA= 1870 C (slope = 1.08)


Thursday, November 28, 2019, 16:22

Temperature creep to 1880 C

Tap down TGHT to 700A, 10.8V

OMEGA= 1845C

IGP1=2.2e-06 Torr


Thursday, November 28, 2019, 16:37

IGP1= 1.9e-06 Torr

OMEGA = 1850C (1.08 slope)

TGHT = 692A, 10.5V  TBHT= 233A, 3.2V

 

Initiating pressure ramp at -2A/min on TGHT and -1A/min on TBHT


Thursday, November 28, 2019, 16:45

IGP1= 1.28e-06 Torr

OMEGA= 1770 C (1.08 slope)

TGHT = 650A, 9.8V

ramp TGHT at -3.5A/min maintain TBHT at -1A/m in


 Thursday, November 28, 2019, 17:11

IGP1= 1.14e-06 Torr

OMEGA = 1730 C (1.08 slope)

ramp TGHT at -5A/min maintain TBHT at -1A/m


Thursday, November 28, 2019, 17:20

IGP1- 8.9e-07 Torr

OMEGA=1636C

ramp TGHT at -6A/min maintain TBHT at -1A/min


 Thursday, November 28, 2019, 17:34

IGP1= 7e-07 Torr

OMEGA= 1500 C (1.08 slope)

ramp TGHT at -8A/min maintain TBHT at -1A/min

TBHT = 183A


 OMEGA 1180C

TGHT =300 A

TBHT = 155A

Initiated -15A/min TGHT and -4A/min TBHT

IGP1= 5.2e-07 Torr


OMEGA below 1000C

begin manual tapdown


Thursday, November 28, 2019, 19:42

Target was dismounted after cooling.  Two graphite discs and end caps inserted.

 

Attachment 1: HPFIBIAD20191124-SinteringTaC.PNG  9 kB  Uploaded Thursday, November 28, 2019, 12:14  | Show | Hide all
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