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Entry  Friday, March 07, 2014, 11:46, Laura Lambert, , 40282-3, TARGET BOAT, In progress, Sintering TaC coated end caps 
    Reply  Friday, March 07, 2014, 22:25, John Wong, , 40282-3, TARGET BOAT, Problems, Sintering TaC coated end caps 
Message ID: 121     Entry time: Friday, March 07, 2014, 11:46     Reply to this: 122
Author: Laura Lambert 
Target Material:  
Target Oven W.O#: 40282-3 
Source: TARGET BOAT 
Status: In progress 
Subject: Sintering TaC coated end caps 

 Friday, March 07, 2014, 11:41

The target container end-caps were sintered previously, but did not fully complete the sintering process [See elog entry # 119 EVAP2]

The caps are inserted in the target boat wrapped in graphite foils with 3 x Ta-heat shields.

The chamber was pumped down overnight.

IGP1 = 2e-7 Torr

HS cooling water valves were opened; no leaks detected.

TGHT was stepped up to 35A, voltage max set at 9.05V. TBHT currently at 0A.


 Friday, March 07, 2014, 11:52

Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.5A/min and max setpoint to 500A.

Will ramp to 500A due to last failed round of end caps breaking with 3-ta heat shields at 580A.

Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.


 Friday, March 07, 2014, 13:21

IGP1 = 8e-7 Torr.

TGHT = 72A

Vacuum stable; therefore, increasing ramping rate up to 1.0A/min


 Friday, March 07, 2014, 14:20

IGP1 = 9.8e-7 Torr

TGHT = 130A

Vacuum stable; therefore, increasing ramping rate up to 2.0A/min


 

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