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Entry  Wednesday, January 15, 2014, 17:45, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container 
    Reply  Thursday, January 16, 2014, 13:06, Laura Lambert, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container  
       Reply  Friday, January 17, 2014, 09:34, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container  
          Reply  Friday, January 17, 2014, 10:18, Laura Lambert, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container 
             Reply  Friday, January 17, 2014, 12:52, John Wong, Empty, 39165-9, LP-SIS, In progress, Sintering TaC coating container  
                Reply  Monday, January 20, 2014, 16:30, Laura Lambert, Empty, 39165-9, LP-SIS, Done, Sintering TaC coating container  
Message ID: 101     Entry time: Friday, January 17, 2014, 12:52     In reply to: 100     Reply to this: 102
Author: John Wong 
Target Material: Empty 
Target Oven W.O#: 39165-9 
Source: LP-SIS 
Status: In progress 
Subject: Sintering TaC coating container  

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

John Wong wrote:

 Wednesday, January 15, 2014, 17:30

Target container is coated with TaC.  No Ta-heat shields are used.

TGHT will be ramped up to 580A at 0.2A/min. 

TBHT will be ramped up to 230A at 0.2A/min.  

 Chamber is currently being pumped.  Tomorrow, the HS water valve can be opened to test for leaks.  

Notes: 

If everything is fine, TGHT/TBHT can be stepped up to 30A-50A.  Watch for the vacuum; once it's stable the auto ramping program can be initiated.  

Once TGHT/TBHT reached above 200A, the ramping rate for TGHT can be increased up to 2A/min.  (This step is to speed up the process; however it's not mandatory) 


 

 Thursday, January 16, 2014, 11:35

Chamber was pumped down overnight to 10-7 Torr. HS water valve was opened and no leak in vacuum was observed.

TGHT and TBHT were stepped up to 35A. Waited ~30min, current stabilized and vacuum starting to drop.

Initiating auto-ramping: Good Vac = 2.0e-5 Torr, Bad Vac = 3.0e-5 Torr.


 

 Friday, January 17, 2014, 09:28

TGHT/TBHT @ 300/200A.  TBHT voltage is limited at 3A.  

TGHT ramping rate increased to 2A/min.  Pressure @ 4.5e-7 Torr.  


 

 Friday, January 17, 2014, 10:14

TBHT stopped at 200A with voltage limit sitting at 3V.

Aborted auto-ramp, changed the voltage limit to 5V and increased ramping rate to 2A/min. Re-started auto-ramp.

IGP1 @ 5.0e-7 Torr

 Friday, January 17, 2014, 12:45

TGHT voltage limiting at 9.9V, and  current stayed at 560A.  Increased the TGHT voltage to 10.5V and continued ramping the heater up.

TGHT/TBHT stabilized at 580A (~10V) and 230A(3.6V). 

Pressure at 1.03e-6 Torr and coming down... 

Target will be heated until 5pm (4hrs) before cooling down at the ramping rate of 2A/min. 

Chamber will be vented in air, next week.


 Friday, January 17, 2014, 16:51

Auto-cooling initiated at 2A/min.

Vac @ 5.3e-7 Torr.


 

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