Tuesday, October 18, 2022, 13:52

38 pieces of samples made of TiO2/C/PVP loaded into a target boat wrapped with 2 layers of Ta-heat shield.

Samples will be heated to 1700, 1800, 1900, and 2000 C

Some of the pieces will be removed after each target temperature 

Target chamber has been pumping down and the current pressure reading is 6.62e-6 T

 Tuesday, October 18, 2022, 14:12

TGHT will be autoramped to 250 A

Good vacuum: 3e-5 Torr

Bad vacuum: 5e-5 Torr

Omega slope: 0.99

Initiate autoramp: 1 A/min

Hannah Toy wrote:

Tuesday, October 18, 2022, 13:52 38 pieces of samples made of TiO2/C/PVP loaded into a target boat wrapped with 2 layers of Ta-heat shield. Samples will be heated to 1700, 1800, 1900, and 2000 C Some of the pieces will be removed after each target temperature  Target chamber has been pumping down and the current pressure reading is 6.62e-6 T  Tuesday, October 18, 2022, 14:12 TGHT will be autoramped to 250 A Good vacuum: 3e-5 Torr Bad vacuum: 5e-5 Torr Omega slope: 0.99 Initiate autoramp: 1 A/min

 Wednesday, October 19, 2022, 09:42

TGHT has reached to 250A/3.95V, Temp at ~1100 C.  (The archiver is currently not working; already contacted Control to look into it.)

Pressure reached below 4.9 e-7 Torr. 

Auto-ramp to 300 A at 2A/min.  Continue to monitor.

 Wednesday, October 19, 2022, 10:24

TGHT reached to 300 A/4.89V.  Temp at 1206 C. 

Pressure went up slightly and came down after the TGHT setpoint was reached, see attachment#1.

Continue to auto-ramp to 350A at 2A/min.

 Wednesday, October 19, 2022, 11:35

TGHT reached to 350A/5.8V.  Temp at 1360C.

Pressure reached above 1e-6 Torr and came down after TGHT reached the setpoint. 

Continue to auto-ramp to 400 A at 2A/min

 Wednesday, October 19, 2022, 11:57

TGHT reached to 400 A/6.89V.  Temp at 1485C.

Pressure went up to 3.3e-6 Torr and came down after TGHT reached the setpoint,  see attachment#2.

A temp vs current plot has been generated (see shared folder \Hannah\) - est TGHT 480A to reach 1700 (T1).

Auto-ramp to 420 at 1A/min.  Continue to monitor closely...

 Wednesday, October 19, 2022, 13:01

TGHT reached 420A/7.23V, Temp at 1520 C.

Continue auto-ramping to 440A at 1A/min.

 Wednesday, October 19, 2022, 13:42

TGHT reached 440A/7.65V.  Temp at 1572 C

Continue auto-ramping to 460A at 1A/min.

Wednesday, October 19, 2022, 14:10

TGHT reached to 460A/8.10 V.  Temp at 1628 C.

Tapping up TGHT to reach 1700 C

 Wednesday, October 19, 2022, 15:33

TGHT was tapped up to 474A, Temp reached to 1700 C since 14:30.

Pressure is slowing coming down, currently at 1.4 e-6 Torr.

Will hold at this target current for a few hours.

 Wednesday, October 19, 2022, 16:58

Temp went up slightly to 1713 C as the pressure is coming down. 

Lower TGHT to 468A/8.45V to maintain the temp at 1700 C.

 Wednesday, October 19, 2022, 19:55

Temp went up again to 1716 C, but this time the pressure also went up, see attachment#3.  Not sure why the target got hotter... the voltage seems normal and consistent. 

Lower TGHT to 462A/8.44V to maintain at 1700 C. 

Continue monitoring...

 Wednesday, October 19, 2022, 22:56

Temp went up another 10 C, to 1710 C, TGHT is holding at 462 A/8.48V.  Notice the TGHT current readback is fluctuating between 458A - 463 A. 

Initiated cooling.. 2A/min

 Friday, October 21, 2022, 08:55

 All the samples were taken out from the Evap on Thursday Oct 20.  We decided to do so because there was not enough sample in each batch for XRD analysis.  All the sample will be analyzed as treated at 1700 C. 

See attachement #$ for the overall TGHT/Vac plot.

Tuesday, November 01, 2022, 17:24

2 samples of np-TiO2/C fibres were produced using the e-spinner.  Each sample was wrapped with a piece of graphite sheet, and then loaded into a target container. 

Sample will be heated to 1700 C.

TGHT will be autoramped to 450 A; this should be close to 1600 C. (see elog#596)

Good vacuum: 3e-5 Torr

Bad vacuum: 5e-5 Torr

Omega slope: 0.99

Initiate autoramp: 1 A/min

Chamber has been pumped down below 4.2e-6 Torr.

 Tuesday, November 01, 2022, 22:46

 Pressure currently at 6.4e-7 Torr.

Initiated auto-ramping

 Wednesday, November 02, 2022, 09:37

TGHT was ramped up to 448A (readback 445-452A / 8.05V - 8.11V).  The voltage is much higher than the last process, see elog #596.

Temperature is much higher at this current, reading at 1870 - 1872 C. 

Will keep at this setting for now and continue to monitor.

See attachment#1 for the TGHT-Pressure plot.

 Wednesday, November 02, 2022, 21:35

Samples have been heated for over 16 hours; temp has been stabilized at 1875 C, vacuum at 7.3 e-7 Torr. 

Initiated cooling at 1A/min.

Chamber will be vented tomorrow morning.

Thursday, November 24, 2022, 11:01

Target container contains one disc of e-spun TiO2/PAN fibrous disc, (Ref sample P-134).

Sample will be heated to 1875C, similar to the previous process, see e-log ID#599.

TGHT will be autoramped to 350 A and monitor the conditions before ramping up further.

Good vacuum: 3e-5 Torr

Bad vacuum: 5e-5 Torr

Omega slope: 0.99

Initiate autoramp: 1 A/min

Chamber has been pumped down below 5.0e-6 Torr.

 Friday, November 25, 2022, 08:38

TGHT reached to 348A/5.8V; temp is holding at 1600 C since 19:00 yesterday, see attachment#1.

Stepping up TGHT to 400A and continue to monitor.

 Friday, November 25, 2022, 09:45

TGHT reached to 400A/6.8V; temp holding at 1758C.  Pressure coming down from 6.6e-7 Torr.

Ramping up to 410A.

 Friday, November 25, 2022, 12:28

TGHT reached 410A/7.08V.  temp holding at 1790 C.  Pressure coming down from 6.9e-7 Torr. 

Ramping up to 430A.

 Friday, November 25, 2022, 13:01

TGHT reached 430A/7.4V. Temp holding at 1837 C.  Pressure coming down from 7.73e-7 Torr.

Ramping up to 440A.

 Friday, November 25, 2022, 13:50

TGHT reached to 440A/7.6V.  Temp holding at 1864C.  Tapping TGHT to 444A (readback 443A - 449 A)/7.7V. 

Desired Temp has reached, 1875 C.  Will continue to hold on this temp over the weekend.

 Sunday, November 27, 2022, 21:14

TGHT has been holding at 442A (lowered by 2 A on Fri to maintain 1875C).  Temp increased to 1887C.  Pressure at 2.5e-7 Torr. 

See attachment#2 for plots/temp. 

Initiated cooling at 1A/min.

Saturday, March 04, 2023, 08:29

Ta LP-FEBIAD with 369 discs plus 5 removable discs wrapped with 3 Ta heat-shields (in layers)

Evap 2 will be pumped down over previous night

Desired temperature = 1500 C as in Elog #52 , TGHT will be ramped up to 300 A and then adjusted manually to 1500C if temperature readings are ok

otherwise will use plot from coating sintering to approximate 1500C.

TBHT will be set fixed at 230A (max).

Good vacuum = 5.00 e-4 Torr

Bad vacuum = 5.00 e-2 Torr

IGP1= 3.4 e-07 Torr

Start autoramp @2A/min to 80 A then autoramp heat @1A/min to 230 A (both TGHT and TBHT)

  Then autoramp TGHT to 300 A

-

Saturday, March 04, 2023, 22:27

At 332 A, 5.6V on TGHT, 230 A, 3.3 V TBHT

OMEGA = 1370 C

Will autoramp to 375A on TGHT @0.25A/min then leave for 4 hours at 1500C

Cooling should start at 6 am march 5th

OMEGA reading 1498 @ 2 am

Sunday, March 05, 2023, 06:03

OMEGA reading 1442 C @550am

ramped up to 394 A on TGHT and OMEGA reads 1500 C

will leave for 40 minutes than test ramp up to observe outgassing

d until 715 am then begin rampdown.

Sunday, March 05, 2023, 07:22

ramped to 425 to test further outgassing temperature increase observed but only while increasing current.

OMEGA = 1590 C

TGHT= 425A, 7.6V

TBHT= 230A, 3.3V

IGP1=2.0e-06 Torr

ramping down @-2A/min on TGHT and -1A/min TBHT

Wednesday, April 26, 2023, 09:32

LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses

50 packs of 5 and the rest are singles

TaC coated (sintered) springs placed at both ends

Initial total Weight = 521.83 g

Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT

OMEGA slope = 0.99

Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr

Vacuum limit up after 200A: 3.0e-05 Torr -- 5.0e-05 Torr

No Ta heat-shields used

Initial IGP1 = 4.1e-07 Torr

Wednesday, April 26, 2023, 09:49

Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min

Wednesday, April 26, 2023, 12:50

Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done.

Wednesday, April 26, 2023, 14:03

IGP1 = 6.0 e-05 Torr

TGHT = 200 A, 2.7V

TBHT = 200 A, 2.6 v

OMEGA = Below lower limit

Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT.

Wednesday, April 26, 2023, 14:13

IGPI= 4.2 e-05 Torr

starting ramping to 400 A on TGHT and 280A on TBHT 

Wednesday, April 26, 2023, 14:26

The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed

Wednesday, April 26, 2023, 14:42

pressure hovering around good vacuum so very slow progress.

Wednesday, April 26, 2023, 15:12

TGHT= 223 A, 3.1 V

TBHT = 226 A, 3.0 V

Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.

Darwin Ortiz Rosales wrote:

Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.

 Vacuum spike at 300A.

Currently:

TGHT= 316A, 4.6V

TBHT=283A, 3.9V

Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A

Carla Babcock wrote:

Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A

 Wednesday, April 26, 2023, 22:12

TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight.

Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview. 

TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.   

John Wong wrote:

Carla Babcock wrote: Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A  Wednesday, April 26, 2023, 22:12 TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight. Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview.  TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.

 Thursday, April 27, 2023, 06:27

IGP1= 1.7e-06 Torr

OMEGA= 1097 C

TGHT= 400A, 6.2V

TBHT= 273A, 3.7 V

Starting ramp up of TGHT @0.2A/min set to 550A

Darwin Ortiz Rosales wrote:

John Wong wrote: Carla Babcock wrote: Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A  Wednesday, April 26, 2023, 22:12 TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight. Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview.  TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.         Thursday, April 27, 2023, 06:27 IGP1= 1.7e-06 Torr OMEGA= 1097 C TGHT= 400A, 6.2V TBHT= 273A, 3.7 V Starting ramp up of TGHT @0.2A/min set to 550A

 Reached 550A on TGHT (paused there until I realized it was stopped) then resumed ramping to 580A at 0.2A/min. Saw both vacuum spikes before 550A. Attaching screenshot from John.

Darwin Ortiz Rosales wrote:

John Wong wrote: Carla Babcock wrote: Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A  Wednesday, April 26, 2023, 22:12 TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight. Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview.  TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.         Thursday, April 27, 2023, 06:27 IGP1= 1.7e-06 Torr OMEGA= 1097 C TGHT= 400A, 6.2V TBHT= 273A, 3.7 V Starting ramp up of TGHT @0.2A/min set to 550A

 Thursday, April 27, 2023, 22:04

TGHT has reached 580A/10.33V. Temp = 1540C. 

The two out-gassing peaks were observed: 1st peak around 1300C and 2nd peak 1370C.  See attachments 1 & 2.

A few minutes after TGHT reached to 580A, there was a small jump in TGHT current/voltage and also the pressure, but didn't notice any change in the temp, see attachment 3&4. 

Pressure is currently at 3.4e-6 Torr; will hold TGHT until pressure reaches close to 1e-6 Torr before cooling down. 

 Friday, April 28, 2023, 01:06

Pressure has reached 1.8 e-6 Torr; TGHT has been holding at 580A for 3.5 hrs, a slight increase in voltage, reading at 10.45V and temperature, 1548C.  See attachment #5 for overview.

Initiating auto-cooling TGHT at -2A/min, TBHT at -1A/min.

John Wong wrote:

Darwin Ortiz Rosales wrote: John Wong wrote: Carla Babcock wrote: Darwin Ortiz Rosales wrote: Wednesday, April 26, 2023, 09:32 LP FEBIAD loaded with 367 TiC discs and 4 TiC removable discs for analyses 50 packs of 5 and the rest are singles TaC coated (sintered) springs placed at both ends Initial total Weight = 521.83 g Initial heating @ 1A/min to 400 A on TGHT and 280A on TBHT OMEGA slope = 0.99 Vacuum limits up to 200A:  3.0e-05 Torr -- 5.0e-04 Torr Vacuum limit up after 200A: 3.0e-05 Torr -- 5.5e-05 Torr No Ta heat-shields used Initial IGP1 = 4.1e-07 Torr Wednesday, April 26, 2023, 09:49 Starting initial ramp up to 200A on both TGHT and TBHT @ 1A/min Wednesday, April 26, 2023, 12:50 Around 120A on TGHT, the pressure started to slowly drop.  First outgassing done. Wednesday, April 26, 2023, 14:03 IGP1 = 6.0 e-05 Torr TGHT = 200 A, 2.7V TBHT = 200 A, 2.6 v OMEGA = Below lower limit Waiting for pressure to fall below 5e0-5 Torr.  Will change bad vacuum to 5.0e-05 Torr and then continue ramping @1A/min to 400 A on TGHT and 280 A on TBHT. Wednesday, April 26, 2023, 14:13 IGPI= 4.2 e-05 Torr starting ramping to 400 A on TGHT and 280A on TBHT  Wednesday, April 26, 2023, 14:26 The IGP1 pressure just fell below 3.0e-05 Torr and ramping has resumed Wednesday, April 26, 2023, 14:42 pressure hovering around good vacuum so very slow progress. Wednesday, April 26, 2023, 15:12 TGHT= 223 A, 3.1 V TBHT = 226 A, 3.0 V Set ramp rate is 1A/min but real rate is slightly less than 0.5A/min due to pressure fluctuation.  Vacuum spike at 300A. Currently: TGHT= 316A, 4.6V TBHT=283A, 3.9V Wednesday, April 26, 2023, 18:18 Ramping TBHT down from 280A to 270A  Wednesday, April 26, 2023, 22:12 TGHT = 400A, 6.1V; TBHT = 274A/3.7V. Temp is holding sturdy ~1100 C and will leave it overnight. Pressure is coming down, currently at 8.8 e-6 Torr.  See attachment for the overview.  TGHT will continue to ramp up tomorrow morning; check the pressure to ensure it has come down below 5e-6 Torr before proceeding.  Refer to the instructions for details.         Thursday, April 27, 2023, 06:27 IGP1= 1.7e-06 Torr OMEGA= 1097 C TGHT= 400A, 6.2V TBHT= 273A, 3.7 V Starting ramp up of TGHT @0.2A/min set to 550A  Thursday, April 27, 2023, 22:04 TGHT has reached 580A/10.33V. Temp = 1540C.  The two out-gassing peaks were observed: 1st peak around 1300C and 2nd peak 1370C.  See attachments 1 & 2. A few minutes after TGHT reached to 580A, there was a small jump in TGHT current/voltage and also the pressure, but didn't notice any change in the temp, see attachment 3&4.  Pressure is currently at 3.4e-6 Torr; will hold TGHT until pressure reaches close to 1e-6 Torr before cooling down.   Friday, April 28, 2023, 01:06 Pressure has reached 1.8 e-6 Torr; TGHT has been holding at 580A for 3.5 hrs, a slight increase in voltage, reading at 10.45V and temperature, 1548C.  See attachment #5 for overview. Initiating auto-cooling TGHT at -2A/min, TBHT at -1A/min.

 Friday, April 28, 2023, 09:27

IGP1= 1.20e-07 Torr

Will dismount target around 10:15 am

Heating curve below.  Non-linear behavior

 Final weight = 517.08 g

Target looks good see attached picture

Wednesday, February 07, 2024, 22:36

Ta container tube TaC coated, wrapped in 4 Ta foil heat-shields, and loaded with 320 D shaped discs in a 12mm graphite cartridge with usable 11mm

Endcaps on the graphite cartridge have holes for outgassing

initial heating @ 2A/min to 90 A then 1A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Thursday, February 08, 2024, 06:18

Starting heat ramp tght

initial pressure = 8.1e-07 Torr IGP1

Thursday, February 08, 2024, 06:54

start of gasoff observed. paused ramp and will continue at 1A/min

Thursday, February 08, 2024, 07:24

lowered TGHT current to 75 A as pressure increasing too rapidly.  will leave at this current until pressure drops

Thursday, February 08, 2024, 09:11

continuing ramp to 120A on TGHT

Thursday, February 08, 2024, 09:24

Increasing ramp to 2A/min to 250A on TGHT

Thursday, February 08, 2024, 10:52

Increased ramp to 3A/min to 250A on TGHT

Thursday, February 08, 2024, 11:10

Everything looks good will continue to 300 A at 3A/min TGHT

Thursday, February 08, 2024, 11:33

Pausing heating at 285A, 4.8V TGHT

OMEGA reads 1430C

Will let pressure drop and then proceed ramping slowly @ 0.2A/min

Thursday, February 08, 2024, 13:53

IGP1= 2.4e-06 Torr

OMEGA = 1432 C

ramp at 0.2A/min towards 1550C

Thursday, February 08, 2024, 14:07

pressure very stable.  will increase to 0.4 A/min

Thursday, February 08, 2024, 15:24

increasing ramp rate to 1A/min

IGP1 = 2.5e-06 Torr

Thursday, February 08, 2024, 18:05

1900 C on OMEGA

will leave 3-4 hours depending on pressure

Thursday, February 08, 2024, 21:10

No additional pressure peaks observed and pressure on IGP1=  1.9e-06 Torr

TGHT= 460 A, 8.1V

OMEGA= 1860 C

ramp down at -2A/min

Wednesday, February 21, 2024, 06:22

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with 201 D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 90 A then 1A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Wednesday, February 21, 2024, 09:12

IGP1 initial = 9e-07 Torr

Starte at 3A/min to 90A

Wednesday, February 21, 2024, 09:21

increased autoramp to 4 A/min until pressure starts rising, then will slow down or pause

Wednesday, February 21, 2024, 09:32

At 74A, paused.  Will continue at 2A/min TGHT

Wednesday, February 21, 2024, 09:40

Pausing at 87A. 

Wednesday, February 21, 2024, 10:34

pressure dropping.  restarting ramp up to 120A at 2A/min

Wednesday, February 21, 2024, 10:37

From previous TiC 220206, will heat up fast until 250A and then at 1A/min until 300A to better resolve out-gassing profile

Wednesday, February 21, 2024, 12:05

Changed ramp to 1A/min to 300A

Wednesday, February 21, 2024, 13:10

Manually ramped up for a while

increased ramp speed to 2A/min

regression line started to match previous one after 1300C

Wednesday, February 21, 2024, 13:16

increased ramp rate to 4A/min to 420A

Wednesday, February 21, 2024, 13:37

Note: the temperature became unrealistic.  suspect window condensate.  Will use regression and to to 441A

Wednesday, February 21, 2024, 13:54

reached 441A, 7.6V

leaving for 3.5 hours or when pressure drops to 2-3 e-06 Torr

Wednesday, February 21, 2024, 18:56

IGP1=2.9e-06 Torr

starting rampdown at -2A/min

Thursday, February 29, 2024, 07:40

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with _________ D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Thursday, February 29, 2024, 07:43

Initial IGP1=  9.31e-7 Torr

Thursday, February 29, 2024, 17:43

Temperature profile suggests 1900 C at 400A.  Now at 400A.  Will keep at this current for 4 hours.

manually ramped the last few amps.

TGHT= 400A, 7.3 V OMEGA = 1901C

Thursday, February 29, 2024, 22:20

IGP1=2.1e-6 Torr

started ramping down at -2A/min

Wednesday, April 03, 2024, 06:46

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with _________ D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Wednesday, April 03, 2024, 06:49

initial IGP1= 1.28e-06 Torr

Wednesday, April 03, 2024, 09:26

IGP1= 2.3e-05 Torr

TGHT = 78 A, 1.3V

Will continue ramp as planned.

Wednesday, April 03, 2024, 11:37

Ramping at 2A./min to 400A

Wednesday, April 03, 2024, 14:01

expected 1900C at 401A

leaving at 402A for 4 hours.  Rampdown start at 4:10 pm at -2A/min

Thursday, April 04, 2024, 12:06

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with _________ D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13 (4th conditioning with this tube)

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Mas current~400A (1900 C)

Friday, April 05, 2024, 09:04  

Ramping to 85A done and pressure trending down.  Will continue ramp to 120A

Friday, April 05, 2024, 16:01

Starting rampdown at -2A/min

IGP1= 3.2e-06 Torr

Wednesday, October 02, 2024, 19:21

Ta endcup at front end of container

End-caps on the graphite cartridge have holes for outgassing. 

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT.  Allow pressure to drop and then ramp to 400 A at 2A/min, leave 4 hours and start ramp down.

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Max current~400A (1900 C)

Wednesday, October 02, 2024, 19:25

Starting IGP1 = 6.65e-06 Torr

Thursday, October 03, 2024, 05:09

Starting rampdown.  Pressure stable at 4.5 e-06 Torr

Top temperature 1850 C on OMEGA

ramping down at -2A/min

 Monday, September 24, 2012, 15:01

The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil.

Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not.

After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.

Nikita Bernier wrote:

Monday, September 24, 2012, 15:01 The target boat with TaC coating is being used again. The inside of the boat is covered with a 0.002 inches thick Ta foil with TaC coating, wrapped with a 0.002 inches thick Ta foil. Chamber was pumped down to 6e-6 Torr before the Heat Shield cooling water valve was opened. A small vacuum bump was detected (See attachment #1). It is not clear if it was caused by a water leak or not. After consulting with Peter, I will wait for the vacuum to be below e-07 Torr before turning the target heater on.

 Monday, September 24, 2012, 18:02

The vacuum was stable until 1e-06 Torr. The target heater was turned on and tapped up to 60 A (0.8 V). 

Evaporator #2 is now auto-ramping overnight at 0.2 A/min, up to 800-850 A, with the maximum voltage limited at 14 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). 

 Tuesday, September 25, 2012, 15:11

Sintering process is going smoothly. See Attachment 1. The auto-ramping was increased to 1 A/min up to 800-850 A.

Tuesday, September 25, 2012, 16:11 

And the voltage limit was increased to 18 V ! See Attachment 2.

 Tuesday, September 25, 2012, 19:13

Around 806 A (readback), voltage increased more quickly than the current. It seems like resistance is building up. After reaching 836 A (readback), the current was tapped down to 800 A (readback)/ 816 A (setting) in an effort to save the Ta boat. See Attachment 3. The current will stay at 800 A for ~4 hours before ramping down.