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Message ID: 185     Entry time: Thursday, April 09, 2015, 09:38
Author: Laura Lambert 
Target Material: Empty 
Target Oven W.O#: 38817-7 
Source: HP-SIS 
Status: Done 
Subject: Sintering TaC coating container for SiC#32 

 Thursday, April 09, 2015, 09:33

Target container is coated with TaC and wrapped with 3-Ta heat shields, not incl center block.

TGHT and TBHT will be ramped up to 820A and 230A, respectively.

Chamber pumped down overnight.

IGP1 = 5.2e-7 Torr.

HS cooling water valves opened; no leaks detected.

TGHT max voltage = 18V, TBHT max voltage = 5V

Stepping TGHT and TBHT up to 35A...


 Thursday, April 09, 2015, 10:07

Waited ~20min, vacuum stable.

IGP1 = 5.3e-7 Torr.

Good vac = 3e-5 Torr. Bad vac = 4e-5 Torr.

Auto-ramp initiated at 0.2A/min.


 Monday, April 13, 2015, 09:06

Reached max setpoints sunday morning [see attached photo for striptool].

Internal temperature measured with OMEGA  = 1965C

IGP1 = 4.4e-7 Torr,

Initiating auto cool for TGHT and TBHT at 2.0A/min and 1.0A/min respectively.


 Tuesday, April 14, 2015, 14:12

Vented in air and opened up this morning.

Fully sintered.


 

Attachment 1: sintering_TaC_coating_for_container.JPG  104 kB  Uploaded Monday, April 13, 2015, 11:18  | Show | Hide all
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