Friday, January 31, 2014, 12:10, Laura Lambert, Empty, 39165-10, LP-SIS, Done, Sintering TaC coating container for Ta?
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Friday, January 31, 2014, 11:28
Target container is coated with TaC.
The container is wrapped with 3 x Ta heat-shield.
Chamber was pumped down to 1.9e-7 Torr.
HS water valves were opened, no leak detected.
TGHT and TBHT were stepped up to 35A. Waited ~20min, current stabilized and vacuum starting to drop.
TGHT will be ramped up to 580A at 0.2A/min, max voltage = 11.05V.
TBHT will be ramped up to 230A at 0.2A/min, max volatge = 5V.
Initiating auto-ramping: Good Vac = 3.0e-5 Torr, Bad Vac = 4.0e-5 Torr.
Monday, February 03, 2014, 10:21
TGHT reached 580A pver the weekend.
TBHT sitting at 1.4A, checked archive: never went over 1.6A. Aborted auto-ramp, re-starting auto ramp process for TBHT.
IGP1 = 1.6e-7 Torr.
Monday, February 03, 2014, 15:23
TBHT running smoothly, must have been and electrical problem.
TBHT currently at 85A, vacuum has not changed, increasing TBHT auto-ramp to 2.0A/min
Tuesday, February 04, 2014, 10:10
TBHT reached 230A yesterday pm. Measured temp this morning at 1800C.
Initiated TGHT/TBHT auto-cooling at 2.0A/min.
Wednesday, February 05, 2014, 11:33
Chamber cooled down overnight, vented and opened up this morning.
Smooth run! Container fully sintered.

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Thursday, April 09, 2015, 09:38, Laura Lambert, Empty, 38817-7, HP-SIS, Done, Sintering TaC coating container for SiC#32
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Thursday, April 09, 2015, 09:33
Target container is coated with TaC and wrapped with 3-Ta heat shields, not incl center block.
TGHT and TBHT will be ramped up to 820A and 230A, respectively.
Chamber pumped down overnight.
IGP1 = 5.2e-7 Torr.
HS cooling water valves opened; no leaks detected.
TGHT max voltage = 18V, TBHT max voltage = 5V
Stepping TGHT and TBHT up to 35A...
Thursday, April 09, 2015, 10:07
Waited ~20min, vacuum stable.
IGP1 = 5.3e-7 Torr.
Good vac = 3e-5 Torr. Bad vac = 4e-5 Torr.
Auto-ramp initiated at 0.2A/min.
Monday, April 13, 2015, 09:06
Reached max setpoints sunday morning [see attached photo for striptool].
Internal temperature measured with OMEGA = 1965C
IGP1 = 4.4e-7 Torr,
Initiating auto cool for TGHT and TBHT at 2.0A/min and 1.0A/min respectively.
Tuesday, April 14, 2015, 14:12
Vented in air and opened up this morning.
Fully sintered.
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Tuesday, June 17, 2014, 13:20, Laura Lambert, Empty, 39530-8, HP-FEBIAD, Done, Sintering TaC coating container for SiC#30 part 2
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Tuesday, June 17, 2014, 13:11
Target container is coated with TaC.
Container is wrapped with 3x Ta-heat shields.
Currently being pumped down.
For sintering process:
TGHT and TBHT will be ramped up to 820A and 300A respectively at 0.1A/min
Tuesday, June 17, 2014, 14:22
HS water cooling valves opened, no leaks detected.
IGP1 @1.8e-6 Torr
TGHT max = 820A/ 17V
TBHT max = 300A/ 5V
Stepped up manually to 40A, waited ~20min, vacuum stable.
Initiating auto-ramp @ 1.0A/min
Wednesday, June 18, 2014, 11:24
TGHT and TBHT reached their respective 820A and 300A last night.
Internal temp measured from side of EVAP2 with mikron = 1830C
IGP1 = 7.6e-7 Torr
Initiating auto-cool down process at 2.0A/min and 1.0A/min for TGHT and TBHT respectively
vented and opened this morning.
smooth run 
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Wednesday, September 07, 2016, 15:02, John Wong, Empty, 39530-9, HP-SIS, In progress, Sintering TaC coating container for SiC Target  
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Wednesday, September 07, 2016, 14:45
Container was previously coated with TaC solution and wrapped with 1-full length layer of Ta- heat shield around the fins.
Chamber is being pumped down. Vac at 5.6e-7 Torr before HS water valves were open; no leaks were detected.
Sintering Temperature 1900C (Omega slope @ 0.98); expected TGHT ~765A/11.90V, TGHT max at 230A.
Thursday, September 08, 2016, 18:14
At about 1600C, it was observed that the coating inside the tube seems to chip off (see attachment 1).
TGHT was ramped up to 745A/11.85V and TBHT to 230A/3.25V. Temperature measured on OMEGA/Mikron = 1914C/1881C; both instruments slopes set at 0.98.
Will remain at this TGHT current over night
Vac at 3.0e-6 Torr and coming down.
Friday, September 09, 2016, 11:01
Target has been heated at the stable temperature at 1914C (for OMEGA) and 1881C (for Mikron) with current at 745A/11.94V (see attachment 2) for almost 19 hours.
No fluctuation in p/s current or temperature was observed. The ramping up process is captured and can be view from the link below:
https://www.dropbox.com/sh/9lgtin54o17ds6j/AABn1-XjvK44mm74TjqTAmvta?dl=0
Pressure at 1.07e-6 Torr.
Cooling down TGHT at 2A/min and TBHT at 1A/min.
Continue to capture the cooling down process.
Friday, September 09, 2016, 15:17
While the target container was cooling down, the chip-like particle began obvious (see attachment 3).
Will inspect the container.. TGHT currently at 260A.
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Tuesday, August 25, 2015, 11:54, Laura Lambert, Empty, , HP-FEBIAD, In progress, Sintering TaC coating container for SiC Target
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Tuesday, August 25, 2015, 11:50
Container coated with TaC using new method: Ends tapped off, with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'
Container is wrapped with 3 x Ta heat shields, not incl center block.
Loaded into EVAP2 and currently pumping down.
Tuesday, August 25, 2015, 13:52
IGP1 = 2.2e-6 Torr.
HS water valves opened.
No leaks detected.
Tapped up manually to 35A.
Vacuum stable.
Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Final setpoints for TGHT = 720A and TBHT = 230A, with final desired temp of 1800C
Wednesday, August 26, 2015, 09:56
IGP1 = 8.8e-7 Torr.
TGHT = 260A, 3.0V
TBHT = 145A, 1.8V
Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, August 26, 2015, 14:15
IGP1 = 3.5e-6 Torr.
TGHT = 720A, 11.3V
TBHT = 230A, 3.2V
DV = 5.48V
OMEGA RS [right side-old port] = 1745C
OMEGA LS [left side-new port] = 1880C
Tapping up manually to achieve 1800C on OMEGA RS
Wednesday, August 26, 2015, 14:44
IGP1 = 3.7e-6 Torr.
TGHT = 748A, 11.9V
DV = 5.78V
OMEGA RS = 1803C
OMEGA LS = 1935C
Thursday, August 27, 2015, 07:31
Remained at max setpoints for ~17hrs.
IGP1 = 1.3e-6 Torr.
DV = 5.79V
OMEGA RS = 1862 [this reading may not be correct due to the laser being moved at max setpoint - this temperature reading may be taken from a different location then the last reading]
OMEGA LS = 1955
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
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Thursday, August 27, 2015, 16:37, John Wong, Empty, , HP-FEBIAD, Done, Sintering TaC coating container for SiC Target
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Laura Lambert wrote: |
Tuesday, August 25, 2015, 11:50
Container coated with TaC using new method: Ends tapped off, with liquid poured in and swirled around entire container, then poured back out - 'flushing technique'
Container is wrapped with 3 x Ta heat shields, not incl center block.
Loaded into EVAP2 and currently pumping down.
Tuesday, August 25, 2015, 13:52
IGP1 = 2.2e-6 Torr.
HS water valves opened.
No leaks detected.
Tapped up manually to 35A.
Vacuum stable.
Initiated auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Final setpoints for TGHT = 720A and TBHT = 230A, with final desired temp of 1800C
Wednesday, August 26, 2015, 09:56
IGP1 = 8.8e-7 Torr.
TGHT = 260A, 3.0V
TBHT = 145A, 1.8V
Increasing ramping rate to 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Wednesday, August 26, 2015, 14:15
IGP1 = 3.5e-6 Torr.
TGHT = 720A, 11.3V
TBHT = 230A, 3.2V
DV = 5.48V
OMEGA RS [right side-old port] = 1745C
OMEGA LS [left side-new port] = 1880C
Tapping up manually to achieve 1800C on OMEGA RS
Wednesday, August 26, 2015, 14:44
IGP1 = 3.7e-6 Torr.
TGHT = 748A, 11.9V
DV = 5.78V
OMEGA RS = 1803C
OMEGA LS = 1935C
Thursday, August 27, 2015, 07:31
Remained at max setpoints for ~17hrs.
IGP1 = 1.3e-6 Torr.
DV = 5.79V
OMEGA RS = 1862 [this reading may not be correct due to the laser being moved at max setpoint - this temperature reading may be taken from a different location then the last reading]
OMEGA LS = 1955
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
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Thursday, August 27, 2015, 16:34
Target is removed from the evaporator and inspected.
The "flushing technique" has a much better result. The inner coated surface is sintered well.
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Thursday, January 16, 2014, 13:06, Laura Lambert, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container
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John Wong wrote: |
Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Thursday, January 16, 2014, 11:35
Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.
TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.
Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.

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Friday, January 17, 2014, 09:34, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container
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Laura Lambert wrote: |
John Wong wrote: |
Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Thursday, January 16, 2014, 11:35
Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.
TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.
Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.

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Friday, January 17, 2014, 09:28
TGHT/TBHT @ 300/200A. TBHT voltage is limited at 3A.
TGHT ramping rate increased to 2A/min. Pressure @ 4.5e-7 Torr.
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Friday, January 17, 2014, 12:52, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container
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Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Thursday, January 16, 2014, 11:35
Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.
TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.
Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.

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Friday, January 17, 2014, 09:28
TGHT/TBHT @ 300/200A. TBHT voltage is limited at 3A.
TGHT ramping rate increased to 2A/min. Pressure @ 4.5e-7 Torr.
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Friday, January 17, 2014, 10:14
TBHT stopped at 200A with voltage limit sitting at 3V.
Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.
IGP1 @ 5.0e-7 Torr

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Friday, January 17, 2014, 12:45
TGHT voltage limiting at 9.9V, and current stayed at 560A. Increased the TGHT voltage to 10.5V and continued ramping the heater up.
TGHT/TBHT stabilized at 580A (~10V) and 230A(3.6V).
Pressure at 1.03e-6 Torr and coming down...
Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min.
Chamber will be vented in air, next week.
Friday, January 17, 2014, 16:51
Auto-cooling initiated at 2A/min.
Vac @ 5.3e-7 Torr.
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Monday, January 20, 2014, 16:30, Laura Lambert, Empty, 39165-9, LP-SIS, Done, Sintering TaC coating container
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John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Thursday, January 16, 2014, 11:35
Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.
TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.
Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.

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Friday, January 17, 2014, 09:28
TGHT/TBHT @ 300/200A. TBHT voltage is limited at 3A.
TGHT ramping rate increased to 2A/min. Pressure @ 4.5e-7 Torr.
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Friday, January 17, 2014, 10:14
TBHT stopped at 200A with voltage limit sitting at 3V.
Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.
IGP1 @ 5.0e-7 Torr

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Friday, January 17, 2014, 12:45
TGHT voltage limiting at 9.9V, and current stayed at 560A. Increased the TGHT voltage to 10.5V and continued ramping the heater up.
TGHT/TBHT stabilized at 850A (~10V) and 230A(3.6V).
Pressure at 1.03e-6 Torr and coming down...
Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min.
Chamber will be vented in air, next week.
Friday, January 17, 2014, 16:51
Auto-cooling initiated at 2A/min.
Vac @ 5.3e-7 Torr.
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Wednesday, January 15, 2014, 17:45, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container
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Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Friday, January 17, 2014, 10:18, Laura Lambert, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container
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John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Wednesday, January 15, 2014, 17:30
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped. Tomorrow, the HS water valve can be opened to test for leaks.
Notes:
If everything is fine, TGHT/TBHT can be stepped up to 30A-50A. Watch for the vacuum; once it's stable the auto ramping program can be initiated.
Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min. (This step is to speed up the process; however it's not mandatory)
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Thursday, January 16, 2014, 11:35
Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.
TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.
Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.

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Friday, January 17, 2014, 09:28
TGHT/TBHT @ 300/200A. TBHT voltage is limited at 3A.
TGHT ramping rate increased to 2A/min. Pressure @ 4.5e-7 Torr.
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Friday, January 17, 2014, 10:14
TBHT stopped at 200A with voltage limit sitting at 3V.
Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.
IGP1 @ 5.0e-7 Torr

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Monday, June 29, 2015, 16:18, Laura Lambert, Empty, 41369-2, LP-SIS, In progress, Sintering TaC coating container
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Monday, June 29, 2015, 16:17
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 01A/min.
Chamber is currently being pumped down.
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Monday, June 29, 2015, 23:42, John Wong, Empty, 41369-2, LP-SIS, In progress, Sintering TaC coating container
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Laura Lambert wrote: |
Monday, June 29, 2015, 16:17
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 01A/min.
Chamber is currently being pumped down.
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Monday, June 29, 2015, 23:37
Opened the HS valves around 5pm. Small leaks or just a vibration in the pipe line caused a rise in vacuum. Leak rate is small, so allow the chamber to continue to pump down over night.
Sintering process can begin tomorrow if vacuum is allowed.
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Tuesday, June 30, 2015, 09:50, Laura Lambert, Empty, 41369-2, LP-SIS, In progress, Sintering TaC coating container   
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John Wong wrote: |
Laura Lambert wrote: |
Monday, June 29, 2015, 16:17
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 01A/min.
Chamber is currently being pumped down.
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Monday, June 29, 2015, 23:37
Opened the HS valves around 5pm. Small leaks or just a vibration in the pipe line caused a rise in vacuum. Leak rate is small, so allow the chamber to continue to pump down over night.
Sintering process can begin tomorrow if vacuum is allowed.
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Tuesday, June 30, 2015, 08:22
IGP1 = 3.6e-7 Torr.
Tapped up manually to 40A.
Vacuum looks good.
IGP1 = 6.9e-7 Torr.
Inititating auto-ramp...
Thursday, July 02, 2015, 09:56
IGP1 = 8.9e-7 Torr.
OMEGA = 1728C
TGHT and TBHT = 580A and 230A respectively.
Tapping up manually to 1800C.
Thursday, July 02, 2015, 11:02
TGHT = 615A, 10.9V
OMEGA = 1800C
IGP1 = 1.1e-6 Torr.
Will continue to heat for 4hrs.
Thursday, July 02, 2015, 15:43
Target container remained at 1800C for 4hrs50min.
Initiating auto-cool for TGHT = 2A/min and TBHT = 1A/min.
Friday, July 03, 2015, 08:24
Vented in air and opened up this morning.
Edge of container on both ends not fully sintered [see photos]
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Monday, July 06, 2015, 12:07, John Wong, Empty, 41369-2, LP-SIS, In progress, Sintering TaC coating container
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Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
Monday, June 29, 2015, 16:17
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 01A/min.
Chamber is currently being pumped down.
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Monday, June 29, 2015, 23:37
Opened the HS valves around 5pm. Small leaks or just a vibration in the pipe line caused a rise in vacuum. Leak rate is small, so allow the chamber to continue to pump down over night.
Sintering process can begin tomorrow if vacuum is allowed.
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Tuesday, June 30, 2015, 08:22
IGP1 = 3.6e-7 Torr.
Tapped up manually to 40A.
Vacuum looks good.
IGP1 = 6.9e-7 Torr.
Inititating auto-ramp...
Thursday, July 02, 2015, 09:56
IGP1 = 8.9e-7 Torr.
OMEGA = 1728C
TGHT and TBHT = 580A and 230A respectively.
Tapping up manually to 1800C.
Thursday, July 02, 2015, 11:02
TGHT = 615A, 10.9V
OMEGA = 1800C
IGP1 = 1.1e-6 Torr.
Will continue to heat for 4hrs.
Thursday, July 02, 2015, 15:43
Target container remained at 1800C for 4hrs50min.
Initiating auto-cool for TGHT = 2A/min and TBHT = 1A/min.
Friday, July 03, 2015, 08:24
Vented in air and opened up this morning.
Edge of container on both ends not fully sintered [see photos]
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Monday, July 06, 2015, 11:54
Inner tube surface isn't homogeneously sintered with TaC (see attachment).
A second coating may help.
For the re-sintering process, the target container will be wrapped with 6.2cm Ta (width) foil as a layer for heat shield on each side of the tube, excluding the centre block - just like the same process was done last time, see e-log ID#217.
The Ta-foil and the target tube will be spaced with Ta wire coiled around it.
TGHT can be ramped up about 520A/9.1V to achieve 1900C. Heating time for 3-4 hours until vacuum comes down to low 10-6 Torr.
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Monday, July 06, 2015, 16:30, Laura Lambert, Empty, 41369-2, LP-SIS, Done, Sintering TaC coating container   
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John Wong wrote: |
Laura Lambert wrote: |
John Wong wrote: |
Laura Lambert wrote: |
Monday, June 29, 2015, 16:17
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 01A/min.
Chamber is currently being pumped down.
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Monday, June 29, 2015, 23:37
Opened the HS valves around 5pm. Small leaks or just a vibration in the pipe line caused a rise in vacuum. Leak rate is small, so allow the chamber to continue to pump down over night.
Sintering process can begin tomorrow if vacuum is allowed.
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Tuesday, June 30, 2015, 08:22
IGP1 = 3.6e-7 Torr.
Tapped up manually to 40A.
Vacuum looks good.
IGP1 = 6.9e-7 Torr.
Inititating auto-ramp...
Thursday, July 02, 2015, 09:56
IGP1 = 8.9e-7 Torr.
OMEGA = 1728C
TGHT and TBHT = 580A and 230A respectively.
Tapping up manually to 1800C.
Thursday, July 02, 2015, 11:02
TGHT = 615A, 10.9V
OMEGA = 1800C
IGP1 = 1.1e-6 Torr.
Will continue to heat for 4hrs.
Thursday, July 02, 2015, 15:43
Target container remained at 1800C for 4hrs50min.
Initiating auto-cool for TGHT = 2A/min and TBHT = 1A/min.
Friday, July 03, 2015, 08:24
Vented in air and opened up this morning.
Edge of container on both ends not fully sintered [see photos]
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Monday, July 06, 2015, 11:54
Inner tube surface isn't homogeneously sintered with TaC (see attachment).
A second coating may help.
For the re-sintering process, the target container will be wrapped with 6.2cm Ta (width) foil as a layer for heat shield on each side of the tube, excluding the centre block - just like the same process was done last time, see e-log ID#217.
The Ta-foil and the target tube will be spaced with Ta wire coiled around it.
TGHT can be ramped up about 520A/9.1V to achieve 1900C. Heating time for 3-4 hours until vacuum comes down to low 10-6 Torr.
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Monday, July 06, 2015, 16:28
Container has been re-coated with TaC.
Target container is wrapped with a single 15.5cm x 8.5cm Ta foil heat shield on each side of the center block, spaced with Ta wire coil.
Chamber is currently being pumped down.
Tuesday, July 07, 2015, 09:36
HS water valves were opened this morning, no leaks detected.
IGP1 = 6e-7 Torr.
Tapped up manually to 30A.
Waited ~1hr.
Vacuum stable, IGP1 = 1.9e-6 Torr.
Initiating auto-ramp at 0.2A/min and 0.1A/min for TGHT and TBHT respectively.
Target container reached max setpoints of 520A/230A and 1950C ~6hrs ago.
IGP1 = 7.6e-7 Torr.
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Friday, July 10, 2015, 11:16
Vented in air and removed from evap2.
Again, edges not fully sintered [see photos]
Inside of container looks better, fully coated.
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Wednesday, July 23, 2014, 15:07, John Wong, Empty, 40282-3, LP-SIS, In progress, Sintering TaC coated target container
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Wednesday, July 23, 2014, 15:07
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped down
Wednesday, July 23, 2014, 17:40
Vacuum came down to mid 10-6 Torr.
Stepped up TGHT and TBHT to 30A - IG1 @ 1.4e-5 Torr.
Initiated auto-ramping.
Thursday, July 24, 2014, 17:19
TGHT and TBHT have reached to 100A, and vacuum is coming down to 1.4e-6 Torr.
Increase ramping rate, TGHT to 1A/min, TBHT 0.5A/min.
Friday, July 25, 2014, 11:26
Target container temperature reaches ~1550C at 580A on TGHT and 230A TBHT, and it has been heated for ~10 hrs.
Auto-cooling initiated at 2A/min.
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Monday, July 28, 2014, 10:52, Laura Lambert, Empty, 40282-3, LP-SIS, Done, Sintering TaC coated target container
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John Wong wrote: |
Wednesday, July 23, 2014, 15:07
Target container is coated with TaC. No Ta-heat shields are used.
TGHT will be ramped up to 580A at 0.2A/min.
TBHT will be ramped up to 230A at 0.2A/min.
Chamber is currently being pumped down
Wednesday, July 23, 2014, 17:40
Vacuum came down to mid 10-6 Torr.
Stepped up TGHT and TBHT to 30A - IG1 @ 1.4e-5 Torr.
Initiated auto-ramping.
Thursday, July 24, 2014, 17:19
TGHT and TBHT have reached to 100A, and vacuum is coming down to 1.4e-6 Torr.
Increase ramping rate, TGHT to 1A/min, TBHT 0.5A/min.
Friday, July 25, 2014, 11:26
Target container temperature reaches ~1550C at 580A on TGHT and 230A TBHT, and it has been heated for ~10 hrs.
Auto-cooling initiated at 2A/min.
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Monday, July 28, 2014, 10:50
vented in air and opened this morning. successful run 
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Tuesday, July 17, 2012, 16:00, John Wong, , targetboat (TaC coated), , Done, Sintering TaC coated regular- & D-endcaps
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Tuesday, July 17, 2012, 15:45
Target boat is filled with TaC coated regular- and D-endcaps.
The boat is wrapped with a Ta heat-shield.
Chamber is being pumped down, currently at 5e-6 Torr.
Tuesday, July 17, 2012, 15:58
Heat-shield cooling water valve opened; no leaks detected.
Initiated TGHT auto-ramping at 0.5A/min, set TGHT max at 580A.
Wednesday, July 18, 2012, 10:44
Yesterday evening, the target heater tripped off a few times due to high vacuum excursion. The TGHT ramping rate was low to 0.2A/min. The current was ramped up sturdily to 500A this morning.
Wednesday, July 18, 2012, 10:46
Increased ramping rate to 2A/min. Vacuum currently at 2.2e-6 Torr.
Wednesday, July 18, 2012, 16:18
TGHt has reached to 580A and stayed for about 5 hrs.
Cooling down in process... 2A/min for TGHT --> 0A.
Thursday, July 19, 2012, 10:31
TGHT reached to 0A.
Evaporator is off.
Venting chamber...
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