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Message ID: 623     Entry time: Thursday, April 20, 2023, 07:00
Author: Darwin Ortiz Rosales 
Target Material: TaC 
Target Oven W.O#: 41790-7 
Source: LP-FEBIAD 
Status: Done 
Subject: TaC coating sintering 

Thursday, April 20, 2023, 06:59

The coated container was wrapped in 3 Ta foil heatshields.

Target temperature on OMEGA= 1830-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~400A (adjustable)

Good vacuum = 5.0 e-04 Torr

Bad vacuum = 5.0E-02 Torr


Thursday, April 20, 2023, 07:02

Started TBHT and TBHT ramp at 1A/min to 230A


Thursday, April 20, 2023, 09:55

From 170 A started ramping at 2A/min to 230 A on both TGHT and TBHT


Thursday, April 20, 2023, 10:27

Starting ramp on TGHT to 300A, TBHT kept at 230A, 3.0 V


Thursday, April 20, 2023, 11:19

ramping at 4A/min (2A/30s) to 340 A on TGHT


Thursday, April 20, 2023, 11:40

After plot, ramping @ 2A/min to 460A on TGHT expected to reeach at 1245.  4 hours at 4:45 pm


Thursday, April 20, 2023, 13:44

Note that top temperature was 1835C @  480 A, 7.9V


Thursday, April 20, 2023, 17:00

Start rampdown at -2A/min TGHT and -1A/min TBHT


Monday, April 24, 2023, 13:35

The coating is not as good as expected.  Maybe too much time between coating and sintering.  Will not use for TiC target.

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