ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
573
|
Thursday, April 21, 2022, 09:45 |
Darwin Ortiz Rosales | TaC | 42218-2 | LP-IG-LIS | Done | TaC coating | Thursday, April 21, 2022, 09:43
TaC coated Target container was placed in Evaporator 2 yesterday and left pressuring down.
Ta Heatshields: 3
Target temperature on OMEGA = 1800-1850 C
OMEGA slope: 0.990
Target time at temperature = 4 hours
Target final TBHT current: 230A
Approximate final TGHT current: 420A (will adjust manually)
Heating autoramp started @ ~2A/min on both TGHT and TBHT
initial IGP1 = 9.3e-7 Torr
Thursday, April 21, 2022, 10:38
Pressure trending down after peak. Start autoramp at 1A/min to 50A on both TGHT and TBHT.
Thursday, April 21, 2022, 10:56
Pressure continues to decrease. Will ramp up faster @4A/min to 90A for both TGHT and TBHT.
Thursday, April 21, 2022, 11:07
Second peak has begun to form . Will keep at 90A awaiting stabilization
Thursday, April 21, 2022, 11:35
pressure stable. Continue to autoramp at 1A/min and if pressure stable increase ramp to 4A/min
Thursday, April 21, 2022, 11:49
small peak observed and stabilizing. Autoramp @ 6A/min to 400A on TGHT and to 230A on TBHT
Thursday, April 21, 2022, 12:35
Regression plot . 1800C should be reached ~1800C.
Thursday, April 21, 2022, 12:44
Target current reached.
OMEGA = 1762 C
Will manually bump current to 415 A
OMEGA = 1802 @ 415 A @ 12:51 pm
Thursday, April 21, 2022, 16:50
OMEGA=1823 C
IGP1= 2.9e-06 Torr
TGHT= 417 A, 7.2 V
TBHT= 232A, 3.0V
Rampdown will start at -2A/min for both TGHT and -1A/min TBHT
|
373
|
Monday, June 05, 2017, 15:20 |
Laura Lambert | Empty | 42218-15 | LP-SIS | Done | Sintering TaC coating on UCx#21 container | Monday, June 05, 2017, 15:20
Container coated with TaC using 'flushing technique' and let dry over weekend.
Cleaned ionizer tube with acetone, no coating inside ionizer tube.
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
Tuesday, June 06, 2017, 10:00
First time not turning water off and flushing lines after last use.
HS water valves have remained open since the last time evap2 was used [conditioning Ta#52]
No leak check done.
Tapped up manually to 35A.
Waited ~25min
Vacuum stable.
IGP1 = 2.9e-6 Torr
IGP2 = 4.8e-6 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 350A
Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Wednesday, June 07, 2017, 09:26
TGHT = 304A, 4.46V
TBHT = 169A, 2.769V
IGP1 = 6.1e-7 Torr
IGP2 = 7.3e-7 Torr
Vacuum stable.
Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.
Wednesday, June 07, 2017, 10:40
TGHT = 350A, 5.28V
TBHT = 203A, 3.39V
IGP1 = 1e-6 Torr
Increasing ramping rate for TBHT to 1.0A/min
Wednesday, June 07, 2017, 12:10
TGHT = 350A, 5.26V
TBHT = 230A, 3.99V
IGP1 = 7.0e-7 Torr
IGP2 = 8.3e-7 Torr
OMEGA = 1600C
Vacuum stable.
Increasing max setpoint of TGHT to 400A
Re-initiating ramping rate of TGHT at 1.0A/min
Wednesday, June 07, 2017, 15:42
Tapped up to reach final desired temperature.
TGHT = 450A, 7.28V
TBHT = 230A, 4.02V
IGP1 = 9.0e-7 Torr
IGP2 = 1.07e-6 Torr
OMEGA = 1910C
Will remain at max setpoints overnight.
Thursday, June 08, 2017, 08:51
Remained at max setpoints for 17hrs.
TGHT = 450A, 7.28V
TBHT = 230A, 4.02V
IGP1 = 2.6e-7 Torr
IGP2 = 2.9e-7 Torr
OMEGA = 1899C
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Thursday, June 08, 2017, 16:28
Vented in air and taken out this afternoon.
Container looks good!
Transferred into glove box.
|
372
|
Tuesday, May 30, 2017, 14:40 |
Laura Lambert | Ta | 42218-14 | LP-SIS | Done | Conditioning Ta#52 | Tuesday, May 30, 2017, 14:36
Target consists of 400 discs.
Total packed length 2.9cm [exactly 8.05cm space on both sides]
Total mass 42.8228g [Incl foils + Ta wire on 4 packs]
Target consists of 320 single discs and 4x20 packs of Ta discs
Discs in target are arranged as follows: 80singles / 1pack / 80singles / 2packs / 80singles / 1pack / 80singles
3x Ta Heat shields.
No endcaps inserted, no Rh foil inserted.
Chamber currently pumping down.
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 350A at 2.0A/min.
Final desired temperature = 1900C
OMEGA slope = 0.98
Windows cleaned.
Vacuum limit stop at 3.0e-5 Torr, backing off at 4.0e-5 Torr.
Wednesday, May 31, 2017, 09:47
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
Vacuum stable.
IGP1 = 4.58e-7 Torr
IGP2 = 3.68e-7 Torr
Initiating auto ramp.
Wednesday, May 31, 2017, 14:07
IGP1 = 1.11e-6 Torr
IGP2 = 1.13e-6 Torr
TGHT = 354A, 5.45V
TBHT =233A, 4.01V
OMEGA = 1565C
Increasing max setpoint to 400A at same ramping rate.
Wednesday, May 31, 2017, 14:41
IGP1 = 1.19e-6 Torr
IGP2 = 1.24e-6 Torr
TGHT = 401A, 6.37V
OMEGA = 1708C
Increasing max setpoint to 425A at same ramping rate.
Wednesday, May 31, 2017, 15:51
Tapped up to ~1900C
TGHT = 480A, 7.85V
TBHT = 230A, 4.06V
OMEGA = 1912C
IGP1 = 1.85e-6 Torr
IGP2 = 2.06e-6 Torr
Will remain at max setpoints for a couple days before cooling
Friday, June 02, 2017, 13:19
Remained at max setpoint for 2days
TGHT = 480A, 7.85V
TBHT = 230A, 4.06V
OMEGA = 1885C
IGP1 = 2.15e-7 Torr
IGP2 = 2.07e-7 Torr
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Monday, June 05, 2017, 15:18
Vented in air and taken out this morning.
Target looks good
Wednesday, June 07, 2017, 15:41
Endcaps inserted.
Ta heat shield removed.
Rh foil inserted.
Handed off to assembly.
|
402
|
Wednesday, February 28, 2018, 15:18 |
Laura Lambert | Empty | 42218-13 | LP-SIS | Done | Sintering TaC coating on UCx#22 container | Wednesday, February 28, 2018, 15:16
Container coated with TaC using 'flushing technique' and let dry.
Q-tip to plug ionizer became stuck in ionizer, removed manually with small drill bit.
Inspected ionizer with microscope, ionizer still good.
Cleaned ionizer tube with acetone.
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Good vac at 3.0e-5, bad vac at 8.0e-5 Torr.
Thursday, March 01, 2018, 10:06
HW water valves opened yesterday, no leaks detected.
IGP1 = 2.8e-7 Torr
Tapped up manually to 40A.
Waited ~3hrs
Vacuum stable.
IGP1 = 5.3e-7 Torr
IGP2 = 5.4e-7 Torr
Initiating auto ramp for TGHT @ 1.0A/min to a max setpoint of 350A
Initiating auto ramp for TBHT @ 0.5A/min to a max setpoint of 230A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Thursday, March 01, 2018, 14:39
Vacuum started to climb very fast - auto-ramp was stopped.
Vacuum climbed up to IGP1 = 1.3e-4 Torr
Tapped TGHT back down to 80A from 90A, TBHT down to 50A from 60A.
Waited ~40min.
Vacuum stable, IGP1 = 2.6e-6 Torr
Restarting auto-ramp.
Thursday, March 01, 2018, 14:54
IGP1 = 2.1e-5 Torr
Vacuum climbing quite rapidly again, stopped auto-ramp and vacuum started to drop right away.
TGHT = 100A
TBHT = 56A
Waited ~10min
IGP1 = 6.0e-6 Torr
IGP2 = 5.2e-6 Torr
Decreasing ramping rate to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively, and re-initiating auto-ramp.
Friday, March 02, 2018, 10:18
TGHT = 350A, 5.61V
TBHT = 230A, 4.04V
IGP1 = 4.3e-7 Torr
IGP2 = 3.8e-7 Torr
OMEGA = 1624C
Vacuum stable.
Increasing max setpoint of TGHT to 400A
Re-initiating auto-ramp of TGHT.
Friday, March 02, 2018, 11:04
TGHT = 372A, 6.05V
IGP1 = 5.0e-7 Torr
Increasing ramping rate for TGHT to 1.0A/min
Friday, March 02, 2018, 11:44
TGHT = 400A, 6.60V
IGP1 = 6.9e-7 Torr
OMEGA = 1780C
Vacuum stable.
Increasing max setpoint of TGHT to 430A
Re-initiating auto-ramp of TGHT.
Friday, March 02, 2018, 12:17
TGHT = 430A, 7.22V
OMEGA = 1866C
IGP1 = 9.5e-7 Torr
Tapped up manually to OMEGA = 1910C
TGHT = 445A, 7.57V
TBHT = 230A, 4.07V
IGP1 = 1.1e-6 Torr
IGP2 = 9.9e-7 Torr
Monday, March 05, 2018, 08:41
Remained at max setpoints over the weekend.
TGHT = 445A, 7.47V
TBHT = 230A, 4.06V
IGP1 = 1.87e-7 Torr
IGP2 = 1.47e-7 Torr
OMEGA = 1894C
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Tuesday, March 20, 2018, 14:53
Vented in air.
Container was transferred to glove box for loading ~1 week ago
Container looks good.
|
340
|
Thursday, December 01, 2016, 16:08 |
Laura Lambert | Empty | 42218-12 | LP-SIS | Done | sintering TaC coating on UCx#19 container | Thursday, December 01, 2016, 16:06
Container coated with TaC using 'flushing technique' and let dry overnight.
Cleaned ionizer tube with acetone, no coating inside ionizer tube
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Friday, December 02, 2016, 11:24
Opened up HS water valves, no leaks detected.
Tapped up manually to 35A.
Waited ~25min, vacuum stable.
IGP1 = 1.65e-6 Torr
Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.
Max setpoints set for 350A and 230A for the TGHT and TBHT respectively.
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Monday, December 05, 2016, 09:38
TGHT = 350A, 5.38V
TBHT = 230A, 4.03V
OMEGA = 1550C
IGP1 = 3.2e-7 Torr
Tapping up to 1900C...
Monday, December 05, 2016, 14:11
OMEGA = 1905C
TGHT = 475A, 7.63V
TBHT = 230A, 4.07V
IGP1 = 8.5e-7 Torr
Tuesday, December 06, 2016, 08:41
TGHT = 475A, 7.76V
TBHT = 230A, 4.07V
IGP1 = 3.9e-7 Torr
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, December 07, 2016, 08:46
Evap2 was vented in air and opened up yesterday afternoon.
Container looks good, coating fully sintered.
|
388
|
Friday, September 15, 2017, 10:56 |
Laura Lambert | Ta | 42218-10 | HP-SIS | Done | Conditioning Ta#54 | Friday, September 15, 2017, 09:44
Target consists of 470 discs.
Total packed length 3.4cm [exactly 7.8cm space on both sides]
Total mass g [Incl foils + Ta wire on 6 packs]
Target consists of 350 single discs and 6x20 packs of Ta discs
Discs in target are arranged as follows: 1pack / 75singles / 1pack / 100singles / 2packs / 100singles / 1pack / 75singles / 1pack
1 long Ta Heat shield on each side, not incl center block.
No endcaps inserted, no Rh foil inserted.
Loaded into evap2 yesterday.
Chamber pumped down overnight.
TBHT will be ramped up to 230A at 1.0A/min.
TGHT will be ramped up to 650A at 2.0A/min.
Final desired temperature = 1900C
OMEGA slope = 0.98
HS water valves were already open.
Tapped up manually to 40A, vacuum stable.
IGP1 = 1.1e-6 Torr
IGP2 = 7.8e-7 Torr
Initiating auto-ramp.
Vacuum limit stop at 3.0e-5 Torr, backing off at 4.0e-5 Torr.
Monday, September 18, 2017, 08:38
TGHT = 647A, 10.04V
TBHT = 233A, 3.51V
IGP1 = 4.65e-7 Torr
IGP2 = 3.78e-7 Torr
OMEGA = 1700C
Increasing max setpoint of TGHT to 750A
Monday, September 18, 2017, 14:49
TGHT = 760A, 11.96V
TBHT = 233A, 3.54V
IGP1 = 8.9e-7 Torr
IGP2 = 8.6e-7 Torr
OMEGA = 1905C
Conditioning process complete.
Initiating auto-cool at 2.0A/min for the TGHT and 1.0A/min for the TBHT.
Tuesday, September 19, 2017, 10:38
Target was cooled down in sections so Yasser could take some temperature measurements with his thermocouples.
Vented in air and removed from evap2 this morning.
Target looks good.
Endcaps inserted and expanded.
Inserting Rh foil this afternoon.
Tuesday, September 26, 2017, 10:53
Tapped up manually to 230A over the course of ~35min.
TBHT striptool = 228A, 0.33V
TBHT direct readout = 230.4A, 0.33V
Vacuum good/ stable.
Minor spike to IGP1 = 1.5e-5 Torr ~5min after reached max setpoint of 230A.
IGP1 striptool = 3e-6 Torr
IGP1 direct readout = 3.79e-6 mBar
Initiating auto-cool at 2.0A/min.
|
350
|
Tuesday, February 21, 2017, 15:21 |
Laura Lambert | Empty | 42218-1 | LP-IG-LIS | Done | sintering TaC coating on UCx#20 container | Tuesday, February 21, 2017, 15:19
Container coated with TaC using 'flushing technique' and let dry overnight.
Cleaned ionizer tube with acetone, no coating inside ionizer tube
Wrapped with 3 x Ta heat shields, incl center block
Currently pumping down in evap2
OMEGA slope = 0.98
Good vac at 3.0e-5, bad vac at 4.0e-5 Torr.
Wednesday, February 22, 2017, 09:41
HS water valves opened, no leaks detected.
Tapped up manually to 35A
Waited ~45min
Vacuum stable.
IGP1 = 1.2e-6 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 350A
Initiating auto ramp for TBHT @ 0.1A/min to a max setpoint of 230A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Friday, February 24, 2017 by Anders
Continue manually to 1900 C
Friday, February 24, 2017, 16:24: TGHT at 400 A 6.35V IG1 = 4.5e-7 Torr 1660 C
Friday, February 24, 2017, 16:57: TGHT at 410 A 6.6 V IG1 = 5.0e-7 Torr 1700 C
Sunday, February 26, 2017 by Anders
Sunday, February 26, 2017, 14:13: TGHT at 425 A 6.9 V IG1 = 2.5e-7 Torr
Lab closed for weekend. No access to temp reading.
Monday, February 27, 2017, 16:12
Tapped up manually to 1900C this morning.
TGHT = 490A, 8.14V
TBHT = 230A, 2.98V
MIKRON = 1911C
OMEGA = 1904C
evap2 has remained at max setpoints for ~6hrs
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Tuesday, February 28, 2017, 11:57
Container finished sintering.
Vented in air and opened up this morning.
Container looks good
|
529
|
Saturday, February 13, 2021, 08:14 |
Darwin Ortiz Rosales | SiC | 41992-1 | TARGET BOAT | Done | Sintering of SiC discs for SEM | Saturday, February 13, 2021, 08:10
Ta boat loaded with 80 discs enclosed in graphite foil in pockets of 20. Sample A at both ends and sample B in the middle spaced out. Boat wrapped in Ta heat-shields (3 layers).
(A B B A)
Desired temperature= 1800C (expected TGHT approx 410 A).
good vacuum = 3.00 e-05 Torr
bad vacuum = 5.00 e-05 Torr
Evap2 left to pump down over previous night.
IGP1= 5.4e-7 Torr and stable
Initiating TGHT ramp up at 1 A/ min to 30 A
Saturday, February 13, 2021, 12:19
IGP1= 6.9e-06 Torr
Ramp to 50 A 1A/min
Saturday, February 13, 2021, 14:35
IGP1 = 6.4e-6 Torr
Pressure trending down.
Saturday, February 13, 2021, 14:56
IGP1= 4.9 e-6 Torr
Initiate Ramp up @ 1 A/min to 400 A
Changed ramp up to 0.5 A/min at around 11:30 pm
Sunday, February 14, 2021, 11:43
The current will be ramped up to 420 A according to the trendline approximation (see attachement 1)
Sunday, February 14, 2021, 12:26
IGP1 = 8.9 e-06 Torr and trending down
TGHT = 420 A, 7.5 V
OMEGA = 1730 C
Will ramp up to 428 A manually
Sunday, February 14, 2021, 12:30
Reached 428 A on TGHT.
OMEGA = 1760 C
Will bump to 430 A and hold for 4 hours
OMEGA= 1765 C
Sunday, February 14, 2021, 18:00
OMEGA = 1789 C
IGP1= 7.5 e -7 Torr
TGHT = 430.5 A , 7.8 V
Start ramping down at -1A/min to zero A
|
392
|
Tuesday, November 21, 2017, 13:55 |
Laura Lambert | Empty | 41882-4 | TARGET BOAT | Done | Sintering TaC coating on fully enclosed target boat for graphite test | Tuesday, November 21, 2017, 12:01
Boat coated with TaC using 'flushing technique' and let dry overnight.
Wrapped with 1 long Ta heat shield 3x
Loaded into evap2 just before lunch
IGP1 = 7.1e-6 Torr
OMEGA slope = 0.98
Good vac at 3.0e-4, bad vac at 8.0e-4 Torr.
HS water valves have remained open since the last time evap2 was used.
No leak check done.
Tapped up manually to 35A.
Waited ~25min
Vacuum stable.
IGP1 = 1.15e-5 Torr
IGP2 = 1.17e-5 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 300A
Once max setpoints achieved, will tap up manually to final desired temperature of 1900C
Wednesday, November 22, 2017, 09:32
TGHT = 270A, 4.15V
OMEGA = 1285C
IGP1 = 1.23e-6 Torr
IGP2 = 1.13e-6 Torr
Vacuum stable.
Increasing ramping rate to 1.0A/min and final setpoint to 350A
Wednesday, November 22, 2017, 10:25
TGHT = 325A, 5.15V
OMEGA = 1500C
IGP1 = 2.80e-6 Torr
IGP2 = 2.93e-6 Torr
Vacuum stable.
Increasing ramping rate to 1.5A/min and final setpoint to 400A
Wednesday, November 22, 2017, 10:49
TGHT = 350A, 5.60V
OMEGA = 1580C
IGP1 = 4.5e-6 Torr
IGP2 = 4.9e-6 Torr
Vacuum stable.
Increasing ramping rate to 2.0A/min
Wednesday, November 22, 2017, 11:18
TGHT = 400A, 6.64V
OMEGA = 1734C
IGP1 = 5.8e-6 Torr
IGP2 = 6.2e-6 Torr
Vacuum stable.
Increasing final setpoint to 450A.
Wednesday, November 22, 2017, 15:59
TGHT = 460A, 8.07V
OMEGA = 1898C
IGP1 = 1.34e-6 Torr
IGP2 = 1.27e-6 Torr
Sintering process complete.
Remained at max setpoints for just over 4hrs.
Initiating auto-cool at 2.0A/min.
Thursday, November 23, 2017, 13:09
Removed from evap2 this morning.
Coating looks good.
|
393
|
Thursday, November 23, 2017, 15:10 |
Laura Lambert | | 41882-4 | TARGET BOAT | Done | Graphite insert test | Thursday, November 23, 2017, 14:54
Graphite insert loaded into previously TaC coated target boat.
One endcap removed to allow for outgassing: left side out, right side in.
Weight of graphite tube + single endcap = 10.2012g
Same Ta heats shields remain on container from sintering TaC coating.
Currently pumping down in evap2.
Friday, November 24, 2017, 11:31
IGP1 = 4.52e-7 Torr
IGP2 = 3.43e-7 Torr
OMEGA slope = 0.98
Good vac at 3.0e-4, bad vac at 8.0e-4 Torr.
HS water valves have remained open since the last time evap2 was used.
No leak check done.
Tapped up manually to 50A.
Vacuum stable.
IGP1 = 5.34e-7 Torr
IGP2 = 5.54e-7 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 300A
Once max setpoints achieved, will tap up manually to final desired temperature of 2000C
Uranium targets go to a max temperature of 1950C online, so graphite insert should be tested to 2000C
Monday, November 27, 2017, 10:15
IGP1 = 2.5e-7 Torr
IGP2 = 1.9e-7 Torr
Reached 300A, 4.61V
OMEGA = 1298C
Tapped up manually to 485A, 8.46V
OMEGA = 1808C
Remained at this setpoint for a day
Tuesday, November 28, 2017, 15:41
IGP1 = 3.88e-7 Torr
IGP2 = 3.58e-7 Torr
Tapping up to 2000C...
Tuesday, November 28, 2017, 16:10
TGHT = 570A, 10.20V
OMEGA = 2005C
IGP1 = 9.64e-7 Torr
IGP2 = 1.05e-6 Torr
There was a minor drop in voltage at 540A, 9.58V - dropped to ~9.4V then slowly went back up to 9.58V [see photo]
Will remain at this setpoint overnight and cool down in the a.m.
Wednesday, November 29, 2017, 08:48
Voltage increased slowly while sitting at max setpoint of 570A [see photo]
TGHT = 570A, 11.20V --> voltage increased by 1.0V over ~16.5hrs
OMEGA = 2114C
IGP1 = 6.6e-7 Torr
IGP2 = 6.5e-7 Torr
Initiating auto-cool at 2.0A/min
Wednesday, November 29, 2017, 16:15
Vented in air and removed today.
Will update tomorrow with results and photos.
|
459
|
Thursday, September 26, 2019, 14:03 |
Aaron Schmidt | Nb | 41882-3 | TARGET BOAT | In progress | HS swap & test Nb target | HS# 42752-7
Thursday, September 26, 2019, 13:46: Remove Flexible lines HS
Thursday, September 26, 2019, 14:03: Assy installed.
Friday, September 27, 2019, 07:07: Vacuum @ 1.16e-06T.
Friday, September 27, 2019, 07:09: Waterlines opened. Vacuum stable @ 1.15e-06T
Monday, September 30, 2019, 10:04: Remove Nb target & assy. Install flexible line HS. |
522
|
Wednesday, November 04, 2020, 17:31 |
Ferran Boix Pamies | Empty | 41882-2 | TARGET BOAT | Done | Parasitic target graphite outgassing. | 2020-11-04 17:31: target installed with boat containing graphite container for outgassing. Roughing pump on.
2020-11-04 17:49 turbo on, leaving it pumping over night.
2020-11-05 11:32 leak check ok. Ramping up target to 200A 2A/10s.
2020-11-05 11:53 IGP1:1.1e-6T . Ramping up target to 300A 1A/10s.
2020-11-05 11:53 IGP1:1.2e-6T . Pyrometer:1320degC. Ramping up target to 400A 1A/10s.
2020-11-05 11:53 IGP1:1.8e-6T . Pyrometer:1650degC. Ramping up target to 500A 1A/10s.
2020-11-05 12:57 IGP1:3.4e-6T . Pyrometer:1910degC. Ramping up target to 525A 1A/10s.
2020-11-05 13:02 IGP1:3.6e-6T . Pyrometer:1990degC. Leaving it hot for 1h.
2020-11-05 14:00 IGP1:2e-6T stable . Pyrometer:1990degC. cooling down 2A/10s.
|
523
|
Thursday, November 05, 2020, 15:13 |
Ferran Boix Pamies | Empty | 41882-2 | TARGET BOAT | Done | cleaning treatment. | 2020-11-05 15:44 empty and naked boat in for heating up system and clean up. Turbo on.
2020-11-06 16:58 IGP1:4e-7T leak check ok. Ramping up target to 500A. 1A/10s.
2020-11-09 12:43 The target was left at 1500degC during the weekend.
2020-11-17 14:11 turbo pump off. Slow venting.
2020-11-18 09:18 Evap2 vented. Target removed. |
545
|
Sunday, April 04, 2021, 16:09 |
Ferran Boix Pamies | Empty | 41882-2 | TARGET BOAT | Done | parasitic target commissioning | 2021-04-04 16:07 New container is in with heatshields, vacuum 8.6E-6 torr. leak check done. ramping up current, checking both pyrometer and TC, 1A/10s.
2021-04-04 16:49 200A TGHT 250degC on TC 1130degC on pyrometer. Too low on TC, ramping down and venting to reposition TC in the foil.
2021-04-04 18:00 TC was slightly broken, repaired now. Pumping chamber.
2021-04-04 18:41 ramping up to 200A 1A/10s.
2021-04-04 18:41 200A TGHT, TC 389degC pyro 1130degC. ramping to 400A 1A/10s.
2021-04-04 18:41 300A TGHT, TC 554degC pyro 1440degC.
2021-04-04 18:41 400A TGHT, TC 735degC pyro 1720degC. ramping to 600A 1A/10s.
2021-04-04 20:15 500A TGHT, TC 891degC pyro 1990degC
2021-04-04 20:15 553A TGHT, TC 975degC pyro 2129degC, ramping down.
2021-04-06 13:44 Parasitic target plus thermocouples were introduced in evap2 the day before and put under vacuum. IG1 3E-7 torr, leak check done. Putting some power into HE while ramping up container to 100A 1a/10s.
2021-04-06 14:06 20W on HE 100A on target container. Everything stable. Ramping up to 200A 1A/10s
2021-04-06 14:06 20W on HE 200A on target container. Everything stable. Ramping up to 300A 1A/10s
2021-04-06 14:06 20W on HE 300A on target container. Everything stable 4.6E-7 torr. Ramping up HE to 40W.
2021-04-06 14:06 40W on HE 300A on target container. Everything stable 4.6E-7 torr. Ramping up container to 400A 1A/10s.
2021-04-06 14:06 40W on HE 400A on target container. Everything stable 1E-6 torr. Ramping up container to 500A 1A/10s.
2021-04-06 15:52 35W on HE 500A on target container. Everything stable 1.6E-6 torr. Ramping up He to 65W.
2021-04-06 18:40 at 50W on HE one of them broke, system ramped down, vented, HE replaced, pumping down system again.
2021-04-07 10:38 HE at 70W, ramping up container to 200A 1A/10s. Vacuum 3.3E-7 torr.
2021-04-07 10:59 HE at 70W, 200A on container, ramping up container to 300A 1A/10s. Vacuum 3.9E-7 torr.
2021-04-07 10:59 HE at 65W, 300A on container, ramping up container to 400A 1A/10s. Vacuum 4.5E-7 torr.
2021-04-07 11:50 HE at 70W, 400A on container, ramping up container to 500A 1A/10s. Vacuum 7.8E-7 torr.
2021-04-07 11:50 HE at 65W, 500A on container, ramping up container to 553A 1A/10s. Vacuum 1.4E-6 torr.
2021-04-07 11:50 HE at 65W, 553A on container. All good, ramping down. 1A,10s. |
585
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Tuesday, June 28, 2022, 09:31 |
Ferran Boix Pamies | Empty | 41882-2 | TARGET BOAT | In progress | TC test on Ta tube | Tuesday, June 27, 2022, early afternoon: We assembled the setup in evap2 and started the pumps leaving it running over night.
Tuesday, June 28, 2022, 09:31 Turbo pump stopped for unknown reasons a few hours after we left. Restarting the pump.
Tuesday, June 28, 2022, 10:23 Vacuum down to 1e-5T start to ramp up TGHT 1A/10s to 200A.
Tuesday, June 28, 2022, 1:20 pm, Ramped from 0-500A. thermocouple reading 900C while pyrometer reads 1600C. begin ramping down to 0A. |
480
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Monday, March 23, 2020, 07:50 |
Marla Cervantes | | 41882-1 | TARGET BOAT | Done | Conditioning graphite target #1 (T2) | Friday, March 20, 2020, 19:39
The target material is loaded in a graphite cartridge.
The graphite cartridge is placed in a new tantalum boat previously without TaC,
the Ta boat was wrapped with three new Ta heat shields.
The system is currently pumping down.
Monday, March 23, 2020, 07:49
IGP1 = 2.2e-7 Torr
Good vacuum= 3.00 e-5 Torr
Bad vacuum = 5.00 e-5 Torr
Ramping TGHT to 40A at 0.5A/min
Monday, March 23, 2020, 10:35
Due to the COVID-19, non-essential activities are wrapped up,
the conditioning of the carbon target will be postponed until further notice |
482
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Wednesday, May 20, 2020, 12:54 |
Marla Cervantes | | 41882-1 | TARGET BOAT | Done | Conditioning graphite target #1 (T2) |
Marla Cervantes wrote: |
Friday, March 20, 2020, 19:39
The target material is loaded in a graphite cartridge.
The graphite cartridge is placed in a new tantalum boat previously without TaC,
the Ta boat was wrapped with three new Ta heat shields.
The system is currently pumping down.
Monday, March 23, 2020, 07:49
IGP1 = 2.2e-7 Torr
Good vacuum= 3.00 e-5 Torr
Bad vacuum = 5.00 e-5 Torr
Ramping TGHT to 40A at 0.5A/min
Monday, March 23, 2020, 10:35
Due to the COVID-19, non-essential activities are wrapped up,
the conditioning of the carbon target will be postponed until further notice
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Wednesday, May 20, 2020, 12:50
On May 19 the pumps of EVAP2 were turned on to purge the system
Today Aaron made a leak check, for details, visit elog-481
Currently IGP1 = 8.17e-7 Torr
Thursday, May 21, 2020, 09:41
IGP1 = 4.5e-7 Torr
TGHT = 0.03 V, 0.028 A
Current will be increased manually to 10 A, and then it will be autoramp to 500 A
Whit this power supply the current increments are register since the beging
TGHT = 0.145 V, 10.35 A
During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to 50A:
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 10:39
The autoramp reached the 50 A set
TGHT = 0.65 V, 49.05 A
Power supply = 0.64 V, 50 A
IGP1 = 4.7e-7 Torr
Everything looks good, autoramp is set to 80 A same conditions
1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 10:49
The autoramp reached the 80 A set
TGHT = 1.075 V, 79.36 A
Power supply = 1.07 V, 80 A
IGP1 = 1.7e-6 Torr and increasing
Autoramp is set to 100 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
There was a jump in the vacuum e-log-482-fig-1.
Thursday, May 21, 2020, 11:01
The autoramp reached the 100 A set
TGHT = 1.4V, 99.9 A
Power supply = 1.4V, 100 A
IGP1 = 0.001 Torr and increasing
Autoramp is set to 120 A,conditions:
1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 11:12
TGHT = 1.75 V, 120.6 A
Power supply = 1.74 V, 120 A
IGP1 = 0.0018 Torr
The current will be hold and to let the vacuum reduce
Thursday, May 21, 2020, 11:34
TGHT = 1.8 V, 120.825 A
Power supply = 1.74 V, 120 A
IGP1 = 9.8e-5 Torr
Thursday, May 21, 2020, 11:37
Autoramp is set to 300 A,conditions:
2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr
Thursday, May 21, 2020, 12:21
TGHT = 5.015 V, 298.125 A
Power supply = 5 V, 300 A
IGP1 = 4.77e-5 Torr
Omega = 1130 degC
Note: Measurments will be taken with ARIEL's pyrometer (I will call it AP in this elog).
The emmisivity this pyrometer accounts for is 0.91 for the range of 1000 C to 1800 C
Above 01800 it will use 0.93 as the emissivity
AP = 977.7 degC
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493
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Friday, July 31, 2020, 11:16 |
Ferran Boix Pamies | Empty | 41882-1 | TARGET BOAT | Done | Thermocouple measurent of boat temperature | Boat with attached thermocouple type C with AREMCO ceramabond glue installed in evap2 the 30-07-2020
Vacuum 3.2e-6torr in IGP1 after night with the roughing pump and morning with turbo.
TGHT heater on.
ramp up started
1A/20s up to 200A
Thermocouple de-attached at about 400A.
Target cooled down. 1A/10s
Turbo and roughing pump off. System left with present vacuum over night. Tomorrow inspection. |
495
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Wednesday, August 05, 2020, 19:14 |
Ferran Boix Pamies | Empty | 41882-1 | TARGET BOAT | Done | Parasitic target cooling test | 2020-08-05 7.13pm Roughing pump on
2020-08-06 10:48am Turbo was turned on by Marla in the morning. Vacuum IGP1 4e-6Torr. Water leak check performed, everything good to start heating up target. Waiting for Anders confirmation to start.
2020-08-06 4:38pm after changing setup to metallic connections only. Roughing on. After some minutes abnormal behavior in vacuum.
Turning water off to see if it is a small water leak.
Water purged, no change in vacuum.
IEVAP2:RV1 was closed. After opening, normal vacuum behavior recovered. The valve is automatically closing when reaching 100Torr. Wasn't doing that before. Turbo on now.
2020-08-07 9:24am pumping over night, vacuum at 8e-7torr. Everything ready for test. Ramping up target heater.Up to 50A 1A/20s
2020-08-07 9:48am all good at 50A, ramping to 250 1A/10s
2020-08-07 10:27am all good at 250A, ramping to 400 1A/10s
2020-08-07 10:57am all good at 400A, ramping to 500 1A/10s
2020-08-07 11:17am Tc type C might have been deatached at 500A, ramping to 600 1A/10s
2020-08-07 11:37am All good, ramping to 700 1A/10s
2020-08-07 11:58am 1950degC on pyrometer, 1200degC on type C TC (probably not well attached anymore), TCs on heatshield [30-40]degC. Pressure 9e-6Torr
2020-08-07 12:44pm All values stable after 45min, starting to ramp up parasitic target heating elements.
2020-08-07 1:15pm Open circuit, would seem that one of the heating elements cracked. Cooling down the target.
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496
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Tuesday, August 11, 2020, 10:17 |
Ferran Boix Pamies | Empty | 41882-1 | TARGET BOAT | In progress | Contamination foils temperature test | The target was prepared and put under vacuum on 2020-08-10
2020-08-11 10:16am The pressure is 1e-6Torr. Leak checked performed, water on no problem. Starting to set target heating curve. 1A/10s up to 300A
2020-08-11 11:23am target at 300A-1200degC Temperatures on exposed foil show to be higher than expected. 300degC already, 70degC on covered by foil thermocouple. Putting 50 more amps at 1A/10s
2020-08-11 12:11pm target at 350A-1340degC. 350degC on exposed thermocouple. Ramping to 400A 1A/10s.
2020-08-11 12:28pm target at 400A-1420degC. 400degC on exposed thermocouple. Ramping to 450A 1A/10s. |
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