Wednesday, September 07, 2016, 14:45
Container was previously coated with TaC solution and wrapped with 1-full length layer of Ta- heat shield around the fins.
Chamber is being pumped down. Vac at 5.6e-7 Torr before HS water valves were open; no leaks were detected.
Sintering Temperature 1900C (Omega slope @ 0.98); expected TGHT ~765A/11.90V, TGHT max at 230A.
Thursday, September 08, 2016, 18:14
At about 1600C, it was observed that the coating inside the tube seems to chip off (see attachment 1).
TGHT was ramped up to 745A/11.85V and TBHT to 230A/3.25V. Temperature measured on OMEGA/Mikron = 1914C/1881C; both instruments slopes set at 0.98.
Will remain at this TGHT current over night
Vac at 3.0e-6 Torr and coming down.
Friday, September 09, 2016, 11:01
Target has been heated at the stable temperature at 1914C (for OMEGA) and 1881C (for Mikron) with current at 745A/11.94V (see attachment 2) for almost 19 hours.
No fluctuation in p/s current or temperature was observed. The ramping up process is captured and can be view from the link below:
https://www.dropbox.com/sh/9lgtin54o17ds6j/AABn1-XjvK44mm74TjqTAmvta?dl=0
Pressure at 1.07e-6 Torr.
Cooling down TGHT at 2A/min and TBHT at 1A/min.
Continue to capture the cooling down process.
Friday, September 09, 2016, 15:17
While the target container was cooling down, the chip-like particle began obvious (see attachment 3).
Will inspect the container.. TGHT currently at 260A.
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