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Message ID: 678     Entry time: Wednesday, October 02, 2024, 19:24
Author: Darwin Ortiz Rosales 
Target Material: TiC 
Target Oven W.O#:  
Source: LP TUBE 
Status: Done 
Subject: sintering TiC Experiment  

Wednesday, October 02, 2024, 19:21

Ta endcup at front end of container

End-caps on the graphite cartridge have holes for outgassing. 

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT.  Allow pressure to drop and then ramp to 400 A at 2A/min, leave 4 hours and start ramp down.

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Max current~400A (1900 C)

 


Wednesday, October 02, 2024, 19:25

Starting IGP1 = 6.65e-06 Torr


Thursday, October 03, 2024, 05:09

Starting rampdown.  Pressure stable at 4.5 e-06 Torr

Top temperature 1850 C on OMEGA

ramping down at -2A/min

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