Tuesday, January 31, 2017, 13:43

Container coated with TaC using new method: Ends taped off,  with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'

Container is wrapped with 3 x Ta heat shields, not incl center block.

Loaded into EVAP2 and currently pumping down.

Tuesday, January 31, 2017, 16:02 

IGP1 = 3.9e-6 Torr.

HS water valves opened.

No leaks detected.

Tapped up manually to 35A.

Vacuum stable.

Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Final setpoints for TGHT = 450A and TBHT = 230A, with final desired temp of 1900C

OMEGA slope = 0.98

 Wednesday, February 01, 2017, 10:01

IGP1 = 5.7e-7 Torr.

TGHT = 254A, 3.0V

TBHT = 142A, 1.8V

Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

 Wednesday, February 01, 2017, 11:48

IGP1 = 1.7e-6 Torr.

TGHT = 450A, 6.27V

TBHT = 230A, 3.14V

OMEGA = 1176C

Increasing max setpoint of TGHT = 600A

 Wednesday, February 01, 2017, 13:09

IGP1 = 3.7e-6 Torr.

TGHT = 600A, 9.0V

TBHT = 230A, 3.18V

OMEGA = 1480C

Increasing max setpoint of TGHT = 700A

 Wednesday, February 01, 2017, 14:08

IGP1 = 3.8e-6 Torr.

TGHT = 700A, 10.96V

TBHT = 230A, 3.2V

OMEGA = 1705C

Increasing max setpoint of TGHT = 750A

 Wednesday, February 01, 2017, 15:02

IGP1 = 5.1e-6 Torr.

TGHT = 750A, 11.87V

TBHT = 230A, 3.2V

OMEGA = 1808C

Increasing max setpoint of TGHT = 800A

 Wednesday, February 01, 2017, 15:30

IGP1 = 6.6e-6 Torr.

TGHT = 800A, 12.86V

TBHT = 230A, 3.2V

OMEGA = 1903C

Will remain at max setpoints overnight.

 Thursday, February 02, 2017, 09:16

Remained at max setpoints for ~18hrs.

IGP1 = 9.5e-7 Torr.

OMEGA =1914C

TGHT = 800A, 12.83V

TBHT = 230A, 3.22V

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.

 Friday, February 03, 2017, 14:24

Vented in air and opened up this morning

Coating looks good.

See photos attached.

Nikita Bernier wrote:

Nikita Bernier wrote: Nikita Bernier wrote:  Friday, August 10, 2012, 19:54   Target boat with TaC coating, inside covered with a 0.002 inches thick Ta foil, wrapped with a 0.002 inches thick Ta foil, contains a Ta foil with TaO coating. See John's Ipad for their recipes. Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 830 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).    Saturday, August 11, 2012, 19:15 Heating process was going smoothly up to 400 A. See Attachment 1. Around 420 A, vacuum went up again and the voltage increased more quickly. It seems like resistance is building up. After reaching 530 A, the current was tapped down to 420 A in an effort to save the Ta boat. See Attachment 2. The current will stay at 420 A for the weekend until John takes a look at this.    Monday, August 13, 2012, 13:46  TGHT was ramped down at 2 A/min and then tapped down to 0A. See Attachment 1.  The target boat will be cooled down for about an hour before turning off the chiller.

 Tuesday, August 14, 2012, 16:56

Summary:

The purpose of this experiment is to test the chemical and high temperature (1600C) resistance of a Ta foil (0.001" thick) coated with Ta2O5, so it can be used as the under-layer for the BeO sintering process.

The Ta2O5 (white powder, -325 mesh) was prepared in a non-aqueous solution and was sprayed on a piece of Ta foil. 

The coated foil was rolled up and inserted in a Ta-coated (previously sintered) target boat for heating.

The foil was heated up to 520A (~1200C) and evidently,Ta2O5 started to react with Ta foil, and the foil became brittle and cracked (see attachment#1).

In conclusion, Ta2O5 is not a good protection layer for Ta material - at least for our applications.

Tuesday, April 03, 2012, 08:54

Yesterday, a new target boat was sprayed with TaC coating and let dried.

The boat was then installed in the Evap#2 chamber and pumped down to 10-6 Torr before the target heater was turned on.  NOTE: Target boat is not wrapped with Ta-heat shield. 

TGHT auto ramping was initiated at 2.0A/min and max setpoint to 700A.  The voltage was set at 3V; therefore, the current only ramped up to 250A over night.

--> Increased the TGHT voltage to 15A, and continue ramping the TGHT to 700A.  Currently vac at low 2.3e-7 Torr. 

 Tuesday, April 03, 2012, 09:12

The vac is at low 10e-7 as the TGHT is ramping up.  Changing ramping rate from 2A/min to 5A/min. 

Tuesday, April 03, 2012, 12:00  

TGHT reached to 700A. Measured temp @ 1280C. 

Tapped up TGHT to:

800A.  Measured temp @ 1400C. 

850A (local 843A/15.60V). Measured temp @ 1450C.  

900A (local 893A/16.88V).  Measured temp @ 1500C

 Tuesday, April 03, 2012, 14:35:

Try autoramping TGHT to 1000A but voltage has gone up close to the max limit (20V).  TGHT could only go up to ~970A (see attachment 1: TGHT_maxcurrent.jpg).  The heater remained at that current for ~1hr but auto cooling was initiated - at 10A/min.

Thursday, September 25, 2014, 17:32

Target boat is filled with Ta-coated endcaps.  The caps are stacked together.  In between each cap, a piece of graphite foil is used for separation so the Ta caps would not fused. 

See link for photos:

https://www.dropbox.com/sh/rydtdho6ggh4l3l/AAAYmvqT0mVQ_pnz4iecS4ksa?dl=0

The boat is wrapped with 3-layers of heatshields.  The chamber is currently being pumped down.

TGHT will be ramped up to 580A and the temperature will be measured.

Monday, September 29, 2014, 11:12

TGHt was stepped up to 40A on last Friday and chamber continues to pump down over the weekend.

Vac @ 2.56e-6 Torr, mp @ 19mTorr.

Ramping up TGHT 580A at 1.0A/min.

 Monday, September 29, 2014, 11:50

TGHT tripped off at 53A.  Reduce ramping rate to 0.5A/min for now.

 Monday, September 29, 2014, 16:17

Vacuum is coming down to 9.5e-7 Torr.  Increased ramping rate to 1.0A/min.

 Tuesday, September 30, 2014, 11:59

TGHT reached to 580A/10.18V.  Target has been heated at that current for almost 12 hrs. Vac @ 4.9e-7 Torr.

Local temp measured with Mikron = (1500C + 250 C correction) = 1750C

Cooling down at 2A/min.

 Thursday, October 02, 2014, 11:13

The coating is fully sintered; no sign of any damage on the endcaps.  

Process is successful.  

Laura Lambert wrote:

Tuesday, September 23, 2014, 15:00 A new target boat [new design with no end caps] was sprayed with TaC coating and let dry. The target boat is wrapped with 3-layers of Ta-heat shield. The boat was installed in EVAP2, chamber is currently being pumped down.

 Tuesday, September 23, 2014, 18:31

Chamber was pumped down to 2.5e-6 Torr. 

HS water valve open; no leaks detected.

Stepping up TGHT to 40A - pressure is increasing...

 Tuesday, September 23, 2014, 19:05

Auto-ramping TGHT to 580A at 0.5A/min.  Temperature will be measured and TGHt will be adjusted accordingly.

 Wednesday, September 24, 2014, 11:57

Pressure is stable at 2.2-6 Torr as TGHT is ramping up.  Increase ramping rate to 2.0A/min.  Currently TGHT at 540A.

 Wednesday, September 24, 2014, 15:36

TGHT at 580A for 2 hrs.  Inner tube temp (left side wall, viewing from the window port) ~1800C (measured with Mikron = 1550C +250C em. correction); Vac @ 1.67e-6 Torr.

Temperature measurement distance from the window to Mikron = 45cm.

Increase TGHT to reach 2000C (Mikron @ 1750C)

 Wednesday, September 24, 2014, 18:14

TGHT has gone up to 725A/13.2V.  Temp measured at 1740C (+250C = ~2000C).  Pressure gone up to 5.5e-6 Torr and it's coming down slowly.

Will continue heating at this temperature for a few hours; then cool down afterward.

 Wednesday, September 24, 2014, 18:56

Temperature is pretty stable at 1740C on Mikron, and pressure is still coming down, currently at 2.9e-6 Torr.

Slow ramping down TGHT at 1.0A/min.  The chamber should be ready for venting tomorrow. 

Target boat will be inspected.

 Thursday, September 25, 2014, 17:25.

The boat was inspected and it turned out great!  The coating was fully sintered and there is no sign of damage on the boat. 

See the link for photos.

https://www.dropbox.com/sh/m7ycqhkj4avfull/AABHVTweTsP4ajeWZ6uoY010a?dl=0

John Wong wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.

 Wednesday, January 22, 2014, 18:09

After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2). 

Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN 

Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes. 

Maybe a fault in the water signal.  If it happens again, the water signal should be replaced.

Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK!

Chamber is a bit warm now.  Will allow time to cool down.

Will vent the chamber tomorrow and the boat will be inspected. 

 Monday, January 20, 2014, 16:32

A new target boat was sprayed with TaC coating and let dry this morning.

The target boat is NOT wrapped with Ta-heat shield.

The boat was installed in Evap#2, chamber is currently being pumped down overnight.

Laura Lambert wrote:

Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.

 Tuesday, January 21, 2014, 11:10

Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.

Laura Lambert wrote:

Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.

 Tuesday, January 21, 2014, 11:51

Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off.

Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.

 close-call!

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!

 Wednesday, January 22, 2014, 09:46

TGHT has been slowly ramping up overnight at a rate of 0.2A/min.

IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.

 Wednesday, January 22, 2014, 13:43

TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr.

Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.

 Wednesday, January 22, 2014, 15:09

TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C.

Note: This is the "old" design boat.  The new design boat was able to heat up to 900A/16.88 - the temperature was measured at about 1500C.  (see elog: https://elog.triumf.ca/TIS/Evaporator_2/15)

Target will be heated for a few hours and will be cooled down later tonight.

The chamber will be vented tomorrow and the boat will be inspected.

John Wong wrote:

John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.

 Thursday, January 23, 2014, 16:18

Chamber vented overnight and was opened up this morning.

Target boat not fully sintered [see attached photos].

Chamber currently being pumped down again in order to continue with sintering TaC coating.

HS cooling water valves were opened, no leaks detected.

Will ramp up to 700A again over the weekend.

Laura Lambert wrote:

John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.

 Friday, January 24, 2014, 14:21

Chamber was pumped down to 1.7e-7 Torr.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A.

Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.

Laura Lambert wrote:

Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.

 Monday, January 27, 2014, 10:05

TGHT reached 700A over the weekend. Measured temp @ 2000C.

TGHT auto-cool inititated at 2.0A/min.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.    Monday, January 27, 2014, 10:05 TGHT reached 700A over the weekend. Measured temp @ 2000C. TGHT auto-cool inititated at 2.0A/min.

 Tuesday, January 28, 2014, 11:53

Chamber cooled down overnight, vented and opened up this morning.

Target boat still has a strip of green, still not fully sintered! [see attached photos].

Chamber currently being pumped down again to attempt sintering - round 3.

Laura Lambert wrote:

Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: John Wong wrote: John Wong wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote: Laura Lambert wrote:  Monday, January 20, 2014, 16:32 A new target boat was sprayed with TaC coating and let dry this morning. The target boat is NOT wrapped with Ta-heat shield. The boat was installed in Evap#2, chamber is currently being pumped down overnight.    Tuesday, January 21, 2014, 11:10 Chamber was pumped down to ~2e-7 Torr. HS cooling water valves were opened, no leaks detected. TGHT was stepped up to 35A, voltage max set at 13V. TBHT currently @ 0A. Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 2.0A/min and max setpoint to 700A. Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.    Tuesday, January 21, 2014, 11:51 Vacuum was grumpy and was well on it's way to tripping off [reached 5e-5 Torr], auto ramping was stopped at ~95A and quickly stepped down to 90A to avoid tripping it off. Allowed vacuum to settle back down to 2.3e-6 Torr. Auto ramping changed to 0.2A/min and re-started.  close-call!    Wednesday, January 22, 2014, 09:46 TGHT has been slowly ramping up overnight at a rate of 0.2A/min. IGP1 = 2.9e-7 Torr, TGHT = 342A; stepping ramping rate up to 2.0A/min.    Wednesday, January 22, 2014, 13:43 TGHT is sitting at 693A, IGP1 = 1.3e-6 Torr. Stepping up TGHT voltage up to 14V from 13.05V to reach the max current of 700A.    Wednesday, January 22, 2014, 15:09 TGHT reached to 700A/12.83V.  Local temperature on the boat surface was measured at ~1500C. Target will be heated for a few hours and will be cooled down later tonight. The chamber will be vented tomorrow and the boat will be inspected.    Wednesday, January 22, 2014, 18:09 After the boat was heated for ~4hrs, TGHT tripped off on IEVAP2:TBHT2 (see attachment #1, #2).  Tried clearing the water interlock via EPICS - failed to clear.  Checked the local water valves - ALL VALVES are OPEN  Tried closing and re-opening the IEVAP2:TBHT2 valves, interlock cleared after a few minutes.  Maybe a fault in the water signal.  If it happens again, the water signal should be replaced. Turned back on the power supply - TGHT current/voltage are holding.  Target boat may be OK! Chamber is a bit warm now.  Will allow time to cool down. Will vent the chamber tomorrow and the boat will be inspected.     Thursday, January 23, 2014, 16:18 Chamber vented overnight and was opened up this morning. Target boat not fully sintered [see attached photos]. Chamber currently being pumped down again in order to continue with sintering TaC coating. HS cooling water valves were opened, no leaks detected. Will ramp up to 700A again over the weekend.  Friday, January 24, 2014, 14:21 Chamber was pumped down to 1.7e-7 Torr. TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently sitting at 0A. Waited 20min, vacuum consistently stable. Auto-ramp initiated at 2.0 A/min and max setpoint to 700A.    Monday, January 27, 2014, 10:05 TGHT reached 700A over the weekend. Measured temp @ 2000C. TGHT auto-cool inititated at 2.0A/min.    Tuesday, January 28, 2014, 11:53 Chamber cooled down overnight, vented and opened up this morning. Target boat still has a strip of green, still not fully sintered! [see attached photos]. Chamber currently being pumped down again to attempt sintering - round 3.

 Tuesday, January 28, 2014, 13:06

Discussed with Peter. Instead of re-sintering the whole boat by itself, end caps will be inserted for sintering and will be placed further down the boat where the sintering process appears complete.

 Tuesday, February 18, 2014, 12:12

A new target boat was sprayed with TaC coating and let dry.
The target boat is NOT wrapped with Ta-heat shield.

Thermocouples have been attached to the target boat in order to monitor the internal temperature of the new target boat design. 

The boat was installed in Evap#2, chamber is currently being pumped down.

 Tuesday, February 18, 2014, 14:20

Chamber was pumped down this morning to 2.9e-6 Torr. HS cooling water valves were opened, no leaks detected.

TGHT was stepped up to 35A, voltage max set at 14V. TBHT currently at 0A.

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 700A.

Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.

Temperature reading on left: thermocouple touching edge of target boat; temperature reading on right: thermocouple floating in center of target boat.

 Wednesday, February 19, 2014, 09:11

TGHT has been slowly ramping up overnight at a rate of 0.2A/min

IGP1 = 3.9e-7 Torr, TGHT = 260A; stepping ramping rate up to 2.0A/min

 Wednesday, February 19, 2014, 15:25

IGP1 = 9.4e-7 Torr

Thermocouple T2 = 1267.8C

Internal temp measured with Mikron = 1600C

Increasing max setpoint to 720A due to previous not fully sintered new design of target boat.

 Thursday, February 20, 2014, 09:17

Thermocouple T2 = 1254.5C

Internal temp measured with Mikron = 1811C

IGP1 = 2.6e-7 Torr

Reached max setpoint yesterday evening.

Initiating auto-cooling at 2.0A/min.

 Friday, February 21, 2014, 10:47

Vented and opened chamber this morning.

Target boat not fully sintered. [see attached photos]

Close to a full sinter, and will re-sinter next week with endcaps, so will not re-sinter by itself.

 Tuesday, September 23, 2014, 15:00

A new target boat [new design with no end caps] was sprayed with TaC coating and let dry.

The target boat is wrapped with 3-layers of Ta-heat shield.

The boat was installed in EVAP2, chamber is currently being pumped down.

 Friday, August 10, 2012, 19:54

Target boat with TaC coating, inside covered with a 0.002 inches thick Ta foil, wrapped with a 0.002 inches thick Ta foil, contains a Ta foil with TaO coating.

See John's Ipad for their recipes.

Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 830 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum).