Laura Lambert wrote: |
Tuesday, September 23, 2014, 15:00
A new target boat [new design with no end caps] was sprayed with TaC coating and let dry.
The target boat is wrapped with 3-layers of Ta-heat shield.
The boat was installed in EVAP2, chamber is currently being pumped down.
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Tuesday, September 23, 2014, 18:31
Chamber was pumped down to 2.5e-6 Torr.
HS water valve open; no leaks detected.
Stepping up TGHT to 40A - pressure is increasing...
Tuesday, September 23, 2014, 19:05
Auto-ramping TGHT to 580A at 0.5A/min. Temperature will be measured and TGHt will be adjusted accordingly.
Wednesday, September 24, 2014, 11:57
Pressure is stable at 2.2-6 Torr as TGHT is ramping up. Increase ramping rate to 2.0A/min. Currently TGHT at 540A.
Wednesday, September 24, 2014, 15:36
TGHT at 580A for 2 hrs. Inner tube temp (left side wall, viewing from the window port) ~1800C (measured with Mikron = 1550C +250C em. correction); Vac @ 1.67e-6 Torr.
Temperature measurement distance from the window to Mikron = 45cm.
Increase TGHT to reach 2000C (Mikron @ 1750C)
Wednesday, September 24, 2014, 18:14
TGHT has gone up to 725A/13.2V. Temp measured at 1740C (+250C = ~2000C). Pressure gone up to 5.5e-6 Torr and it's coming down slowly.
Will continue heating at this temperature for a few hours; then cool down afterward.
Wednesday, September 24, 2014, 18:56
Temperature is pretty stable at 1740C on Mikron, and pressure is still coming down, currently at 2.9e-6 Torr.
Slow ramping down TGHT at 1.0A/min. The chamber should be ready for venting tomorrow.
Target boat will be inspected.
Thursday, September 25, 2014, 17:25.
The boat was inspected and it turned out great! The coating was fully sintered and there is no sign of damage on the boat.
See the link for photos.
https://www.dropbox.com/sh/m7ycqhkj4avfull/AABHVTweTsP4ajeWZ6uoY010a?dl=0
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