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Entry  Wednesday, September 07, 2016, 15:02, John Wong, Empty, 39530-9, HP-SIS, In progress, Sintering TaC coating container for SiC Target  coating_chipped_off.JPGautoTaC_sintering_20.JPEGcoating_chipped_off_2.JPG
    Reply  Monday, September 12, 2016, 17:22, John Wong, Empty, 39530-9, HP-SIS, Failed, TaC coating chipped off Screen_Shot_2016-09-12_at_4.52.53_PM.png
       Reply  Monday, September 12, 2016, 17:27, John Wong, Empty, 39530-9, HP-SIS, Done, RUSH. Round 2: Sinering TaC coating  Screen_Shot_2016-09-14_at_5.05.08_PM.pngScreen_Shot_2016-09-14_at_5.03.48_PM.png
Message ID: 319     Entry time: Wednesday, September 07, 2016, 15:02     Reply to this: 320
Author: John Wong 
Target Material: Empty 
Target Oven W.O#: 39530-9 
Source: HP-SIS 
Status: In progress 
Subject: Sintering TaC coating container for SiC Target  

 Wednesday, September 07, 2016, 14:45

Container was previously coated with TaC solution and wrapped with 1-full length layer of Ta- heat shield around the fins.  

Chamber is being pumped down.  Vac at 5.6e-7 Torr before HS water valves were open; no leaks were detected. 

Sintering Temperature 1900C (Omega slope @ 0.98); expected TGHT ~765A/11.90V, TGHT max at 230A.


 Thursday, September 08, 2016, 18:14

At about 1600C, it was observed that the coating inside the tube seems to chip off (see attachment 1).

TGHT was ramped up to 745A/11.85V and TBHT to 230A/3.25V.  Temperature measured on OMEGA/Mikron = 1914C/1881C; both instruments slopes set at 0.98.

Will remain at this TGHT current over night

Vac at 3.0e-6 Torr and coming down.


Friday, September 09, 2016, 11:01 

Target has been heated at the stable temperature at 1914C (for OMEGA) and 1881C (for Mikron) with current at 745A/11.94V (see attachment 2) for almost 19 hours. 

No fluctuation in p/s current or temperature was observed.  The ramping up process is captured and can be view from the link below:

https://www.dropbox.com/sh/9lgtin54o17ds6j/AABn1-XjvK44mm74TjqTAmvta?dl=0

Pressure at 1.07e-6 Torr. 

Cooling down TGHT at 2A/min and TBHT at 1A/min. 

Continue to capture the cooling down process. 


 Friday, September 09, 2016, 15:17

 While the target container was cooling down, the chip-like particle began obvious (see attachment 3).  

Will inspect the container.. TGHT currently at 260A.


 

Attachment 1: coating_chipped_off.JPG  17 kB  Uploaded Friday, September 09, 2016, 12:08  | Show | Hide all
Attachment 2: autoTaC_sintering_20.JPEG  259 kB  Uploaded Friday, September 09, 2016, 12:13  | Show | Hide all
Attachment 3: coating_chipped_off_2.JPG  92 kB  Uploaded Friday, September 09, 2016, 16:19  | Show | Hide all
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