Thursday, April 20, 2023, 06:59
The coated container was wrapped in 3 Ta foil heatshields.
Target temperature on OMEGA= 1830-1900 C
OMEGA slope:= 0.990
Target time at max temperature = 4 hours
Final Current TBHT= 230A
Final TGHT current= ~400A (adjustable)
Good vacuum = 5.0 e-04 Torr
Bad vacuum = 5.0E-02 Torr
Thursday, April 20, 2023, 07:02
Started TBHT and TBHT ramp at 1A/min to 230A
Thursday, April 20, 2023, 09:55
From 170 A started ramping at 2A/min to 230 A on both TGHT and TBHT
Thursday, April 20, 2023, 10:27
Starting ramp on TGHT to 300A, TBHT kept at 230A, 3.0 V
Thursday, April 20, 2023, 11:19
ramping at 4A/min (2A/30s) to 340 A on TGHT
Thursday, April 20, 2023, 11:40
After plot, ramping @ 2A/min to 460A on TGHT expected to reeach at 1245. 4 hours at 4:45 pm
Thursday, April 20, 2023, 13:44
Note that top temperature was 1835C @ 480 A, 7.9V
Thursday, April 20, 2023, 17:00
Start rampdown at -2A/min TGHT and -1A/min TBHT
Monday, April 24, 2023, 13:35
The coating is not as good as expected. Maybe too much time between coating and sintering. Will not use for TiC target. |