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Message ID: 658     Entry time: Thursday, April 04, 2024, 12:07
Author: Darwin Ortiz Rosales 
Target Material: TiC 
Target Oven W.O#:  
Source: LP TUBE 
Status: Done 
Subject: 240404TiC sintering/conditioning 

Thursday, April 04, 2024, 12:06

Ta container tube, wrapped in 4 Ta foil heat-shields, and loaded with _________ D shaped discs in a 12mm graphite cartridge with usable 11mm

conditioning tube WO = 44692-13 (4th conditioning with this tube)

End-caps on the graphite cartridge have holes for outgassing.  One spring each end in the Ta container

initial heating @ 2A/min to 85 A then 2A/min to 120A TGHT

OMEGA slope = 0.99

Vacuum limits up to 400A: 5.0e-04 Torr -- 1.0e-02 Torr

Mas current~400A (1900 C)

 


Friday, April 05, 2024, 09:04  

Ramping to 85A done and pressure trending down.  Will continue ramp to 120A


Friday, April 05, 2024, 16:01

Starting rampdown at -2A/min

IGP1= 3.2e-06 Torr

 

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