Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2, Page 12 of 35  Not logged in ELOG logo
ID Date Author Target Material Target Oven W.O#down Source Status Subject
  459   Thursday, September 26, 2019, 14:03 Aaron SchmidtNb41882-3TARGET BOATIn progressHS swap & test Nb target

 HS# 42752-7

Thursday, September 26, 2019, 13:46: Remove Flexible lines HS

Thursday, September 26, 2019, 14:03: Assy installed.


Friday, September 27, 2019, 07:07: Vacuum @ 1.16e-06T. 

Friday, September 27, 2019, 07:09: Waterlines opened. Vacuum stable @ 1.15e-06T 


Monday, September 30, 2019, 10:04: Remove Nb target & assy. Install flexible line HS. 

  522   Wednesday, November 04, 2020, 17:31 Ferran Boix PamiesEmpty41882-2TARGET BOATDoneParasitic target graphite outgassing.

 2020-11-04 17:31: target installed with boat containing graphite container for outgassing. Roughing pump on.

 2020-11-04 17:49 turbo on, leaving it pumping over night.

 2020-11-05 11:32 leak check ok. Ramping up target to 200A 2A/10s.

 2020-11-05 11:53 IGP1:1.1e-6T . Ramping up target to 300A 1A/10s.

 2020-11-05 11:53 IGP1:1.2e-6T . Pyrometer:1320degC. Ramping up target to 400A 1A/10s.

 2020-11-05 11:53 IGP1:1.8e-6T . Pyrometer:1650degC. Ramping up target to 500A 1A/10s.

 2020-11-05 12:57 IGP1:3.4e-6T . Pyrometer:1910degC. Ramping up target to 525A 1A/10s.

 2020-11-05 13:02 IGP1:3.6e-6T . Pyrometer:1990degC. Leaving it hot for 1h.

 2020-11-05 14:00 IGP1:2e-6T stable . Pyrometer:1990degC. cooling down 2A/10s.

 

  523   Thursday, November 05, 2020, 15:13 Ferran Boix PamiesEmpty41882-2TARGET BOATDonecleaning treatment.

 2020-11-05 15:44 empty and naked boat in for heating up system and clean up. Turbo on.

 2020-11-06 16:58 IGP1:4e-7T leak check ok. Ramping up target to 500A. 1A/10s.

 2020-11-09 12:43 The target was left at 1500degC during the weekend. 

 2020-11-17 14:11 turbo pump off. Slow venting.

 2020-11-18 09:18 Evap2 vented. Target removed.

  545   Sunday, April 04, 2021, 16:09 Ferran Boix PamiesEmpty41882-2TARGET BOATDoneparasitic target commissioning

 2021-04-04 16:07 New container is in with heatshields, vacuum 8.6E-6 torr. leak check done. ramping up current, checking both pyrometer and TC, 1A/10s.

 2021-04-04 16:49 200A TGHT 250degC on TC 1130degC on pyrometer. Too low on TC, ramping down and venting to reposition TC in the foil. 

 2021-04-04 18:00 TC was slightly broken, repaired now. Pumping chamber.

 2021-04-04 18:41 ramping up to 200A 1A/10s.

2021-04-04 18:41 200A TGHT, TC 389degC pyro 1130degC. ramping to 400A 1A/10s.

2021-04-04 18:41 300A TGHT, TC 554degC pyro 1440degC. 

2021-04-04 18:41 400A TGHT, TC 735degC pyro 1720degC. ramping to 600A 1A/10s. 

2021-04-04 20:15 500A TGHT, TC 891degC pyro 1990degC

2021-04-04 20:15 553A TGHT, TC 975degC pyro 2129degC, ramping down.

2021-04-06 13:44 Parasitic target plus thermocouples were introduced in evap2 the day before and put under vacuum. IG1 3E-7 torr, leak check done. Putting some power into HE while ramping up container to 100A 1a/10s.

2021-04-06 14:06 20W on HE 100A on target container. Everything stable. Ramping up to 200A 1A/10s 

2021-04-06 14:06 20W on HE 200A on target container. Everything stable. Ramping up to 300A 1A/10s 

2021-04-06 14:06 20W on HE 300A on target container. Everything stable 4.6E-7 torr. Ramping up HE to 40W.

2021-04-06 14:06 40W on HE 300A on target container. Everything stable 4.6E-7 torr. Ramping up container to 400A 1A/10s.

2021-04-06 14:06 40W on HE 400A on target container. Everything stable 1E-6 torr. Ramping up container to 500A 1A/10s.

2021-04-06 15:52 35W on HE 500A on target container. Everything stable 1.6E-6 torr. Ramping up He to 65W.

2021-04-06 18:40 at 50W on HE one of them broke, system ramped down, vented, HE replaced, pumping down system again.

2021-04-07 10:38 HE at 70W, ramping up container to 200A 1A/10s. Vacuum 3.3E-7 torr.

2021-04-07 10:59 HE at 70W, 200A on container, ramping up container to 300A 1A/10s. Vacuum 3.9E-7 torr.

2021-04-07 10:59 HE at 65W, 300A on container, ramping up container to 400A 1A/10s. Vacuum 4.5E-7 torr.

2021-04-07 11:50 HE at 70W, 400A on container, ramping up container to 500A 1A/10s. Vacuum 7.8E-7 torr.

2021-04-07 11:50 HE at 65W, 500A on container, ramping up container to 553A 1A/10s. Vacuum 1.4E-6 torr.

2021-04-07 11:50 HE at 65W, 553A on container. All good, ramping down. 1A,10s.

  585   Tuesday, June 28, 2022, 09:31 Ferran Boix PamiesEmpty41882-2TARGET BOATIn progressTC test on Ta tube

Tuesday, June 27, 2022, early afternoon: We assembled the setup in evap2 and started the pumps leaving it running over night.

Tuesday, June 28, 2022, 09:31 Turbo pump stopped for unknown reasons a few hours after we left. Restarting the pump.

Tuesday, June 28, 2022, 10:23 Vacuum down to 1e-5T start to ramp up TGHT 1A/10s to 200A.

Tuesday, June 28, 2022, 1:20 pm, Ramped from 0-500A. thermocouple reading 900C while pyrometer reads 1600C. begin ramping down to 0A.

  480   Monday, March 23, 2020, 07:50 Marla Cervantes 41882-1TARGET BOATDoneConditioning graphite target #1 (T2)

Friday, March 20, 2020, 19:39

The target material is loaded in a graphite cartridge.

The graphite cartridge is placed in a new tantalum boat previously without TaC,

the Ta boat was wrapped with three new Ta heat shields.

The system is currently pumping down. 


Monday, March 23, 2020, 07:49

IGP1 = 2.2e-7 Torr

Good vacuum= 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Ramping TGHT to 40A at 0.5A/min 


Monday, March 23, 2020, 10:35

Due to the COVID-19, non-essential activities are wrapped up,

the conditioning of the carbon target will be postponed until further notice 

  482   Wednesday, May 20, 2020, 12:54 Marla Cervantes 41882-1TARGET BOATDoneConditioning graphite target #1 (T2)

Marla Cervantes wrote:

Friday, March 20, 2020, 19:39

The target material is loaded in a graphite cartridge.

The graphite cartridge is placed in a new tantalum boat previously without TaC,

the Ta boat was wrapped with three new Ta heat shields.

The system is currently pumping down. 


Monday, March 23, 2020, 07:49

IGP1 = 2.2e-7 Torr

Good vacuum= 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Ramping TGHT to 40A at 0.5A/min 


Monday, March 23, 2020, 10:35

Due to the COVID-19, non-essential activities are wrapped up,

the conditioning of the carbon target will be postponed until further notice 

 Wednesday, May 20, 2020, 12:50

On May 19 the pumps of EVAP2 were turned on to purge the system

Today Aaron made a leak check, for details, visit elog-481

Currently IGP1 = 8.17e-7 Torr


 Thursday, May 21, 2020, 09:41

IGP1 = 4.5e-7 Torr

TGHT = 0.03 V, 0.028 A

Current will be increased manually to 10 A, and then it will be autoramp to 500 A

Whit this power supply the current increments are register since the beging 

TGHT = 0.145 V, 10.35 A

During the input of the 10 A there was no anomaly with the pressure and the autoramp was set to 50A:

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 


Thursday, May 21, 2020, 10:39

The autoramp reached the 50 A set

TGHT = 0.65 V, 49.05 A

Power supply = 0.64 V, 50 A

IGP1 = 4.7e-7 Torr

Everything looks good, autoramp is set to 80 A same conditions

1 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 


Thursday, May 21, 2020, 10:49 

The autoramp reached the 80 A set

TGHT = 1.075 V, 79.36 A

Power supply = 1.07 V, 80 A

IGP1 = 1.7e-6 Torr and increasing

Autoramp is set to 100 A,conditions:

1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 

There was a jump in the vacuum e-log-482-fig-1.


Thursday, May 21, 2020, 11:01 

The autoramp reached the 100 A set

TGHT = 1.4V, 99.9 A

Power supply = 1.4V, 100 A

IGP1 =  0.001 Torr and increasing

Autoramp is set to 120 A,conditions:

1 A each 20 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 


Thursday, May 21, 2020, 11:12 

TGHT = 1.75 V, 120.6 A

Power supply = 1.74 V, 120 A

IGP1 = 0.0018 Torr

The current will be hold and to let the vacuum reduce 


Thursday, May 21, 2020, 11:34

 TGHT = 1.8 V, 120.825 A

Power supply = 1.74 V, 120 A

IGP1 = 9.8e-5 Torr


Thursday, May 21, 2020, 11:37

 Autoramp is set to 300 A,conditions:

2 A each 10 s with a good vacuum of 3e-2 Torr and a bad vacuum 5e-2 Torr 


Thursday, May 21, 2020, 12:21

TGHT = 5.015 V, 298.125 A

Power supply = 5 V, 300 A

IGP1 = 4.77e-5 Torr 

Omega = 1130 degC

Note: Measurments will be taken with ARIEL's pyrometer (I will call it AP in this elog).

The emmisivity this pyrometer accounts for is 0.91 for the range of 1000 C to 1800 C

Above 01800 it will use 0.93 as the emissivity

AP = 977.7 degC


 

Attachment 1: e-log482-fig-1.JPG
e-log482-fig-1.JPG
  493   Friday, July 31, 2020, 11:16 Ferran Boix PamiesEmpty41882-1TARGET BOATDoneThermocouple measurent of boat temperature

Boat with attached thermocouple type C with AREMCO ceramabond glue installed in evap2 the 30-07-2020

Vacuum 3.2e-6torr in IGP1 after night with the roughing pump and morning with turbo.

TGHT heater on.

ramp up started

1A/20s up to 200A

Thermocouple de-attached at about 400A.

Target cooled down. 1A/10s

Turbo and roughing pump off. System left with present vacuum over night. Tomorrow inspection.

  495   Wednesday, August 05, 2020, 19:14 Ferran Boix PamiesEmpty41882-1TARGET BOATDoneParasitic target cooling test

 2020-08-05 7.13pm Roughing pump on

2020-08-06 10:48am Turbo was turned on by Marla in the morning. Vacuum IGP1 4e-6Torr. Water leak check performed, everything good to start heating up target. Waiting for Anders confirmation to start.

2020-08-06 4:38pm after changing setup to metallic connections only. Roughing on. After some minutes abnormal behavior in vacuum.

Turning water off to see if it is a small water leak.

Water purged, no change in vacuum.

 

IEVAP2:RV1 was closed. After opening, normal vacuum behavior recovered. The valve is automatically closing when reaching 100Torr. Wasn't doing that before. Turbo on now.

2020-08-07 9:24am pumping over night, vacuum at 8e-7torr. Everything ready for test. Ramping up target heater.Up to 50A 1A/20s

2020-08-07 9:48am all good at 50A, ramping to 250 1A/10s

2020-08-07 10:27am all good at 250A, ramping to 400 1A/10s

2020-08-07 10:57am all good at 400A, ramping to 500 1A/10s

2020-08-07 11:17am Tc type C might have been deatached at 500A, ramping to 600 1A/10s

2020-08-07 11:37am All good, ramping to 700 1A/10s

2020-08-07 11:58am 1950degC on pyrometer, 1200degC on type C TC (probably not well attached anymore), TCs on heatshield [30-40]degC. Pressure 9e-6Torr

2020-08-07 12:44pm All values stable after 45min, starting to ramp up parasitic target heating elements.

2020-08-07 1:15pm Open circuit, would seem that one of the heating elements cracked. Cooling down the target.

 

  496   Tuesday, August 11, 2020, 10:17 Ferran Boix PamiesEmpty41882-1TARGET BOATIn progressContamination foils temperature test

The target was prepared and put under vacuum on 2020-08-10

 

2020-08-11 10:16am The pressure is 1e-6Torr. Leak checked performed, water on no problem. Starting to set target heating curve. 1A/10s up to 300A 

2020-08-11 11:23am target at 300A-1200degC Temperatures on exposed foil show to be higher than expected. 300degC already, 70degC on covered by foil thermocouple. Putting 50 more amps at 1A/10s 

2020-08-11 12:11pm target at 350A-1340degC. 350degC on exposed thermocouple. Ramping to 400A 1A/10s.

2020-08-11 12:28pm target at 400A-1420degC. 400degC on exposed thermocouple. Ramping to 450A 1A/10s.

  506   Thursday, September 10, 2020, 07:53 Aaron SchmidtEmpty41790-8LP-FEBIADDoneFernando FEBIAD / Anode testing.

 FEBIAD installed. Anode PS installed. ANODE connected!.

Leak check

Thursday, September 10, 2020, 07:46: Vacuum @ 6.30e-07T

Thursday, September 10, 2020, 07:47: HS Waterline open. Stable vacuum.

Thursday, September 10, 2020, 07:51: Auto-ramp TGHT / TBHT to 400 / 200 A @ 2 A per min. 


FM

Thursday, September 10, 2020, 13:28: Pyrometer aligned.  Current reading 1106.7 @ slope=0.9

Thursday, September 10, 2020, 13:46: Auto-ramp TGHT / TBHT to 580/ 250A @ 2 A per min. 

Thursday, September 10, 2020, 13:47: Recording pyrometer data 

Thursday, September 10, 2020, 15:33: Auto-ramp finished. Temperature=1568.0 @slope=0.9

Thursday, September 10, 2020, 15:35: Voltage power supply limited to 150 mA.

Thursday, September 10, 2020, 15:36: Voltage power supply is set to output. Nothing strange on the other PS.

Thursday, September 10, 2020, 15:42: Slowly increased the voltage to 150 V but nothing read. two times during the voltage sweep the current on the Ps showed 1mA. Nothing strangeon the vacumm or the other power supply voltages

Thursday, September 10, 2020, 15:45: Auto-rampup TBHT to 290 @ 2A/min 

Thursday, September 10, 2020, 16:08: Voltage sweep  

Thursday, September 10, 2020, 17:24: Auto-rampup to 300 @ 2A/min


Friday, September 11, 2020, 11:05: Auto-ramping to 290 @ -2A/min 

Friday, September 11, 2020, 13:22: auto-ramping to 305 @ 2A/min 

Friday, September 11, 2020, 14:10: The power supply is not reading current anymore. At 305 A I couldn't get any reading. I lowered the current to 290 A and the PS displays 0 mA even at 500 V, whereas before it showed 13 mA.

Vacuum looks normal not any sort of spike.

I will open the system to inspect the interior.

Friday, September 11, 2020, 14:15: Auto-cooling to 0 A TGHT/TBHT @-2A/min 


Saturday, September 12, 2020, 10:52: Venting 

Saturday, September 12, 2020, 14:00: Confirmed anode de-attached. I will spot welded again. 

Saturday, September 12, 2020, 18:29: After many failures I aborted the spot welding. The anode ended up looking pretty bad. 


 Sunday, September 13, 2020, 19:06: Opened waterlines. Vacuum still decreasing.

Monday, September 14, 2020, 09:12: Vacuum @  8.15e-7 T. and decreasing. I will start the ramping now.

Monday, September 14, 2020, 09:28: Auto-ramping to 400/200 A @ 4/min (1 A/15 s) .

No reading on the 2-color pyrometer channel. 1-color channels indicate around 1000C

 Monday, September 14, 2020, 12:49: Recording temperature and vacuum. Auto-ramp TBHT to 210 @ 4A/min.

 Monday, September 14, 2020, 12:57: Emissivity slope sweep. Only "under" is being shown

Monday, September 14, 2020, 12:58:  Auto-ramp TBHT to 220 @ 4A/min. 

Monday, September 14, 2020, 13:05: Emissivity slope sweep. Only "under" is being shown

Monday, September 14, 2020, 13:06: Auto-ramp TBHT to 240 @ 4A/min.  

Monday, September 14, 2020, 13:17: Auto-ramp TBHT to 250 @ 4A/min.   

Monday, September 14, 2020, 13:22: Emissivity slope sweep. Only "under" is being shown 

Monday, September 14, 2020, 13:23: Auto-ramp TBHT to 260 @ 4A/min.    

Monday, September 14, 2020, 13:27 : Emissivity slope sweep. Only "under" is being shown 

Monday, September 14, 2020, 13:27 : Auto-ramp TBHT to 275 @ 4A/min.    

Monday, September 14, 2020, 13:36: Emissivity slope sweep. Only "under" is being shown for the 2-color channel. 1-color channel displays around 1200 C. Maybe there is a different  cutoff for the 2-color channel

Monday, September 14, 2020, 13:38: At 400V the PS reads back 1mA 

Monday, September 14, 2020, 13:39 : Auto-ramp TBHT to 290 @ 4A/min.   

Monday, September 14, 2020, 17:41: Roughing 


Tuesday, September 15, 2020, 07:03: Vacuum stable at 4.65e-7T.

Tuesday, September 15, 2020, 07:03:  Auto-ramp TGHT / TBHT to 400/ 200A @ 4 A per min. 

Tuesday, September 15, 2020, 10:00:  Auto-ramp TGHT  to 500 @ 4 A per min. 

Tuesday, September 15, 2020, 11:13:  Auto-ramp  TBHT to 250@ 4 A per min. 

Tuesday, September 15, 2020, 15:44: There is a short inside the system. I  thought it might be the vanadium wire but increasing the tbht current did not indicate a clear evaporation so I don't think this is the case.

I'll ramp down to 0 at 8A/min to open and inspect. My measurements don't make any sense without both the pyrometer and the anode leakage current reading.

Tuesday, September 15, 2020, 15:49: Auto-cooling TGHT/TBHT to 0A at 8A/min (2A /15 s).

 Tuesday, September 15, 2020, 16:00: Auto-cooling aborted, the system is no longer current limited. The contact causing the issue probably moved while cooling.

***many ramp ups.downs, Temperature measurements, voltage sweeps, inverse temperature estimations. Absolute temperature measurements for when the vanadium wire melted, the pyrometer was already reading 1920, a slightly adjust on the emissivity slope move it to 1911C

Tuesday, September 15, 2020, 18:47: Ramp down TGHT/TBHT to 500/250 A @ -1A/min

Tuesday, September 15, 2020, 18:48: Done for today. 


Wednesday, September 16, 2020, 10:02: Auto-ramp up TGHT/TBHT to 580/285 A @ 2A/min 

Wednesday, September 16, 2020, 12:59: Auto-ramp  up TGHT/TBHT to 600 A @ 2 A/min 

Wednesday, September 16, 2020, 13:45: Auto-ramp up TBHT to 290 A @ 1A/min 

Wednesday, September 16, 2020, 18:45: Auto-ramp down TGHT/TBHT to 400/200 A @ -2A/min 


Thursday, September 17, 2020, 08:46: Auto-ramp up TBHT to 285 A @ 2A/min 

Thursday, September 17, 2020, 12:03: Auto-cooling TGHT/TBHT to 0A @ -4A/min

Thursday, September 17, 2020, 13:49: Turbo off. Roughing pump off 

  623   Thursday, April 20, 2023, 07:00 Darwin Ortiz RosalesTaC41790-7LP-FEBIADDoneTaC coating sintering

Thursday, April 20, 2023, 06:59

The coated container was wrapped in 3 Ta foil heatshields.

Target temperature on OMEGA= 1830-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


Thursday, April 20, 2023, 07:02

Started TBHT and TBHT ramp at 1A/min to 230A


Thursday, April 20, 2023, 09:55

From 170 A started ramping at 2A/min to 230 A on both TGHT and TBHT


Thursday, April 20, 2023, 10:27

Starting ramp on TGHT to 300A, TBHT kept at 230A, 3.0 V


Thursday, April 20, 2023, 11:19

ramping at 4A/min (2A/30s) to 340 A on TGHT


Thursday, April 20, 2023, 11:40

After plot, ramping @ 2A/min to 460A on TGHT expected to reeach at 1245.  4 hours at 4:45 pm


Thursday, April 20, 2023, 13:44

Note that top temperature was 1835C @  480 A, 7.9V


Thursday, April 20, 2023, 17:00

Start rampdown at -2A/min TGHT and -1A/min TBHT


Monday, April 24, 2023, 13:35

The coating is not as good as expected.  Maybe too much time between coating and sintering.  Will not use for TiC target.

  327   Wednesday, September 28, 2016, 17:09 Laura LambertEmpty41790-6LP-SISDonesintering TaC coating on UCx container

 Wednesday, September 28, 2016, 17:08

Container coated with TaC using 'flushing technique' today, cleaned ionizer tube with acetone, no coating inside ionizer tube

Dried by blowing air into tube

Wrapped with 3 x Ta heat shields, incl center block - new method of each layer being one long single Ta foil covering entire container incl center block

Currently pumping down in evap2


 Thursday, September 29, 2016, 11:11

HS water valves opened

Tapped up to 35A

Waited ~45min, vacuum stable

IGP1 = 1.4e-6 Torr

Initiating auto ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Max setpoints for TGHT = 350A and TBHT  = 230A

Once max setpoints achieved, will tap up manually to final desired temperature of 1900C


 Friday, September 30, 2016, 10:51

IGP1 = 7.8e-7 Torr

TGHT = 315A, 4.57V

TBHT = 174A, 2.8V

Increasing ramping rate to 1.0A/min and 0.5A/min for the TGHT and TBHT respectively.


 Friday, September 30, 2016, 11:44

Changed OMEGA slope to 0.98

IGP1 = 1e-6 Torr

TGHT = 350A, 5.2V

TBHT = 201A, 3.4V

Increasing ramping rate of TBHT to 1.0A/min

OMEGA = 1625C / MIKRON = 1625C


 Friday, September 30, 2016, 15:45

IGP1 = 1.1e-6 Torr

TGHT = 430A, 6.79V

TBHT = 230A, 4.07V

OMEGA = 1903C

Will remain at max setpoints over weekend.

See attached link for raw data of manual tap up.

Also see attached photos of screenshots showing oval - not circular - tube of target container at two different temperatures...


 Monday, October 03, 2016, 13:28

IGP1 = 1.79e-7 Torr

TGHT = 430A, 6.87V

TBHT = 230A, 4.06V

OMEGA = 1892C

MIKRON = 1847C

Attached is a picture taken through the MIKRON, the slight oval shape appears to be a minor bend in the target container:

With the ionizer tube facing into the page, the bend appears to be in the center with both ends of the container bent slightly towards the page

This possible bend in the container gives the appearance of the oval shape through the camera while it is being heated, due to the angle of the camera

Remained at max setpoints over weekend.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Tuesday, October 04, 2016, 13:40

Vented in air and opened up this morning.

Container done, TaC coating looks good.

Waiting further inspection...


 Tuesday, October 04, 2016, 14:48

Container placed on jig and inspected.

Approved to go ahead for use online by Anders and Friedhelm.


 

Attachment 1: sintering_TaC_coating.xlsx
Attachment 2: sintering_TaC_coating.JPG
sintering_TaC_coating.JPG
Attachment 3: sintering_TaC_coating2.JPG
sintering_TaC_coating2.JPG
Attachment 4: sintering_TaC_coating-combo_of_both_pics.JPG
sintering_TaC_coating-combo_of_both_pics.JPG
  328   Friday, October 07, 2016, 16:42 Laura LambertTa41790-5LP-SISIn progressConditioning Ta#50

Friday, October 07, 2016, 16:40

Target consists of 470 discs.

Total packed length 3.4cm [exactly 7.8cm space on both sides]

Total mass 47.6889g [Incl foils + Ta wire on 6 packs]

Note: Target consists of 350 single discs and 6x20 packs of Ta discs

3x Ta Heat shields.

No endcaps inserted, no Rh foil inserted.

Chamber currently pumping down.

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


 Tuesday, October 11, 2016, 10:02
 
HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 2e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

 Wednesday, October 12, 2016, 16:15

Tapped up to 1900C? [see attached link for data concerning temperature readings]

TGHT = 450A, 7.16V

TBHT = 230A, 4.1V

OMEGA = 1748C

IGP1 = 6.1e-7 Torr


 

Attachment 1: Ta#50_no_endcaps_3xh.s..xlsx
  329   Wednesday, October 12, 2016, 21:18 John WongTa41790-5LP-SISIn progressConditioning Ta#50

Laura Lambert wrote:

Friday, October 07, 2016, 16:40

Target consists of 470 discs.

Total packed length 3.4cm [exactly 7.8cm space on both sides]

Total mass g [Incl foils + Ta wire on 6 packs]

Note: Target consists of 350 single discs and 6x20 packs of Ta discs

3x Ta Heat shields.

No endcaps inserted, no Rh foil inserted.

Chamber currently pumping down.

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


 Tuesday, October 11, 2016, 10:02
 
HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 2e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

 Wednesday, October 12, 2016, 16:15

Tapped up to 1900C? [see attached link for data concerning temperature readings]

TGHT = 450A, 7.16V

TBHT = 230A, 4.1V

OMEGA = 1748C

IGP1 = 6.1e-7 Torr


 

 Wednesday, October 12, 2016, 21:14

Current status before cooling down:

TGHT at 450A/7.32V; TBHT at 230A/4.10V; OMEGA at 1747C

Vacuum at 4.05 e-7 Torr.

Initiate auto-rampping at 2A/min for TGHT and 1A/min for TBHT


 

  330   Thursday, October 13, 2016, 17:32 Laura LambertTa41790-5LP-SISDoneConditioning Ta#50

John Wong wrote:

Laura Lambert wrote:

Friday, October 07, 2016, 16:40

Target consists of 470 discs.

Total packed length 3.4cm [exactly 7.8cm space on both sides]

Total mass g [Incl foils + Ta wire on 6 packs]

Note: Target consists of 350 single discs and 6x20 packs of Ta discs

3x Ta Heat shields.

No endcaps inserted, no Rh foil inserted.

Chamber currently pumping down.

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


 Tuesday, October 11, 2016, 10:02
 
HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 2e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

 Wednesday, October 12, 2016, 16:15

Tapped up to 1900C? [see attached link for data concerning temperature readings]

TGHT = 450A, 7.16V

TBHT = 230A, 4.1V

OMEGA = 1748C

IGP1 = 6.1e-7 Torr


 

 Wednesday, October 12, 2016, 21:14

Current status before cooling down:

TGHT at 450A/7.32V; TBHT at 230A/4.10V; OMEGA at 1747C

Vacuum at 4.05 e-7 Torr.

Initiate auto-rampping at 2A/min for TGHT and 1A/min for TBHT


 

 Thursday, October 13, 2016, 17:32

vented in air and opened up this morning.

target looks good.

  331   Thursday, October 13, 2016, 18:05 Laura LambertTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

  332   Saturday, October 15, 2016, 12:42 Aurelia LaxdalTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

  333   Sunday, October 16, 2016, 17:55 Aurelia LaxdalTa41790-5LP-SISIn progressTemperature measurements for Ta#50

Aurelia Laxdal wrote:

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

 Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand. 

  334   Tuesday, October 18, 2016, 09:23 Laura LambertTa41790-5LP-SISDoneTemperature measurements for Ta#50

Aurelia Laxdal wrote:

Aurelia Laxdal wrote:

Laura Lambert wrote:

Thursday, October 13, 2016, 18:04

Target loaded into evap2

No heat shields.

Both endcaps inserted and expanded.

Rh foil inserted [when inserting, the Ta rod used to expand the Rh foil inside the ionizer tube snapped off inside the container - this piece was able to be shaken out and is no longer inside]

Chamber pumped down.

HS water valves opened, no leaks detected
 
Tapped up manually to 35A
 
Vacuum stable, IGP1 = 5e-7 Torr
 
Initiating auto-ramp.
 
OMEGA slope = 0.98

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 300A at 2.0A/min.

Final desired temperature = 1900C


Friday, October 14, 2016, 13:28

TGHT and TBHT had reached 300A/ 230A respectively.

Power bump ~10min ago caused evap2 to trip off.

Tapped back up manually to 35A.

Re-initiating auto ramp now.


 

Friday October 14: the target was ramp up to 300A/230A after Laura started it. Then, I cooled down at 6pm before leaving TRIUMF. <br>

Saturday October 15: restated the auto-ramp for Ta#50 in EVAP2. It's currently set to go to 300A/230A.

 Sunday October 16: the target temperature measurements up to 620A/230A were performed today not on October 15 (yesterday, it was cooled down before reaching 300A/230A). Currently the target is cooling down, to be ready tomorrow morning for the Test Stand. 

 Monday, October 17, 2016, 09:21

Vented in air and taken out this morning.

Target looks good!


 

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