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ID |
Date |
Author |
Target Material |
Target Oven W.O# |
Source |
Status |
Subject |
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115
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Tuesday, January 28, 2014, 15:46 |
Laura Lambert | | 40282-4 | TARGET BOAT | Failed | Sintering TaC coated end caps | Tuesday, January 28, 2014, 15:43
The target containers end-caps were coated with TaC spray and let dry.
Each cap is wrapped with a small piece of graphite foil and inserted in the target boat. [see attached photo]
The chamber is currently being pumped down overnight.
Wednesday, January 29, 2014, 11:32
Chamber was pumped down to 1.6e-7 Torr overnight.
HS cooling water valve opened; no leaks detected.
TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.
Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.
Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.
Thursday, January 30, 2014, 09:06
TGHT has been slowly ramping up overnight at a rate of 0.2A/min.
IGP1 = 2.4e-7 Torr, TGHT = 283A; stepping ramping rate up to 2.0A/min.
Thursday, January 30, 2014, 15:53
TGHT reached 580A at 11:45. Measured temp @1650C.
Initiating TGHT auto-cooling now at 2.0A/min.
Friday, January 31, 2014, 09:04
Chamber cooled down overnight, vented and opened this morning.
Smooth run!
Friday, January 31, 2014, 11:21
Opened up the end caps, turns out it wasn't such a smooth run...they're not fully sintered
See attached photo comparison between fully sintered end cap [silver] and end cap from this run [green].
Will re-install and re-sinter next week.
Wednesday, February 05, 2014, 11:34
End-caps re-installed into EVAP2
Target boat is wrapped with 3 x Ta heat-shield.
Chamber is currently being pumped down.
Wednesday, February 05, 2014, 14:31
Chamber was pumped down to 5e-7 Torr this morning.
HS cooling water valve opened, no leaks detected.
TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.
Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.
Good Vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.
Thursday, February 06, 2014, 09:06
TGHT has been slowly ramping up overnight at a rate of 0.2A/min.
IGP1 = 1.1e-7 Torr, TGHT = 259A; stepping ramping rate up to 2.0A/min.
Friday, February 07, 2014, 10:10
TGHT reached 580A yesterday. Measured internal temp @ 1500C.
Initiated TGHT auto-cooling this morning at 2.0A/min
Tuesday, February 11, 2014, 13:30
Vented and opened chamber this morning.
Endcaps are toast [see pictures attached]
Some of the endcaps broke/fried, others deformed-none useable.
Possibly due to new target boat resulting in more current?
Too much heat with Ta heat shields?
Bad News Bears
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Attachment 1: end_caps
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Attachment 2: IMG_20140131_101959838.jpg
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Attachment 3: feb11-2014(3).jpg
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Attachment 4: feb11-2014(2).jpg
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153
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Thursday, August 07, 2014, 10:13 |
Laura Lambert | | | TARGET BOAT | Failed | Sintering TaC coated end caps |
John Wong wrote: |
Laura Lambert wrote: |
Tuesday, August 05, 2014, 12:02
The target container end caps were coated with TaC spray and let dry.
The caps are inserted in the target boat vertically, wrapped in graphite foil with 3 x Ta-heat shield. [see attached photo]
The chamber is currently being pumped down.
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Tuesday, August 05, 2014, 17:19
HS water valve opened; no leaks detected.
Pressure @ 2.5e-6 Torr.
Ramping up TGHT to 580A @ 1A/min.
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Thursday, August 07, 2014, 08:11
Yesterday the target boat was taken out.
The boat broke as it turns out it was used for a Niobium target and therefore wasn't coated with TaC.
The end caps were fully sintered.
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155
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Thursday, September 11, 2014, 14:23 |
Laura Lambert | | 40282-3 | TARGET BOAT | Failed | Sintering TaC coated end caps | Thursday, September 11, 2014, 13:14
The target container end caps were coated with TaC spray and let dry.
The caps are inserted in the target boat wrapped in graphite foil with 3 x Ta-heat shields.
The chamber is currently pumping down.
Friday, September 12, 2014, 14:17
Chamber was pumped down overnight.
HS cooling water valves opened, no leaks detected.
IGP1 = 7.2e-7 Torr.
TGHT stepped up to 35A, TBHT at 0A.
Waited ~30min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min.
Will ramp TGHT to 580A with a max 10V.
Good vacuum: 3.00e-5 Torr; Bad vacuum: 4.00e-5 Torr.
Monday, September 15, 2014, 11:31
TGHT stopped at 500A due to not high enough voltage max.
Increased max voltage to 12V
Monday, September 15, 2014, 14:17
IGP1 = 6.3e-7 Torr
Increasing ramping rate to 1.0A/min
Tuesday, September 16, 2014, 09:04
TGHT reached 577A and finished auto-ramping, then proceeded to drop down to 560A overnight.
Increased max voltage to 13.05A and TGHT to 580A.
Tuesday, September 16, 2014, 13:52
TGHT reached 580A and sat there for ~5hrs.
IGP1 = 6.1e-7 Torr.
Initiating auto-cool at 2.0A/min.
Wednesday, September 17, 2014, 13:03
Vented in air.
Opened up....looked 'deceivingly' ok.
then i took a layer of Ta off....grrrr
the 1st layer of Ta was holding the boat together. as soon as that layer was taken off the target boat broke.
see attached photos.
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Attachment 1: IMG_20140917_142605683.jpg
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Attachment 2: IMG_20140917_143120141.jpg
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Attachment 3: IMG_20140917_143343399_HDR.jpg
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Attachment 4: Capture.JPG
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Attachment 5: Capture2.JPG
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320
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Monday, September 12, 2016, 17:22 |
John Wong | Empty | 39530-9 | HP-SIS | Failed | TaC coating chipped off |
John Wong wrote: |
Wednesday, September 07, 2016, 14:45
Container was previously coated with TaC solution and wrapped with 1-full length layer of Ta- heat shield around the fins.
Chamber is being pumped down. Vac at 5.6e-7 Torr before HS water valves were open; no leaks were detected.
Sintering Temperature 1900C (Omega slope @ 0.98); expected TGHT ~765A/11.90V, TGHT max at 230A.
Thursday, September 08, 2016, 18:14
At about 1600C, it was observed that the coating inside the tube seems to chip off (see attachment 1).
TGHT was ramped up to 745A/11.85V and TBHT to 230A/3.25V. Temperature measured on OMEGA/Mikron = 1914C/1881C; both instruments slopes set at 0.98.
Will remain at this TGHT current over night
Vac at 3.0e-6 Torr and coming down.
Friday, September 09, 2016, 11:01
Target has been heated at the stable temperature at 1914C (for OMEGA) and 1881C (for Mikron) with current at 745A/11.94V (see attachment 2) for almost 19 hours.
No fluctuation in p/s current or temperature was observed. The ramping up process is captured and can be view from the link below:
https://www.dropbox.com/sh/9lgtin54o17ds6j/AABn1-XjvK44mm74TjqTAmvta?dl=0
Pressure at 1.07e-6 Torr.
Cooling down TGHT at 2A/min and TBHT at 1A/min.
Continue to capture the cooling down process.
Friday, September 09, 2016, 15:17
While the target container was cooling down, the chip-like particle began obvious (see attachment 3).
Will inspect the container.. TGHT currently at 260A.
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Monday, September 12, 2016, 16:54
The TaC coating chipped off from the surface and didn't get sintered with the container. (See attachment1).
There are a few possible reasons why this happened:
1. The coating was too think. This may cause the TaC layer to curl up while the heater was ramped up.
2. The coated material got brittle. The container was flushed with TaC (probably a few weeks ago?) before it went through the sintering process. Prolong exposure to air/light usually degrade the polymers viscoelasticity.
3. TaC solution has got bad. The particles can agglomerate over time and this can cause uneven surface.
4. Combination of all... ???
Anyway, the chipped off TaC layer was gently scraped off with a stainless steel rod. Then using kimwipes, i was able to remove most of the chipped off coating; it was not easy - especially trying to remove it from the inner tube.
Instead of "flushing" the tube with TaC, I decided to spray it with thin layer. And using the air supply, I could quickly dry the coating and installed it back to the evaporator for 2nd Round sintering as we are approaching the deadline!
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Attachment 1: Screen_Shot_2016-09-12_at_4.52.53_PM.png
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3
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Monday, February 13, 2012, 16:24 |
John Wong | | | | Done | Evaporator #2 Commissioned | Monday, February 13, 2012, 16:21
The Evaporator 2 is now commissioned. See attachment#1 for the commissioning report or refer to Document #43321. |
Attachment 1: Evap2_Commissioning_Report.PDF
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4
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Tuesday, February 28, 2012, 11:00 |
John Wong | Empty | Test oven | LP-SIS | Done | Measuring temperatures, currents & voltages | Tuesday, February 28, 2012, 10:36
Two thermocouples were inserted through the left side of the copper heat shield, see attachment #1. One thermocouple is attached to the target tube with a Ta-wire, and the other is attached to the back block.
Data gathering:
1. Target heater (IEVAP2:TGHT) setpoint current/voltage
2. Target heater (IEVAP2:TGHT) readback current/voltage
4. Tube heater (IEVAP2:TBHT) setpoint current/voltage
3. Thermocouples voltages & controls' readback (IEVAP2:TCM)
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Attachment 1: Evap_2_thermocouple.jpg
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6
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Monday, March 19, 2012, 17:10 |
Nikita Bernier | BeO | Target boat #1 | | Done | Sintering BeO pellets | Monday, March 19, 2012, 17:04
Target boat contains 4 BeO pellets with 30% PVB:
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 4.943, 0.9628, 1.265
2 4.930, 0.9685, 1.276
3 4.758, 0.9607, 1.312
4 4.979, 0.9872, 1.288
Target chamber is currently being pumped down. Leak check will be done tomorrow by turning on the cooling water for the heat shield.
Wednesday, March 21, 2012, 18:30
The Evaporator #2 backing pump (IEVAP2BP1) muffler has been connected to the exhaust system.
The auto-ramp program has been tested today and works well.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 500 A, between 5.00e-05 and 6.00e-05 Torr.
ISAC ops have been informed of the process and they will include it in their walkaround. |
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7
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Tuesday, March 20, 2012, 14:35 |
John Wong | | | | Done | Evap#2 Backing up muffler not connected to the exhaust system. | Tuesday, March 20, 2012, 14:22
The Evaporator #2 backing pump (IEVAP2:BP1) muffler has not connected to the exhaust duct.
See attachment#1 as to where the muffler should be connected to the exhaust ducting system.
The Evaporator chamber is currently under vacuum; the BeO sintering process will be pending for now until the backing pump is properly installed.
(ISAC E-fault 5880)
Wednesday, March 21, 2012, 13:55
Edi Dalla Valle is connecting the evaporator backing scroll pump exhaust to the existing nuclear exhaust. (See attachment#2: scroll_pump_exhause.jpg). A filter is also added between the exhaust line
to prevent any back flow of oil from the Evaporator #1 backing pump (An oil pump).
Work is covered under ISAC WP# 2012-03-21-3.
The evaporator is now operational.
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Attachment 1: Evap2_backingpump.jpg
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Attachment 2: scroll_pump_exhaust.jpg
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8
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Tuesday, March 20, 2012, 14:39 |
John Wong | BeO | Target boat #1 | | Done | Sintering BeO pellets |
Nikita Bernier wrote: |
Monday, March 19, 2012, 17:04
Target boat contains 4 BeO pellets with 30% PVB:
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 4.943, 0.9628, 1.265
2 4.930, 0.9685, 1.276
3 4.758, 0.9607, 1.312
4 4.979, 0.9872, 1.288
Target chamber is currently being pumped down. Leak check will be done tomorrow by turning on the cooling water for the heat shield.
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Tuesday, March 20, 2012, 14:35
It was found out that the Evaporator #2 backing pump (IEVAP2BP1) muffler is not connected to the exhaust system. The sintering process is on hold until the pump is properly setup (see message ID#7 for more details).
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9
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Thursday, March 22, 2012, 00:34 |
John Wong | BeO | Target boat #1 | | Done | Sintering BeO pellets |
Nikita Bernier wrote: |
Monday, March 19, 2012, 17:04
Target boat contains 4 BeO pellets with 30% PVB:
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 4.943, 0.9628, 1.265
2 4.930, 0.9685, 1.276
3 4.758, 0.9607, 1.312
4 4.979, 0.9872, 1.288
Target chamber is currently being pumped down. Leak check will be done tomorrow by turning on the cooling water for the heat shield.
* Note: Target a boat is wrapped with a piece of Ta-foil as a heat shield - JW.
Wednesday, March 21, 2012, 18:30
The Evaporator #2 backing pump (IEVAP2BP1) muffler has been connected to the exhaust system.
The auto-ramp program has been tested today and works well.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 500 A, between 5.00e-05 and 6.00e-05 Torr.
ISAC ops have been informed of the process and they will include it in their walkaround.
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Thursday, March 22, 2012, 00:25
TGHT SETPOINT was ramped up to 266A but the actual p/s current remained at 90A; that was because the voltage was set 1.05V. (See attachment1: voltage_limiting.jpg).
Increased TGHT voltage to 20V, and increased the auto-ramping final value from 500A to 1000A (~1780C as previously measured by a pyrometer, see Attachment 2: Temp-Cal vs Measured.jgp)
Thursday, March 22, 2012, 10:17
TGHT ramped up at the rate of 1A/min to 534A/8.89V, local @ 525A/8.90V. Pressure is coming down to low 10e-6. (See attachment 3: TGHT_525A.jpg)
Increased ramping rate to 2A/min until TGHT reaches to 1000A.
Thursday, March 22, 2012, 13:32
A decision was made to stop the TGHT autoramping program, and set the current to 700A, (local at 690A). The temperature was measured to be around 1780C on the target boat, and
1500C on the Ta-heat shield. The current remained at that current for about 2 hours before it's ramping down at zero at -10A/min.
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Attachment 1: voltage_limiting.jpg
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Attachment 2: Temp_-_Cal_vs_Measured.JPG
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Attachment 3: TGHT_525A.JPG
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10
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Thursday, March 22, 2012, 17:56 |
Nikita Bernier | BeO | Target boat #1 | | Done | Sintering BeO pellets |
Nikita Bernier wrote: |
Monday, March 19, 2012, 17:04
Target boat contains 4 BeO pellets with 30% PVB:
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 4.943, 0.9628, 1.265
2 4.930, 0.9685, 1.276
3 4.758, 0.9607, 1.312
4 4.979, 0.9872, 1.288
Target chamber is currently being pumped down. Leak check will be done tomorrow by turning on the cooling water for the heat shield.
Wednesday, March 21, 2012, 18:30
The Evaporator #2 backing pump (IEVAP2BP1) muffler has been connected to the exhaust system.
The auto-ramp program has been tested today and works well.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 500 A, between 5.00e-05 and 6.00e-05 Torr.
ISAC ops have been informed of the process and they will include it in their walkaround.
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After sintering at up to 500 A (~1000°C), the 4 BeO pellets have shrunk and feel robust. We can manipulate them with tweesers or hands. Also we can drop them from a couple of inches high and they don't break.
One of the pellets rolled to the extremity of the target boat tube and still has black traces from bad sintering on one side.
Sample, Thickness (mm), Mass (g), Diameter (mm), Density (g/cm3)
1 3.688, 0.7118, 11.231, 1.948
2 3.822, 0.7196, 11.241, 1.897
3 3.810, 0.7037, 11.188, 1.879
4 3.803, 0.7077, 11.269, 1.866
The average thickness before sintering was 4.90 mm. After sintering, 3.78 mm. Thus the average thickness loss is 1.12 mm (22.9%)
The average mass before sintering was 0.9698 g. After sintering, 0.7107 g. Thus the average mass loss is 0.2591 g (26.7%)
The average diameter before sintering was 14.35 mm. After sintering, 11.23 mm. Thus the average diameter loss is 3.12 mm (21.7%)
The average density after sintering is 1.897 g/cm3, compared to the density of BeO (3.01 g/cm3). Thus the pellets have a BeO density of 63.0%.
Evaporator #2 is now off. |
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11
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Thursday, March 29, 2012, 19:30 |
Nikita Bernier | BeO | Target boat #1 | | Done | Sintering new BeO pellets | Thursday, March 29, 2012, 19:17
Target boat contains 3 BeO pellets :
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 9.06, 1.9713, 1.413
2 9.11, 1.9900, 1.419
3 13.54, 1.9916, 0.956
Samples 1 and 2 are made of BeO powder with 30% PVB which was washed with excess acetone and let to dry on a greased baking sheet (with PAM Butter flavoured). The flakes were then milled for 26 minutes at 400 RPM. It resulted in a very fine grey powder, much denser than the BeO powder with 30% PVB (not washed with acetone) that was used for Sample 3.
The initial settings on Evaporator #2 were 100 A and 0.83 V until the vacuum increased.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 700 A, with the maximum voltage limited at 14 V, between 5.00e-05 (Good vacuum) and 6.00e-05 Torr (Bad vacuum).
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12
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Thursday, March 29, 2012, 22:44 |
John Wong | BeO | Target boat #1 | | Done | Sintering new BeO pellets |
Nikita Bernier wrote: |
Thursday, March 29, 2012, 19:17
Target boat contains 3 BeO pellets :
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 9.06, 1.9713, 1.413
2 9.11, 1.9900, 1.416
3 13.54, 1.9916, 0.956
Samples 1 and 2 are made of BeO powder with 30% PVB which was washed with excess acetone and let to dry on a greased baking sheet (with PAM Butter flavoured). The flakes were then milled for 26 minutes at 400 RPM. It resulted in a very fine grey powder, much denser than the BeO powder with 30% PVB (not washed with acetone) that was used for Sample 3.
The initial settings on Evaporator #2 were 100 A and 0.83 V until the vacuum increased.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 700 A, with the maximum voltage limited at 14 V, between 5.00e-05 (Good vacuum) and 6.00e-05 Torr (Bad vacuum).
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Thursday, March 29, 2012, 22:31:
TGHT tripped off a few times over the past hours. After changing the Good Vac to 2.00e-5 torr and Bad Vac to 3.00e-5 Torr, the target heater are regulating properly and the max pressure is well maintained below 6.5e-5 Torr [Trip point @ 8.0e-5 Torr]. (see attachment#1: parameter.jpg) |
Attachment 1: Parameter.jpg
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13
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Friday, March 30, 2012, 23:21 |
John Wong | BeO | Target boat #1 | | Done | Sintering new BeO pellets |
John Wong wrote: |
Nikita Bernier wrote: |
Thursday, March 29, 2012, 19:17
Target boat contains 3 BeO pellets :
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 9.06, 1.9713, 1.413
2 9.11, 1.9900, 1.416
3 13.54, 1.9916, 0.956
Samples 1 and 2 are made of BeO powder with 30% PVB which was washed with excess acetone and let to dry on a greased baking sheet (with PAM Butter flavoured). The flakes were then milled for 26 minutes at 400 RPM. It resulted in a very fine grey powder, much denser than the BeO powder with 30% PVB (not washed with acetone) that was used for Sample 3.
The initial settings on Evaporator #2 were 100 A and 0.83 V until the vacuum increased.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 700 A, with the maximum voltage limited at 14 V, between 5.00e-05 (Good vacuum) and 6.00e-05 Torr (Bad vacuum).
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Thursday, March 29, 2012, 22:31:
TGHT tripped off a few times over the past hours. After changing the Good Vac to 2.00e-5 torr and Bad Vac to 3.00e-5 Torr, the target heater are regulating properly and the max pressure is well maintained below 6.5e-5 Torr [Trip point @ 8.0e-5 Torr]. (see attachment#1: parameter.jpg)
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Friday, March 30, 2012, 23:19
Archive of the target current and vacuum over the past 24 hours. (see attachment #1: archive_24hr)
Saturday, March 31, 2012, 12:12
The organic materials have been burnt off. The target heater ramping up is no longer restricted by the vacuum limit.
Archive of the target current and vacuum over the past 10 hours. (see attachment #2: TGHT@240A).
Saturday, March 31, 2012, 22:52
TGHT has stayed at 700A/12.37V, local @ 693A/12.43 = Temp @ 1780C.
The striptool shows some out-gassing when TGHT reached to 700A. (see attachment #3 marked with black circle: TGHT@700A.jpg)
Increasing TGHT to 750A to see if there is any further reaction...
Sunday, April 01, 2012, 10:24
TGHT was ramped up to 750A, local 730A/13.90V. The pressure has come down to low 10e-6 but not stable; Some reaction may be ongoing therefore it's causing the vacuum excursion. (See attachment #4: TGHT @ 750A). Notice the current readback is not constant and it's slowly decreasing as the voltage readback is increasing. There might be some resistant building up.
--> Initiating the cool-down process at 2A/min.
Sunday, April 01, 2012, 19:30
TGHT has ramped down to 0A, and the pressure is going down (currently at 7.e-8 Torr) with no excursion. (see attachment #5: TGHT@0A).
The chamber will be vented tomorrow, and the target materials will be inspected.
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Attachment 1: archive_24hr.jpg
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Attachment 2: TGHT@240A.jpg
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Attachment 3: TGHT@700A.jpg
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Attachment 4: TGHT@750A.jpg
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Attachment 5: TGHT@0A.jpg
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14
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Monday, April 02, 2012, 16:26 |
Nikita Bernier | BeO | Target boat #1 | | Done | Sintering new BeO pellets |
John Wong wrote: |
John Wong wrote: |
Nikita Bernier wrote: |
Thursday, March 29, 2012, 19:17
Target boat contains 3 BeO pellets :
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 9.06, 1.9713, 1.413
2 9.11, 1.9900, 1.416
3 13.54, 1.9916, 0.956
Samples 1 and 2 are made of BeO powder with 30% PVB which was washed with excess acetone and let to dry on a greased baking sheet (with PAM Butter flavoured). The flakes were then milled for 26 minutes at 400 RPM. It resulted in a very fine grey powder, much denser than the BeO powder with 30% PVB (not washed with acetone) that was used for Sample 3.
The initial settings on Evaporator #2 were 100 A and 0.83 V until the vacuum increased.
Evaporator #2 is now auto-ramping overnight at 1 A/min, up to 700 A, with the maximum voltage limited at 14 V, between 5.00e-05 (Good vacuum) and 6.00e-05 Torr (Bad vacuum).
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Thursday, March 29, 2012, 22:31:
TGHT tripped off a few times over the past hours. After changing the Good Vac to 2.00e-5 torr and Bad Vac to 3.00e-5 Torr, the target heater are regulating properly and the max pressure is well maintained below 6.5e-5 Torr [Trip point @ 8.0e-5 Torr]. (see attachment#1: parameter.jpg)
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Friday, March 30, 2012, 23:19
Archive of the target current and vacuum over the past 24 hours. (see attachment #1: archive_24hr)
Saturday, March 31, 2012, 12:12
The organic materials have been burnt off. The target heater ramping up is no longer restricted by the vacuum limit.
Archive of the target current and vacuum over the past 10 hours. (see attachment #2: TGHT@240A).
Saturday, March 31, 2012, 22:52
TGHT has stayed at 700A/12.37V, local @ 693A/12.43 = Temp @ 1780C.
The striptool shows some out-gassing when TGHT reached to 700A. (see attachment #3 marked with black circle: TGHT@700A.jpg)
Increasing TGHT to 750A to see if there is any further reaction...
Sunday, April 01, 2012, 10:24
TGHT was ramped up to 750A, local 730A/13.90V. The pressure has come down to low 10e-6 but not stable; Some reaction may be ongoing therefore it's causing the vacuum excursion. (See attachment #4: TGHT @ 750A). Notice the current readback is not constant and it's slowly decreasing as the voltage readback is increasing. There might be some resistant building up.
--> Initiating the cool-down process at 2A/min.
Sunday, April 01, 2012, 19:30
TGHT has ramped down to 0A, and the pressure is going down (currently at 7.e-8 Torr) with no excursion. (see attachment #5: TGHT@0A).
The chamber will be vented tomorrow, and the target materials will be inspected.
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Monday, April 02, 2012, 16:11
After sintering , the 3 BeO pellets have shrunk and feel robust.
The first sample ate through the Ta target boat, shrank a lot and has white and black marks. We suspect the PAM (mostly made of canola oil) to be responsible for the boat damage and the weird sintering process (see John's posts).
Sample 2 is holding well.
Sample 3, which was not washed with acetone, shows some cracks.
Sample, Thickness (mm), Mass (g), Density (g/cm3)
1 -----, 0.6254, -----
2 5.81, 0.9229, 1.032
3 8.89, 1.1073, 0.809
The average mass before sintering was 1.9843 g. After sintering, 0.8852 g. Thus the average mass loss is 0.9757 (49.0%).
We are starting a new batch of treated powder washed with acetone without PAM.
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16
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Thursday, April 05, 2012, 16:40 |
Nikita Bernier | BeO | Target boat #2 | | Done | Sintering BeO pellets #3 | Thursday, April 05, 2012, 16:31
Target boat contains 6 BeO pellets :
Sample, Mass (g), Thickness (mm), Density (g/cm3)
1 1.2842, 5.406, 1.4647
2 1.2619, 5.150, 1.5108
3 1.2886, 5.316, 1.4946
4 1.2858, 5.310, 1.4931
5 1.3382, 5.520, 1.4948
6 1.3916, 5.650, 1.5187
Samples are made of BeO powder with 30% PVB which was treated at 400 RPM for 26 minutes. A ratio of 1:0.1 of mineral oil was added before another high speed treatment for 10 minutes. The powder was then pressed into pellets.
Pellets are loaded on a target boat coated/sintered with TaC. The target boat is wrapped with a Ta foil that is 0.002 inches thick.
**** Sintering is postponed until the situation with the ventilation in the lab06 is cleared. ****
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17
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Tuesday, May 15, 2012, 12:26 |
John Wong | SiC | 38481-2 | HP-SIS | Done | Re-condition the HP-SIS SiC target | Tuesday, May 15, 2012, 12:24
The HP-SIS SiC target was made on Nov 03, 2010. The target consists of 405 discs, 18.5cm in length. It was sintered in the Evaporator#1.
This target is going into Evap#2 for re-conditioning. It is currently being pumped down.
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22
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Friday, May 18, 2012, 12:19 |
Nikita Bernier | SiC | 38481-2 | HP-SIS | Done | Re-condition the HP-SIS SiC target |
John Wong wrote: |
Tuesday, May 15, 2012, 12:24
The HP-SIS SiC target was made on Nov 03, 2010. The target consists of 405 discs, 18.5cm in length. It was sintered in the Evaporator#1.
This target is going into Evap#2 for re-conditioning. It is currently being pumped down.
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Friday, May 18, 2012, 12:19
The target is wrapped with only one heat shield.
Evaporator #2 Target Heater is now auto-ramping at 0.5 A/min, up to 820 A, with the maximum voltage limited at 2 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). Tube Heater is auto-ramping at 0.5 A/min, up to 230 A, with the maximum voltage limited at 1 V. See attachments.
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Attachment 1: autoramp1.png
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Attachment 2: ievap2autoheat1.png
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23
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Friday, May 18, 2012, 13:17 |
John Wong | SiC | 38481-2 | HP-SIS | Done | Re-condition the HP-SIS SiC target |
Nikita Bernier wrote: |
John Wong wrote: |
Tuesday, May 15, 2012, 12:24
The HP-SIS SiC target was made on Nov 03, 2010. The target consists of 405 discs, 18.5cm in length. It was sintered in the Evaporator#1.
This target is going into Evap#2 for re-conditioning. It is currently being pumped down.
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Friday, May 18, 2012, 12:19
The target is wrapped with only one heat shield.
Evaporator #2 Target Heater is now auto-ramping at 0.5 A/min, up to 820 A, with the maximum voltage limited at 2 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). Tube Heater is auto-ramping at 0.5 A/min, up to 230 A, with the maximum voltage limited at 1 V. See attachments.
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Friday, May 18, 2012, 13:15
Increased TBHT voltage to 5V, and TGHT to 15V. Currently, TBHT =83A, 0.986V, TGHT= 144A, 1.65V, IGP1 = 5.2e-7 Torr, IGP2 = 4.3e-7 Torr.
Continue ramping up...
Tuesday, May 22, 2012, 12:02
TGHT and TBHT were ramped up to 830A/13.65V (local), and 235A/3.85V, respectively. The target was conditioned over the long weekend.
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24
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Tuesday, May 22, 2012, 12:15 |
Nikita Bernier | SiC | 38481-2 | HP-SIS | Done | Re-condition the HP-SIS SiC target |
John Wong wrote: |
Nikita Bernier wrote: |
John Wong wrote: |
Tuesday, May 15, 2012, 12:24
The HP-SIS SiC target was made on Nov 03, 2010. The target consists of 405 discs, 18.5cm in length. It was sintered in the Evaporator#1.
This target is going into Evap#2 for re-conditioning. It is currently being pumped down.
|
Friday, May 18, 2012, 12:19
The target is wrapped with only one heat shield.
Evaporator #2 Target Heater is now auto-ramping at 0.5 A/min, up to 820 A, with the maximum voltage limited at 2 V, between 2.00e-05 (Good vacuum) and 3.00e-05 Torr (Bad vacuum). Tube Heater is auto-ramping at 0.5 A/min, up to 230 A, with the maximum voltage limited at 1 V. See attachments.
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Friday, May 18, 2012, 13:15
Increased TBHT voltage to 5V, and TGHT to 15V. Currently, TBHT =83A, 0.986V, TGHT= 144A, 1.65V, IGP1 = 5.2e-7 Torr, IGP2 = 4.3e-7 Torr.
Continue ramping up...
Tuesday, May 22, 2012, 12:02
TGHT and TBHT were ramped up to 830A/13.65V (local), and 235A/3.85V, respectively. The target was conditioned over the long weekend.
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Tuesday, May 22, 2012, 12:13
Initiating the cool-down process at 5 A/min.
See archive plots of the Target Heater (Attachment 1) and the Tube Heater (Attachment 2). |
Attachment 1: TGHT-VAC1.JPG
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Attachment 2: TBHT-VAC1.JPG
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