Thursday, November 23, 2017, 14:54
Graphite insert loaded into previously TaC coated target boat.
One endcap removed to allow for outgassing: left side out, right side in.
Weight of graphite tube + single endcap = 10.2012g
Same Ta heats shields remain on container from sintering TaC coating.
Currently pumping down in evap2.
Friday, November 24, 2017, 11:31
IGP1 = 4.52e-7 Torr
IGP2 = 3.43e-7 Torr
OMEGA slope = 0.98
Good vac at 3.0e-4, bad vac at 8.0e-4 Torr.
HS water valves have remained open since the last time evap2 was used.
No leak check done.
Tapped up manually to 50A.
Vacuum stable.
IGP1 = 5.34e-7 Torr
IGP2 = 5.54e-7 Torr
Initiating auto ramp for TGHT @ 0.2A/min to a max setpoint of 300A
Once max setpoints achieved, will tap up manually to final desired temperature of 2000C
Uranium targets go to a max temperature of 1950C online, so graphite insert should be tested to 2000C
Monday, November 27, 2017, 10:15
IGP1 = 2.5e-7 Torr
IGP2 = 1.9e-7 Torr
Reached 300A, 4.61V
OMEGA = 1298C
Tapped up manually to 485A, 8.46V
OMEGA = 1808C
Remained at this setpoint for a day
Tuesday, November 28, 2017, 15:41
IGP1 = 3.88e-7 Torr
IGP2 = 3.58e-7 Torr
Tapping up to 2000C...
Tuesday, November 28, 2017, 16:10
TGHT = 570A, 10.20V
OMEGA = 2005C
IGP1 = 9.64e-7 Torr
IGP2 = 1.05e-6 Torr
There was a minor drop in voltage at 540A, 9.58V - dropped to ~9.4V then slowly went back up to 9.58V [see photo]
Will remain at this setpoint overnight and cool down in the a.m.
Wednesday, November 29, 2017, 08:48
Voltage increased slowly while sitting at max setpoint of 570A [see photo]
TGHT = 570A, 11.20V --> voltage increased by 1.0V over ~16.5hrs
OMEGA = 2114C
IGP1 = 6.6e-7 Torr
IGP2 = 6.5e-7 Torr
Initiating auto-cool at 2.0A/min
Wednesday, November 29, 2017, 16:15
Vented in air and removed today.
Will update tomorrow with results and photos.
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