ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
648
|
Friday, October 20, 2023, 07:24 |
Darwin Ortiz Rosales | TaC | 45447-11 | LP-SIS | Done | TaC coating sintering | Friday, October 20, 2023, 07:20
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial = 9.9 e-07 Torr
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Friday, October 20, 2023, 07:24
Starting initial ramp
Vacuum IGP1 initial = 9.9 e-07 Torr
Friday, October 20, 2023, 08:55
After initial pressure bump continued heating at 1A/min to 120A to observe any other possible pressure bump.
Friday, October 20, 2023, 09:05
increased ramp to 4A/min to 400 TGHT and 230 TBHT
Friday, October 20, 2023, 09:35
OMEGA=1280 C
TGHT= 221.5 A, 3.24V
TBHT=228.9, 3.9V
Friday, October 20, 2023, 10:22
OMEGA 1852 C at TGHT = 390A, 6.5 V ; TBHT = 232 A, 4.0 V
Will leave for 4 hours
Friday, October 20, 2023, 14:16
About to start rampdown
TGHT @ -2A/min
TBHT@ -1A/min
Final OMEGA = 1840 C
IGP1 = 1.83e-06 Torr |
619
|
Tuesday, April 04, 2023, 12:50 |
Darwin Ortiz Rosales | TaC | 45447-1 | HP-FEBIAD | Done | TaC coating sintering | Tuesday, April 04, 2023, 12:48
Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers + 1 inner layer around fins including center fins)
Desired temperature = 1850 C , TBHT will be set fixed at 230A (max).
Evap 2 will be pumped down over previous night
OMEGA slope= 0.990
Good vacuum = 5.00 e-4 Torr
Bad vacuum = 5.00 e-2 Torr
OMEGA target temp = 1850 C
Wednesday, April 05, 2023, 07:37
IGP1= 4.3e-07 Torr
starting autoramp @ 1A/min to 230A on both TGHT and TBHT
Wednesday, April 05, 2023, 10:56
Starting Autoramp at 4A/min to 400 A on TGHT
Wednesday, April 05, 2023, 14:14
OMEGA Reached 1877C @ 743A, 11.3V TGHT
rampdown @ 6:00 pm
Wednesday, April 05, 2023, 14:38
Decreased TGHT current to 736A because temperature was creeping up
rampdown was started at 6:05 pm
Final pressure at 0 V - 1.7e-07 Torr
|
652
|
Friday, January 26, 2024, 07:06 |
Darwin Ortiz Rosales | TaC | 45447-1 | HP-FEBIAD | Done | TaC coating sintering | Friday, January 26, 2024, 07:05
The coated container was wrapped in 4 Ta foil heatshield and left in evap2 over night to attain vacuum.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~700A (adjustable)
Heating autoramp starged at 1A/min on TGHT and TBHT to 120A
Then at 2 A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Initial IGP1= 5.7e-05 Torr
Friday, January 26, 2024, 09:20
Pressure starts increasing at 125 A on TGHT and TBHT. Leaving it to equilibrate then will start ramping at 3A/min (1.5A/30s) to 700A on TGHT and 230A on TBHT
Friday, January 26, 2024, 13:18
leave sintering at 1838C . Will start rampdown at 5 pm.
IGP1= 6.10e-06 Torr
TGHT=680A, 10.14V
TBHT = 230A, 3.13V
Friday, January 26, 2024, 16:52
IGP1 = 3.0e10-6 Torr
OMEGA=1821 C
start rampdown @-2A/min TGHT and -1A/min TBHT |
609
|
Thursday, February 23, 2023, 18:24 |
Darwin Ortiz Rosales | TaC | 45441-2 | HP-FEBIAD | Done | TaC coating sintering | Thursday, February 23, 2023, 18:20
Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3 layers) and 1 under layer that doesn't cover the middle section.
Desired temperature = 1800 C , TBHT will be set fixed at 230A (max).
Evap 2 will be pumped down to 5e-06 Torr range
OMEGA slope= 0.990
Good vacuum = 5.00 e-4 Torr
Bad vacuum = 5.00 e-2 Torr
IGP1=2.5 e-06 Torr
Start autoramp @1A/min to 80 A then autoramp heat @1A/min to 150 A. Then autoramp TGHT to approx 675A and TBHT to 230A.1
Friday, February 24, 2023, 09:10
heated overnight @0.5 A/min to 400 A. Then started heating at 1A/min to 600 A while taking readings for current/Temp regression.
regression so far points to 682A to get to 1800C. Will continue taking readings and possible heat to 1850 C.
Friday, February 24, 2023, 09:43
autoramping to 690A at 1A/min
Friday, February 24, 2023, 11:24
ramping manually to 690A from 650A
Friday, February 24, 2023, 11:32
4 hours at 330pm
TGHT 492A, 10.6V
TBHT = 230A, 3.2V
IGP1=5.11e-06 Torr
OMEGA =1840 C
Friday, February 24, 2023, 15:36
TGHT = 692A, 10.6V
TBHT = 230 A, 3.2V
OMEGA = 1835 C
IGP1= 2.4e-06 Torr
Starting rampdown at -2A/min TGHT and -1A/min TBHT |
617
|
Thursday, March 16, 2023, 14:47 |
Darwin Ortiz Rosales | TaC | 45220-9 | LP-SIS | Done | TaC coating sintering | Thursday, March 16, 2023, 13:38
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1860-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-02 Torr
Bad vacuum = 5.0E-04 Torr
Thursday, March 16, 2023, 22:21
Started ramping TGHT and TBHT @ 1.5A/min to 387 A and 230A respectively.
IGP1 initial = 9.6 e-07 Torr
Cooling projected at 6:48 am tomorrow.
Friday, March 17, 2023, 06:59
Final IGP1= 1.6e-o6 Torr
Started rampdown @-2A/min TGHT and -1A/min TBHT
Coating looks good uniformely.
OMEGA 1850 C (was 1868 initially)
TGHT was 387A, 6.6 V and TBHT was 230A, 4.1 V
Coating very nice |
618
|
Thursday, March 30, 2023, 12:45 |
Aaron Schmidt | Ta | 45220-7 | LP-SIS | In progress | Conditioning Ta#65 | Thursday, March 30, 2023, 12:27:
Ta#65 LP-SIS target description:
Total Ta foils = 470 [6x20 packs + 350 single discs]
Foil Thickness = 0.033mm (0.0013") avg Measured.
Target material batch: Ta 2023-1 Mt'l PO# TR-2022-03028
Target density = 18.2685 g/cm3
Target length = 3.40 cm
Total Mass = 62.113 g [Incl foils + Ta wire on 6 packs]
Total mass w/ Target oven= 460.8 g (w/ end caps)
Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack
Dimpling direction on foils/ Packs. --> Center <--
End caps installed (Not expanded). No Ta foil heat shield added
Tuesday, May 16, 2023, 10:44: End cap removed post conditioning to remove the rhenium foil. End cap replaced, & weight updated. Length remains the same.
Final desired temperature = 1900C.
Thursday, March 30, 2023, 12:41: RP on.
Thursday, March 30, 2023, 12:42: Roughing
Thursday, March 30, 2023, 12:44: OMEGA slope = 0.98.
Thursday, March 30, 2023, 12:59: TP1 on.
Thursday, March 30, 2023, 13:00: TP1 off.
Thursday, March 30, 2023, 13:03: Venting. (Steel pair of shields req'd - Install)
Thursday, March 30, 2023, 13:05: Roughing.
Thursday, March 30, 2023, 13:20: TP1 on.
Thursday, March 30, 2023, 13:29: TP1 trip @ 38 krpm. Quick Reset. Fully "green". OK.
Thursday, March 30, 2023, 13:31: Vacuum @ 5.84e-05T. TGHT / TBHT PS on.
Thursday, March 30, 2023, 13:32: Operation Check. TGHT / TBHT tapped up to 5 / 5 A. Ok. Back to 0A.
Friday, March 31, 2023, 06:32: Auto-ramping TGHT / TBHT to 500 / 200 A @ 2 A per minute. Vacuum @ 6.52e-07T.
Friday, March 31, 2023, 12:08: TGHT / TBHT @ 500 / 200 A. Vacuum @ 2.24e-06T. Temperature @ 1575 C. Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min
Friday, March 31, 2023, 13:05: TGHT / TBHT @ 580 / 230 A. Vacuum @ 3.69e-06T. Temperature @ 1748 C. Auto-ramping TGHT to 600 @ 2 A per min
Friday, March 31, 2023, 13:27: TGHT / TBHT @ 600 / 230 A. Vacuum @ 3.83e-06T. Temperature @ 1790 C. Auto-ramping TGHT to 620 @ 2 A per min
Friday, March 31, 2023, 13:42: TGHT / TBHT @ 620 / 230 A. Vacuum @ 4.34e-06T. Temperature @ 1820 C. Auto-ramping TGHT to 640 @ 2 A per min
Friday, March 31, 2023, 13:51: TGHT / TBHT @ 640 / 230 A. Vacuum @ 5.51e-06T. Temperature @ 1858 C. Tap up TGHT to 650 A
Friday, March 31, 2023, 13:54: Vacuum @ 6.03e-06T. Temp @ 1902 C. Tapped up TGHT to 660 manually. Desired temperature reached.
Friday, March 31, 2023, 13:57: Auto-cooling @ 2 A per minute.
Friday, March 31, 2023, 17:31:
Monday, April 03, 2023, 07:35: PS off. TP off. |
598
|
Friday, October 28, 2022, 07:59 |
Darwin Ortiz Rosales | TaC | 45220-6 | LP-SIS | Done | TaC coating sintering | Friday, October 28, 2022, 07:58
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~420A (adjustable)
Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A
Then at 1A/min on both heaters to 120A.
Good vacuum = 5.0 e-02 Torr
Bad vacuum = 5.0E-04 Torr
IGP1 initial = 4.5e-07 Torr
Friday, October 28, 2022, 10:50
after reaching 120A and leaving until pressure drop, autoramp at 2.5A/30s (5A/min) towards 400A TGHT and 230A TBHT.
Friday, October 28, 2022, 11:22
OMEGA= 1890 @ 412A, 7.1 V on TGHT
Leaving for 4 hours
|
646
|
Wednesday, September 20, 2023, 14:26 |
Aaron Schmidt | Ta | 45220-5 | LP-SIS | In progress | Conditioning Ta#66 | Ta#66 LP-SIS target description:
Total Ta foils = 470 [6x20 packs + 350 single discs]
Foil Thickness = 0.033mm (0.0013") avg Measured.
Target material batch: Ta 2023-1 Mt'l PO# TR-2022-03028
Target density = 12.446 g/cm3
Target length = 5.0 cm
Total Mass = 62.230 g [Incl foils + Ta wire on 6 packs]
Total mass w/ Target oven= g (w/ end caps)
Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack
Dimpling direction on foils/ Packs. --> Center <--
End caps installed (Not expanded). No Ta foil heat shield added
Desired temperature 1900C
Wednesday, September 20, 2023, 14:18: Roughing.
Wednesday, September 20, 2023, 14:35: TP Started.
Wednesday, September 20, 2023, 14:43: TP on.
Wednesday, September 20, 2023, 14:45: TGHT / TBHT raised to 5 / 5 A & lowered. Quick check ok.
Thursday, September 21, 2023, 07:47: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min. Vacuum @ 8.30e-07T.
Thursday, September 21, 2023, 09:54: Slope set to 0.98
Thursday, September 21, 2023, 13:42: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1748 C. Vacuum @ 2.47e-06T.
Thursday, September 21, 2023, 14:10: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1843 C. Vacuum @ 3.30e-06T.
Thursday, September 21, 2023, 14:23: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 660 A @ 2 A per min (648 A w/ offset). Temperature @ 1879 C. Vacuum @ 3.77e-06T.
Thursday, September 21, 2023, 14:29: Tapped TGHT to 662. TGHT / TBHT @ 662 / 230 A (649 / 233 A). Temperature @ 1903 C. Vacuum @ 4.08e-06T. Desired Temperature reached.
Thursday, September 21, 2023, 14:33: Auto-cooling started @ 1 A per min.
Monday, September 25, 2023, 08:09: Turbo pump off. |
649
|
Monday, November 06, 2023, 14:07 |
Darwin Ortiz Rosales | Empty | 45220-4 | LP-SIS | Done | TaC coating sintering | Monday, November 06, 2023, 09:59
The coated container was wrapped in 4 Ta foil heatshields.
Vacuum IGP1 initial =3.1 e-07 Torr
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 2A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Monday, November 06, 2023, 14:07
OMEGA =1852 C
IGP1= 3.14e-06 Torr
TGHT= 399A, 6.6V
TBHT= 233A, 4.1V
Tuesday, November 07, 2023, 12:28
Cooled down previous evening and took out today.
rampdown was @-2A/min for TGHT and -1A/min TBHT |
647
|
Thursday, October 05, 2023, 12:47 |
Aaron Schmidt | Ta | 45220-3 | LP-SIS | In progress | Conditioning Ta#68 (Spare) | Ta#(Spare) LP-SIS target description:
Total Ta foils = 470 [6x20 packs + 350 single discs]
Foil Thickness = 0.033mm (0.0013") avg Measured.
Target material batch: Ta 2023-1 Mt'l PO# TR-2022-03028
Target density = 12.515 g/cm3
Target length = 4.97 cm
Total Mass = 62.202 g [Incl foils + Ta wire on 6 packs]
Total mass w/ Target oven = 461g (w/ end caps)
Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack
Dimpling direction on foils/ Packs. --> Center <--
End caps installed (Not expanded). No Ta foil heat shield added
Was labelled Ta#67 until the Thin foil target 45447-14 became so.
Thursday, October 05, 2023, 12:44: Roughing.
Thursday, October 05, 2023, 13:10; TP1 on.
Thursday, October 05, 2023, 13:11: TGHT / TBHT test. Tap up to 5 / 5 A & back to 0 A. Ok.
Thursday, October 05, 2023, 13:13: Slope Set @ 0.98
Friday, October 06, 2023, 05:54: Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min.
Friday, October 06, 2023, 11:50: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (640 A w/ offset). Temperature @ 1716 C. Vacuum @ 2.76e-06T.
Friday, October 06, 2023, 12:20: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1809 C. Vacuum @ 3.77e-06T.
Friday, October 06, 2023, 12:37: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 665 A @ 2 A per min (650 A w/ offset). Temperature @ 1844 C.
Friday, October 06, 2023, 12:53: Tapped up to TGHT / TBHT @ 670/ 230 A (657 / 233 A). Temperature @ 1880 C. Vacuum @ 4.94e-06T.
Friday, October 06, 2023, 12:57: Tapped TGHT to 675. TGHT / TBHT @ 675 / 230 A (662 / 233 A). Temperature @ 1889 C. Vacuum @ 5.03e-06T.
Friday, October 06, 2023, 13:00: Tapped TGHT to 682. TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1901 C. Vacuum @ 5.46e-06T. Desired Temperature reached.
Friday, October 06, 2023, 13:01: Auto-cooling @ 2 A per min.
Tuesday, October 10, 2023, 08:37: PS & TP off. |
594
|
Monday, October 17, 2022, 11:32 |
Darwin Ortiz Rosales | TaC | 45220-2 | LP-SIS | Done | TaC coating sintering | Monday, October 17, 2022, 10:03
The coated container was wrapped in 4 Ta foil heatshields. (The 4 shields appear to work well)
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~420A (adjustable)
Heating autoramp started at 2A/min on both TGHT and TBHT to40A
Then at 1A/min on both heaters to 120A.
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Monday, October 17, 2022, 12:45
Autoramping @4A/min on both TGHT and TBHT to 400 and 30A respectively
Monday, October 17, 2022, 12:56
slowed ramp to 2A/min on both heaters as pressure was increasing too fast. (1A/30s).
Monday, October 17, 2022, 13:30
increased ramp rate to 4A/min on TGHT as TBHT is already at 230A
Monday, October 17, 2022, 14:16
leaving at TGHT : 393A, 6.5V ; TBHT 233A, 4.2V
OMEGA reads 1864C. Will start rampdown at 6:17 pm
Monday, October 17, 2022, 18:16
OMEGA read 1875C at max and now reads 1856C
starting ramp down at -2A/min TGHT and -1A/min TBHT
Final IGP1= 1.4e-06 Torr
Tuesday, October 18, 2022, 09:37
IGP1= 2.72e-7 Torr
Turning heaters off on epics and turning vacuums off. |
621
|
Sunday, April 16, 2023, 14:08 |
Darwin Ortiz Rosales | TaC | 45220-14 | LP-SIS | Done | TaC coating sintering | Sunday, April 16, 2023, 14:08
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1860-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Ramped at 2A/min to 230 A on both TGHT and TBHT.
Then ramped @4A/min to 385 A on TGHT. Then ramped manually to 1850 C
Sunday, April 16, 2023, 18:31
At 428A reached 1830C on OMEGA
Sunday, April 16, 2023, 22:24
Start ramp down @ -2A/min TGHT and -1A/min TBHT |
601
|
Thursday, November 10, 2022, 07:40 |
Darwin Ortiz Rosales | TaC | 45220-13 | LP-SIS | Done | TaC coating sintering | Thursday, November 10, 2022, 07:40
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A
Then at 1A/min on both heaters to 120A.
Good vacuum = 5.0 e-02 Torr
Bad vacuum = 5.0E-04 Torr
IGP1 initial = 2.8e-07 Torr
Thursday, November 10, 2022, 10:31
TGHT 230A 3.4V and TBHT at 230A , 3.9V
Continue ramp up for TGHT at 4A/min (2A/30s) to 380A
Thursday, November 10, 2022, 11:30
OMEGA =1886 C @ 430A, 7.1V TGHT; will leave for 4 hours
Thursday, November 10, 2022, 15:43
rampdown at -2A/min TGHT and -1A/min TBHT |
604
|
Tuesday, November 22, 2022, 14:59 |
Darwin Ortiz Rosales | TaC | 45220-12 | LP-SIS | Done | TaC coating sintering | Tuesday, November 22, 2022, 14:58
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1860-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A
Then at 2A/min on both heaters to 120A.
Good vacuum = 5.0 e-02 Torr
Bad vacuum = 5.0E-04 Torr
leaving to pressure down.
Wednesday, November 22, 2022, 19:10
OMEGA = 1942 C @ 396A on TGHT
lowered to 386A to 1900 and left for 4 hours.
After four hours, started rampdown at-2A/min TGHT and -1A/min TBHT
|
606
|
Friday, December 02, 2022, 09:50 |
Darwin Ortiz Rosales | | 45220-12 | TARGET BOAT | Done | Grahite disc conditioning 221130-Graphite | Friday, December 02, 2022, 09:46
297 graphite discs packed into a Ta tube wrapped in four heatshields.
Good vacuum 5.0e-04 Torr
Bad vacuum 5.0 e-02 Torr
Will be conditioned @ 2000 C for 5 hours and then for one hour at 10A greater than final current. Final current will be calculated from
regression.
IGP1= 5.7 e-07 Torr
ramping to 40A @ 2A/min TGHT
Friday, December 02, 2022, 20:59
Was ramped to 320A but the window must be coated because Temperature readings are drastically off. Will cool down and repeat on Monday after cleaning window. Will ramp down at -2A/min
OMEGA= 1360 C, expect much higher.
Tuesday, December 06, 2022, 10:58
ramp started at 4A/min . Initial pressure was 2.6 e-07 Torr
Tuesday, December 06, 2022, 12:45
OMEGA readings low (1290 @ 331A, 5.6V )
Will tap up until pressure bump observed.
Tuesday, December 06, 2022, 13:04
Pressure bump observed around 440 A, 7.9 V
IGP1= 8.4 e-06 Torr.
Current stopped and will keep at this current for 10 hours (11 pm rampdown)
Tuesday, December 06, 2022, 13:24
Ramped to 500A, Will leave at 500A for the rest of the conditioning.
Tuesday, December 06, 2022, 23:05
Starting rampdown at -2A/min
IGP1= 4.9e-07 Torr
TGHT= 500A, 9.3V
Wednesday, December 07, 2022, 09:43
Dismounting today.
IGP1 final = 9.6e-08 Torr
Wednesday, December 07, 2022, 13:29
Reinstalled in the evaporator. Window was not shaded. Will try heating to 500A once more.
ramp at 6A/min |
622
|
Tuesday, April 18, 2023, 06:48 |
Darwin Ortiz Rosales | TaC | 45220-11 | LP-SIS | Done | TaC coating sintering | Tuesday, April 18, 2023, 06:46
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1830-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02Torr
Tuesday, April 18, 2023, 06:47
IGP1 initial = 3.80e-07 Torr
Start ramp up at 2A min to 230 on both TBHT and TGHT
Tuesday, April 18, 2023, 09:43
Autoramping TGHT to 380 A @4/min (2/A 30s)
Tuesday, April 18, 2023, 10:36
manually ramped to 416A, 6.8 V on TGHT
TBHT = 230 A, 4.0V
Holding here for 4 hours.
OMEGA = 1863 c
Tuesday, April 18, 2023, 11:26
increased current on TGHT to 418 because temperature had slipped below 1850 C
Tuesday, April 18, 2023, 14:52
ramping down @-2A/min TGHT and -1A/min TBHT |
642
|
Saturday, August 26, 2023, 09:41 |
Darwin Ortiz Rosales | TaC | 45220-10 | LP-SIS | Done | TaC coating sintering |
Saturday, August 26, 2023, 09:39
The coated container was wrapped in 4 Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Initial IGP1= 8.7e-07 Torr
Saturday, August 26, 2023, 10:54
IGP1= 1.2e-06 Torr
Start ramp up at 4A/min on both heaters (2A/30s) until TGHT = 400A and TBHT=230A
Saturday, August 26, 2023, 11:32
Paused ramp to allow temperature to stabilize and record data
OMEGA= 1396 C
IGP1= 2.47e-06 Torr
Saturday, August 26, 2023, 11:52
Paused ramp to record data
OMEGA = 1544 C
IGP1=3.4e-06 Torr
Saturday, August 26, 2023, 12:09
Paused ramp to record data
OMEGA = 1653
IGP1 = 4.5e-06 Torr
Saturday, August 26, 2023, 12:33
Omega went up to 1878C. Lowered the current on TGHT to reach OMEGA = 1857 C
Will keep until 430 pm
IGP1- 3.4e-06 Torr
Saturday, August 26, 2023, 16:10
ramping down at -2A/min tght 1A/min tbht
1837 C OMEGA
|
643
|
Tuesday, August 29, 2023, 12:47 |
Darwin Ortiz Rosales | TaC | 45220-10 | LP-SIS | Done | TaC coating sintering | Tuesday, August 29, 2023, 12:46
The coated container was wrapped in 4 Ta foil heatshields.
Target temperature on OMEGA= 1850-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230 A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 2A/min(1A/30s) on TGHT 100A
Then at 4A/min to =400 A TGHT and 230A TBHT
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Tuesday, August 29, 2023, 12:49
Initial heating start
IGP1= 6.0 e-06 Torr
Tuesday, August 29, 2023, 14:31
Paused ramping to take reading
IGP1= 5.98e-06 Torr
OMEGA = 1500 C
Tuesday, August 29, 2023, 15:24
OMEGA 1866 C
IGP1= 6.6e-6 Torr
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603
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Friday, November 18, 2022, 15:13 |
Darwin Ortiz Rosales | TaC | 45220-1 | LP-SIS | Done | TaC coating sintering | Friday, November 18, 2022, 15:08
The coated container was wrapped in four Ta foil heatshields.
Target temperature on OMEGA= 1860-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Heating autoramp starged at 4A/min on both TGHT and TBHT to 40A
Then at 2A/min on both heaters to 120A.
Good vacuum = 5.0 e-02 Torr
Bad vacuum = 5.0E-04 Torr
leaving to pressure down over weekend
Sunday, November 20, 2022, 12:11
start heatup IGP1=1.63e-07 Torr
Sunday, November 20, 2022, 14:21
OMEGA= 1900 at 395A, 6.6V on TGHT
Will leave until 6;20 pm |
570
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Wednesday, March 23, 2022, 10:52 |
Darwin Ortiz Rosales | TaC | 44692-9 | HP-FEBIAD | Done | TaC coating | Wednesday, March 23, 2022, 10:49
Ta HP-FEBIAD was coated with TaC and wrapped with Ta heat-shields (3.5 layers) (two pieces around the fins only and 3 layers around the whole )
Desired temperature = 1800 C , TBHT will be set fixed at 230A (max). TGHT expected to reach desired Temperature @~700A
Evap 2 was pumped down over previous night
Good vacuum = 3.00 e-4 Torr
Bad vacuum = 5.00 e-2 Torr
IGP1= 1.2 e-06 Torr
Start autoramp @0.5 A/min to 60 A
Wednesday, March 23, 2022, 11:37
Increase autoramp to 1A/min to 60A for both TGHT and TBHT
Wednesday, March 23, 2022, 12:24
Pressure increasing at 60A so will leave at this current until pressure drops
Wednesday, March 23, 2022, 13:32
IGP1 = 2.9e-06 Torr
Will autoramp at 0.5A/min to 90A both TGHT and TBHT
Thursday, March 24, 2022, 16:35
1800C reached at 724A TGHT . TBHT @ 230A. Will keep at this temperature for 4 hours.
Thursday, March 24, 2022, 20:20
IGP1 = 6.9 e-06 Torr
OMEGA= 1828 C
TGHT = 724 A, 11.6 V
TBHT = 232.8 A, 3.1 V
Will start ramp-down at 2035 @ -2A/min TGHT and -1A/min TBHT
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