Thursday, August 25, 2022, 10:06

Target container is loaded with 379 Discs of TiC for Target and 5 extra discs for analysis on left end

Target length = 12.5

3 Ta foil heatshields and on TaC coated Ta spring on right side

Total weight including heatshields and spring = 1551.4 g   Final total weight = 1545.5 g

Final power should be ~10988 Watt

TGHT ramp up to 820A, and TGHT to 300A at 0.1A/min.

IGP1= 7.7e-7 Torr

Good vacuum =3.0e-05 Torr

Bad vacuum = 5e-04 Torr

Initial TGHT and TBHT autoramped @1A/min to 50A

TBHT mas 230A

TGHT max depends on final power

Thursday, August 25, 2022, 11:17 

Start autoramp at 1A/min to 80A on both TGHT and TBHT

Thursday, August 25, 2022, 11:54 

leaving at 80A until pressure stops rising

Thursday, August 25, 2022, 22:29

left to autoramp to 230A TBHT and 750 A TGHT since approximately 2:00 pm

Will leave ramping @1A/min to 750 A on TGHT

TBHT currently at 230A

 Friday, August 26, 2022, 07:27

TGHT = 850A, 9.3V

Started autoramp to 850A at 1A/min for TGHT

TBHT held at 230A

OMEGA = 1584C

Friday, August 26, 2022, 09:34

Target running at ~820A, 13.1 V since 9

Cooling to start between 1:15 to 1:30 pm

OMEGA reads 1668 C at top current

current reading oscillates between 812A and 828A and 13.1V  to 13.2V.

Monday, August 29, 2022, 12:21

Cooling at -2A/min for TGHT and -1A/min TBHT started on time on Friday August 26th.

Target remained under vacuum after cooling, over the weekend.

Target removed this morning and looks good. 5 discs removed for analysis

 Thursday, September 02, 2021, 06:36

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down over previous night

Good vacuum = 3.00 e-5 Torr

Bad vacuum = 5.00 e-4 Torr

IGP1=7.7e-07 Torr

Initiate autoramp to 50 A @ 1A/min

Thursday, September 02, 2021, 06:54 

Stopped autoramp after reading email about EF-12 trip and compressed air issue.  Reset to 0 A both TGHT and TBHT

Thursday, September 02, 2021, 12:01

Ispite of site compressed air issues, EVAP 2 has not tripped.  Will manually increase current to40A for both TGHT and TBHT.

IGP1= 1.06 E-06 Torr. 

Friday, September 03, 2021, 08:06

 IGP1= 7.2e-07 Torr

TGHT= 43A, 0.5 V

TBHT= 41A, 0.48 V

Start autoramp at 1A/min to 90A on both TGHT and TBHT

Friday, September 03, 2021, 10:22

IGP1= 1.55 e-06 Torr

TGHT = 90.1 A, 1.1 V

TBHT= 90.0 A, 1.2 V

Continue ramp up at 1A/min to 400 A for TGHT and 230A for TBHT 

Friday, September 03, 2021, 16:05

430A on TGHT will keep for four hours.  OMEGA = 1856 C but according to regression should be 1900.  will keep at this temp. 

Friday, September 03, 2021, 21:11

OMEGA has been at 1875C for 4 hours.  Will start ramp down @ -2A per minute for TGHT and -1A min for TBHT

TGHT = 430 A, 7.3 V   (current actually fluctuates between 428 and 433 A since new power supply

TBHT = 233A, 4.0V  (set to 230 but displays 233) 

Tuesday, March 02, 2021, 11:26 

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Initial weight including heat-shields = 433.8 g

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over night.

Good vacuum = 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

Wednesday, March 03, 2021, 13:28

IGP1 = 4.0 e-7 Torr

Start ramping @ 1A/min to 20A on both TGHT and TBHT

Wednesday, March 03, 2021, 15:03

Start ramping @1/min to 60A on Both TGHT and TBHT

Wednesday, March 03, 2021, 22:42

TGHT = 60A, TBHT = 60A

IGP1= 4.2 e-7 stable

Start ramping to 400A @ .5A/min for TGHT and @0.5A/min for TBHT to 230A

Thursday, March 04, 2021, 11:56

TGHT = 400 A, TBHT =230A

IGP1= 1.9e-6 Torr

OMEGA = 1695 C

Continue ramp up @0.5A/min to 430A on TGHT

Thursday, March 04, 2021, 14:02

IGP1 = 1.87e-6 Torr

TGHT = 434 A , 7.2 V

OMEGA = 1787 C

Will tap up manually 450A @ on TGHT and leave at that current for ~4 hours

Thursday, March 04, 2021, 19:35

After ~ 5 hours at 1829 C max OMEGA reading

OMEGA = 815 C 

Start ramp down at 1A/min on TGHT and 0.8A/min for TBHT

IGP1= 1.2e-6 Torr

 Ta#62 LP-SIS target description: (REPLACEMENT FOR 44139-10)

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm

Target density = 14.29 g/cm3

Target length = 3.4 cm

Total Mass = 48.602 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven= 456 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (Not expanded). No Ta foil heat shield added

Wednesday, June 23, 2021, 17:46: Roughing.

Wednesday, June 23, 2021, 18:03: TP1 on.

Wednesday, June 23, 2021, 18:09: TP1 @ speed. Vacuum @ 1.53e-04T & dropping.

TBHT will be ramped up to 230A 

TGHT will be ramped up to 600A +

Final desired temperature = 1900C.

OMEGA slope = 0.98.

Thursday, June 24, 2021, 07:38: PS on.  

Thursday, June 24, 2021, 07:45: TGHT / TBHT tapped up to 10 A. Slope @ 0.98

Thursday, June 24, 2021, 07:46: Auto Ramping TGHT / TBHT to 350 / 150 A @ @ A per min.

Thursday, June 24, 2021, 10:47: TGHT / TBHT @ 350 / 150 A. Auto Ramping TGHT / TBHT to 580 / 230 A @ @ A per min. Temp @ 1120 C

Thursday, June 24, 2021, 12:59: TGHT / TBHT @ 580 / 230 A. Vacuum @ 8.24e-06T. Temp @ 1717 C. Auto-ramping TGHT to 600 A @ 2 A per min.   

Thursday, June 24, 2021, 13:10: Vacuum @ 8.83e-06T. Temp @ 1758 C. Auto-ramping TGHT to 620 A @ 2 A per min. 

Thursday, June 24, 2021, 13:21: Vacuum @ 1.0e-05T. Temp @ 1798 C. Auto-ramping TGHT to 645 A @ 2 A per min.  

Thursday, June 24, 2021, 13:37: Vacuum @ 1.15e-05T. Temp @ 1845 C. Tap up TGHT to 650 manually.

Thursday, June 24, 2021, 13:45: Vacuum @ 1.21e-05T. Temp @ 1875 C. Tap up TGHT to 665+ manually.

Thursday, June 24, 2021, 13:47: Vacuum @ 1.34e-05T. Temp @ 1901 C. Tapped up TGHT to 677 manually. Desired temperature reached.

Thursday, June 24, 2021, 13:51: Auto-cooling @ 2A per min 

Friday, June 25, 2021, 05:30: TP1 off. BP1 off.    

Friday, June 25, 2021, 07:36: Venting. 

 Wednesday, October 27, 2021, 11:07

Monday, October 25, 2021, 11:52

Ta LPSIS tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over previous night

Good vacuum = 3.00 e-3 Torr

Bad vacuum = 5.00 e-2 Torr

Initial total weight = 464.8 g

Final weight after sintering = 

 Thursday, October 28, 2021, 07:46

IGP1= 7.4e-07 Torr

Initiating autoramp to 40 A on both TGHT and TBHT

ramp rate = 1 A/min

Will keep at 40A for approximately 1 hour or until pressure below 1e-05 Torr

 Thursday, October 28, 2021, 09:41

IGP1= 1.9e-06 Torr TGHT = 40.3 A, 0.48 V TBHT = 39.0 A, 0.48V

Autoramp @ 1A/min to 100A on both TGHT and TBHT

 Thursday, October 28, 2021, 12:57

IGP1= 1.1e-06 Torr

TGHT = 100 A, 1.3 V

TBHT = 100 A, 1.2 V

Start autoramp at 2A/min to 400 for TGHT and 230 for TBHT

The current from the plot (below) required to reach 1900 C seems too high.

Will take to 430 A as previous.  The slope was chequed previously.  Need to check OMEGA.

Thursday, October 28, 2021, 20:08

IGP1=  3.34 e-06 Torr

TGHT = 430A , 7.2 V

TBHT = 233A, 4.1V

OMEGA  = 1628C

Start ramp down at -2A/min for TGHT and -1A/min for TBHT

	44691-3 TaC coating
		TGHT		TBHT			Temperature (C)	Current (A)
	Temperature ( C )	Voltage (V)	Current (A)	Voltage (V)	Current  (A)		1900	512.88
	1250	3.90	255.0				1700	434.06
	1302	4.30	279.0				1800	473.47
	1343	4.60	294.0
	1423	5.10	325.0
	1484	5.7	348.0
	1555	6.2	377.0
										Slope	2.537
										Y intercept	598.66
										R2	0.999

Thursday, August 05, 2021, 11:10

Total number of foils: 380

Total length packed 13.5 cm

container has 3 Ta heat shields.

No endcaps inserted to facilitate out-gassing

Two Ta discs at either end and three graphite discs as separators 

[Left end [ blade--no blade--blade---no blade]  Right end ]

Initially to ramp TGHT and TBHT to 50A at0.5 A/min

Then heat manually to OMEGA ~1400 C , ramping TGHT manually and automatically  to reach 430A A (Omega slope set = 0.990)

Then temperature = 1800C

TBHT will be set fixed at 230 A (max).  TBHT heated manually and automatically to max.

Good vac at 3.00 e -5 Torr

Bad vac at 5.00 e-5 Torr

Total weight into Evap2 =503.8 g

Friday, August 06, 2021, 11:33

IGP1= 8.3e-07 Torr

Start heating at 0.5 A/min on both TGHT and TBHT up to 50A

Friday, August 06, 2021, 22:34

 IGP1= 7.0e-06 Torr

TGHT= 50.1 A, 0.6 V    TBHT = 50.0A, 0.6V

Continue heating at 0.5A/min to 400A on TGHT and 230A on TBHT

Saturday, August 07, 2021, 10:11

Stopped autoramping.  Will allow some time at 63 A on both TGHT and TBHT

Saturday, August 07, 2021, 12:19

IGP1= 1.9e-05 Torr

Manually increase TGHT and TBHT to 65 A 

Saturday, August 07, 2021, 23:01

IGP1= 5.8e-06 Torr

TGHT= 64.5 A, 08V  TBHT=64.6A, 0.8V

Ramp up manually while monitoring pressure 

Sunday, August 08, 2021, 08:46

IGP1= 6.0e-06 Torr

TGHT = 69A, 0.85V  TBHT = 69A, 0.90V

ramp up manually  

Monday, August 09, 2021, 08:54 

IGP1= 1.38e-05 Torr

TGHT= 90.0 A, 1.1V, TBHT= 90.0A 1.3V

Start autoramp at 0.5 A/min on both TGHT and TBHT to 400A and 230A respectively.

Changed bad vacuum to 5e-04 Torr

Monday, August 09, 2021, 21:37

IGP1= 6.6e-06 Torr

TGHT= 300.3 A, 5.0 V, TBHT = 233.0 A, 4.1V

 Increase ramp rate to 2A/min for TGHT to 400 A,

OMEGA = 1430 C

Monday, August 09, 2021, 22:09

Will autoramp at 2A/min up to 424A as per regression line on attached file 

Monday, August 09, 2021, 22:58

Temperature drop on OMEGA.  Unexpected.  Will lower current on TGHT to 418A and keep there for 4 hours.  OMEGA may not be reliable 

Tuesday, August 10, 2021, 3:16

IGP1=8.8e-07 Torr

TGHT = 414A, 7.5V TBHT = 233A, 4.1V

ramp down at -2A/min for TGHT and -1A/min for TBHT

Tuesday, August 10, 2021, 10:35

IGP1= 3.6e-07 Torr

Dismount

Some discs, especially end sections were coated with a golden layer.  

Thursday, September 01, 2022, 10:34

The coated container was wrapped in three Ta foil heatshields.

Target temperature on OMEGA= 1850-1900 C

OMEGA slope:= 0.990

Target time at max temperature = 4 hours

Final Current TBHT= 230A

Final TGHT current= ~420A (adjustable)

Heating autoramp starged at 2A/min on both TGHT and TBHT to 40A

Then at 1A/min on both heaters to 120A.

Good vacuum = 5.0 e-05 Torr

Bad vacuum = 5.0E-04 Torr

Thursday, September 01, 2022, 12:39

Has been stabilizing at 40A on both heaters.

Starting 1A/min autoramp to 80A

A discrepancy between setpoint and readback currents was observed for both TGHT and TBHT.  The difference is substancial and warrants investigation.  This process will be paused until further notice

Tuesday, September 06, 2022, 14:45

Controls has been troubleshooting EVAP2.  In the process TBHT has been damaged. Arthur will take a look at it ASAP and his group will try and fix it tomorrow. 

Regarding our initial problem, it appears that when an electrical safety box was installed, the copper water lines connected to output terminals of the power supply, were moved so that they were in contact with the evaporator cage.  See the figure below.

Thursday, September 08, 2022, 12:47

 Target has been removed and a new test target (HP-FEBIAD) has been placed inside.  System left to generate enough vacuum and then testing will be performed.

Friday, September 09, 2022, 15:58

System was tested and all seems good.  This coat/sintering will continue after conditioning of graphite material

Saturday, September 24, 2022, 09:13

Continuation of process. 

IGP1= 4.3e-07 Torr

ramping @ 1A/min to 230 A on both TGHt and TBHT

Saturday, September 24, 2022, 16:28

ramped to 430A, 7.2V on TGHT and 233A, 4.2V on TBHT.  Will leave until 7 pm.

Saturday, September 24, 2022, 19:44

Starting rampdown @-2A/min TGHT -1A/min TBHT

camera offline

IGP1= 1.2e-6 Torr

Monday, September 26, 2022, 09:41

IGP1=2.2e-07 Torr.  Shutting off TBHT and TGHT.

Thursday, September 29, 2022, 09:53

Final notes: coating looks good .  Probably 3 hours at final temperature is better to prevent material degradation.

 Ta#64 LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.0254mm (0.0010") Measured.

Target density = 12.005 g/cm3

Target length = 3.35 cm

Total Mass = 40.2166 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven= 446 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (Not expanded). No Ta foil heat shield added

Final desired temperature = 1900C.

Thursday, June 02, 2022, 16:49: Roughing 

Thursday, June 02, 2022, 17:02: OMEGA slope = 0.98. 

Thursday, June 02, 2022, 17:10: TP1 on.

Thursday, June 02, 2022, 17:21: TP1 is up to speed. PS on. 

Friday, June 03, 2022, 05:22: Auto-ramping TGHT / TBHT to 500 / 200 A @ 2 A per min. Vacuum @ 1.78e-06T.

Friday, June 03, 2022, 08:59: TGHT / TBHT @ 424 / 200 A. Vacuum @ 3.42e-06T. Temperature @ 1318 C. Auto ramp ongoing.

Friday, June 03, 2022, 09:40: TGHT / TBHT @ 500 / 200 A. Vacuum @ 4.47e-06T. Temperature @ 1469 C. Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per min

Friday, June 03, 2022, 10:47: TGHT / TBHT @ 580 / 230 A. Vacuum @ 6.26e-06T. Temperature @ 1620 C. Auto-ramping TGHT to 600 @ 2 A per min 

Friday, June 03, 2022, 11:08: TGHT / TBHT @ 600 / 230 A. Vacuum @ 6.54e-06T. Temperature @ 1655 C. Auto-ramping TGHT to 630 @ 2 A per min  

Friday, June 03, 2022, 11:30: TGHT / TBHT @ 630 / 230 A. Vacuum @ 7.73e-06T. Temperature @ 1708 C. Auto-ramping TGHT to 650 @ 2 A per min

Friday, June 03, 2022, 11:45: TGHT / TBHT @ 650 / 230 A. Vacuum @ 8.32e-06T. Temperature @ 1748 C. Auto-ramping TGHT to 660 @ 2 A per min

Friday, June 03, 2022, 11:53: TGHT / TBHT @ 660 / 230 A. Vacuum @ 8.83e-06T. Temperature @ 1755 C. Auto-ramping TGHT to 670 @ 2 A per min

Friday, June 03, 2022, 12:05: TGHT / TBHT @ 670 / 230 A. Vacuum @ 9.03e-06T. Temperature @ 1780 C. Auto-ramping TGHT to 680 @ 2 A per min

Friday, June 03, 2022, 12:11: TGHT / TBHT @ 680 / 230 A. Vacuum @ 9.14e-06T. Temperature @ 1795 C. Auto-ramping TGHT to 700 @ 2 A per min 

Friday, June 03, 2022, 12:23: TGHT / TBHT @ 700 / 230 A. Vacuum @ 9.50e-06T. Temperature @ 1822 C. Auto-ramping TGHT to 720 @ 2 A per min

Friday, June 03, 2022, 12:29: TGHT / TBHT @ 720 / 230 A. Vacuum @ 1.00e-05T. Temperature @ 1853 C. Auto-ramping TGHT to 730 @ 2 A per min

Friday, June 03, 2022, 12:36: TGHT / TBHT @ 725 / 230 A. Vacuum @ 1.04e-05T. Temperature @ 1860 C. Manually tap up TGHT to reach desired temperature

Friday, June 03, 2022, 13:04: TGHT / TBHT @ 760 / 230 A. Vacuum @ 1.07e-05T. Temperature @ 1901 C. Desired temperature reached

Friday, June 03, 2022, 13:13: Auto-cooling at 2 A per min. 

Monday, June 06, 2022, 07:07: PS off. BV1 closed & TP1 off.

Monday, June 06, 2022, 08:47: Venting. 

Ta#63 LP-SIS target description: 

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm

Target density = 15.38 g/cm3

Target length = 3.4 cm

Total Mass = 52.296 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven= 457 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (Not expanded). No Ta foil heat shield added

https://elog.triumf.ca/TIS/Target+Production/114

TBHT will be ramped up to 230A 

TGHT will be ramped up to 600A +

Final desired temperature = 1900C.

OMEGA slope = 0.98.

Wednesday, November 10, 2021, 18:05: Roughing. 

Wednesday, November 10, 2021, 18:14: Omega Laser set. On end cap / ok. Slope = 0.980 

Wednesday, November 10, 2021, 18:24: Turbo pump on.

Wednesday, November 10, 2021, 18:25: RV1 valve hissing. Stop TP. Reset, open / close RV1 multiple times. Hissing stopped on its own. Won't affect the pump down, letting pressure out, not in. Will need to replace later.

Wednesday, November 10, 2021, 18:27: Turbo pump on. 

Wednesday, November 10, 2021, 18:32: TP ok. PS on. 

Thursday, November 11, 2021, 11:08: Vacuum @ 4.56e-07T. Auto ramping TGHT / TBHT to 580 / 230 A @ 2A per minute.

Thursday, November 11, 2021, 13:49: TGHT / TBHT @ 313 / 230 A. Vacuum @ 1.46e-06T. Temperature @ 1051 C. Auto ramp continues.

Thursday, November 11, 2021, 16:55: TGHT / TBHT @ 580 / 230 A. Vacuum @ 5.11e-06T. Temperature @ 1621 C. Auto ramp TGHT to 610 A @ 2 A per min.

Thursday, November 11, 2021, 17:13: TGHT / TBHT @ 610 / 230 A. Vacuum @ 6.54e-06T. Temperature @ 1670 C. Auto ramp TGHT to 630 A @ 2 A per min.

Thursday, November 11, 2021, 17:32: TGHT / TBHT @ 630 / 230 A. Vacuum @ 7.82e-06T. Temperature @ 1709 C. Auto ramp TGHT to 650 A @ 2 A per min. 

Thursday, November 11, 2021, 18:49: TGHT / TBHT @ 650 / 230 A. Vacuum @ 7.40e-06T. Temperature @ 1758 C. Auto ramp TGHT to 665 A @ 2 A per min. 

Thursday, November 11, 2021, 19:02: TGHT / TBHT @ 665 / 230 A. Vacuum @ 8.37e-06T. Temperature @ 1790 C. Auto ramp TGHT to 685 A @ 2 A per min. 

Thursday, November 11, 2021, 19:22: TGHT / TBHT @ 685 / 230 A. Vacuum @ 9.56e-06T. Temperature @ 1830 C. Auto ramp TGHT to 700 A @ 2 A per min. 

Thursday, November 11, 2021, 19:41: TGHT / TBHT @ 700 / 230 A. Vacuum @ 1.18e-05T. Temperature @ 1870 C. Manually tap up to 705 A

Thursday, November 11, 2021, 19:43: TGHT / TBHT @ 705 / 230 A. Vacuum @ 1.25e-05T. Temperature @ 1885 C. Manually tap up to 710 A

Thursday, November 11, 2021, 19:44: TGHT / TBHT @ 710 / 230 A. Vacuum @ 1.34e-05T. Temperature @ 1890 C. Manually tap up to 715 A 

Thursday, November 11, 2021, 19:46: TGHT / TBHT @ 715 / 230 A. Vacuum @ 1.75e-05T. Temperature @ 1898 C. Manually tap up to 717 A

Thursday, November 11, 2021, 19:46: TGHT @ 717 A. Temperature @ 1901 C. Temperature reached.

Thursday, November 11, 2021, 19:48: Begin auto-cooling @ 2 A per min.

Friday, November 12, 2021, 06:13: PS off. TP1 off. 

 Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Note:  placed tantalum foil heatshield on both sides of the copper heatshield assembly.

Desired temperature = 1800 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down yesterday

Good vacuum = 3.00 e-03Torr

Bad vacuum = 5.00 e-02 Torr

Wednesday, November 03, 2021, 09:27

Start autoramp at 1A/min to 40A on both TGHT and TBHT

IGP1 initial:  5.3 e-07 Torr

Wednesday, November 03, 2021, 10:22

IGP1= 1.1 e-05 Torr

TGHT = 40 A, 0.5 V 

TBHT= 38.5 A, 0.41 V

Will keep while monitoring pressure at 0.5 A/min to 60A

Wednesday, November 03, 2021, 10:35

IGP1 pressure trending down

IGP1= 6.7 e-06 Torr 

Start ramp up to 60A at 0.5A/min

Wednesday, November 03, 2021, 11:24

IGP1 2.6 e-06 Torr and trending down

Start ramp up to 400A on TGHT and 230A on TBHT at 1A/min

Wednesday, November 03, 2021, 13:28 

 IGP1= 1.4e-05 Torr and trending down slowly.  Will increase ramp speed to 1.5A/min on both TGHT and TBHT to the same final current as before.

Wednesday, November 03, 2021, 15:56 

 IGP1= 2.1 e-05 Torr

TGHT = 400 A,  6.9 V

TBHT = 233 A, 4.1 V

 OMEGA = 1645 C

Will manually ramp up to 1800 C

Wednesday, November 03, 2021, 16:43 

 TGHT = 450 A, 7.9 V

TBHT = 233 A, 4.1 V

OMEGA = 1770 C

IGP1 increasing in Pressure.  Will leave for 4 hours at this current.

Wednesday, November 03, 2021, 20:48

IGP1= 1.0 e-05 Torr

TBHT= 233A, 4.1 V

TGHT = 450 A, 7.9 V

OMEGA = 1751 C

Starting ramp down at -2A/min on TGHT and -1A/min on TBHT

 Friday, March 05, 2021, 10:47

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Initial weight including heat-shields = 431.0 g

Desired temperature = 1900 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 will be pumped down over night.

Good vacuum = 3.00 e-5 Torr

Bad vacuum = 5.00 e-5 Torr

 Saturday, March 06, 2021, 10:29

IGP1= 2.7 e-07 Torr and stable

AutoRamp at 1A/min to 40 A on TGHT and TBHT

Saturday, March 06, 2021, 22:36

IGP1= 2.2e-07 Torr

TGHT = 40.3 A, .46V

TBHT = 38.48 A, .48 V  (set to 40 A)

Start Autoramp at 0.5A/min to 400 A on TGHT and 230A on TBHT

Sunday, March 07, 2021, 07:48

IGP1=8.5e-7 Torr

TGHT = 287 A, 4.6V

TBHT = 232 A, 4.0 V

OMEGA = 1493C

 Increase ramp speed on TGHT to 2A/min to 400A

Sunday, March 07, 2021, 08:36 

 IGP1=1.7 e-06 Torr

TGHT = 373.7 A, 6.3V

TBHT = 232.9 A, 4.1 V

OMEGA = 1752 C

Sunday, March 07, 2021, 08:53

 IGP1= 1.7e-06 Torr

TGHT = 400 A, 6.8 V

TBHT = 232.8 A, 4.1 V

OMEGA= 1842

Ramp TGHT @ 2A/min to 420 A as per attached current approximation

Sunday, March 07, 2021, 09:25

OMEGA=1915 C

TGHT = 420A, 7.2V

TBHT= 232.8 A, 4.1V

IGP1= 1.6 e-06 Torr

Tap down manually to approx 1900 C

TGHT = 412.9 A, 7.0 V and OMEGA=1900 C

Will leave for about 4 hours at this temperature

Sunday, March 07, 2021, 13:05

IGP1= 1.1 e-06 Torr

TGHT = 415 A, 7.2 V

TBHT = 232.8 A, 4.1 V

OMEGA = 1880C

Start cool down at -2A/min on TGHT and -1A/min TBHT

 Monday, November 01, 2021, 07:37

Ta tube was coated with TaC and wrapped with Ta heat-shields (3 layers)

Note* on the leading end of the assembly I placed tantalum foil heatshield similar to what I previously observed there.  I believe it may impact temperature at the entrance of the container tube. 

Desired temperature = 1800 C (expected TGHT ~430 A), TBHT will be set fixed at 230A (max).

Evap 2 was pumped down over the weekend

Good vacuum = 3.00 e-03Torr

Bad vacuum = 5.00 e-02 Torr

Monday, November 01, 2021, 07:39

Starting autoramp at 1 A/min to 40 A on both TGHT and TBHT 

IGP1= 3.5 e-07 Torr

Monday, November 01, 2021, 09:08

 IGP1= 1.6 e-06 Torr

TGHT = 40A, 0.99 V

TBHT = 39A, 1,2 V

Start autoramp @ 1A/min for both TGHT and TBHT to 400A and 230A respectively.

Monday, November 01, 2021, 14:33

OMEGA= 1545 C

TGHT =  354 A, 6.0 V

TBHT = 233 A, 4.8 V

IGP1= 1.7 e-05 Torr

increase ramp rate to 2A/min

Monday, November 01, 2021, 14:44 

OMEGA= 1585C

TGHT =  367A, 6.3 V

TBHT = 233 A, 4.8 V

IGP1= 1.7 e-05 Torr

Monday, November 01, 2021, 14:49

OMEGA= 1604 C

TGHT =  377A, 6.5V

TBHT = 233 A, 4.8 V

IGP1= 2.1 e-05 Torr 

Monday, November 01, 2021, 14:53 

OMEGA= 1624C

TGHT =  384 A, 6.6V

TBHT = 233 A, 4.8 V

Monday, November 01, 2021, 15:00

OMEGA= 1660C

TGHT =  400 A, 6.8V

TBHT = 233 A, 4.8 V

IGP1= 2.4 e-05 Torr 

Monday, November 01, 2021, 15:17

Initiate autoramp to 430A on TGHT @2A/min

Monday, November 01, 2021, 16:34 

 OMEGA = 1750 C

TGHT = 430 A, 7.3 V

Better heat insulation than before.  Next time need to place a Ta heatshield at the other end on the copper assembly.  Will raise T to 435 A and keep until 1930  hours.

Monday, November 01, 2021, 20:23

IGP1= 1.6 e-05 Torr

Omega = 1760 C

TGHT= 436 A, 7.4 V

TBHT = 232 A, 4.8 V

* Note: kept a approx 1 hour extra hoping that pressure would drop further

Started ramp down at -2A/min for TGHT and -1A/min for TBHT

Coating looks reasonably good.  

 Nb#9 LP-SIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm

Target density =  7.24 g/cm3

Target length = 3.5 cm

Total Mass = 25.343 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  425 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (not yet expanded). No Ta foil heat shield added.

Final desired temperature = 1900C.

OMEGA slope = 0.98.

Wednesday, October 21, 2020, 14:09: Roughing. 

Wednesday, October 21, 2020, 14:32: Turbo pump on. 

Wednesday, October 21, 2020, 15:29: Waterlines opened. Vacuum ok @ 1.05E-05T. 

Wednesday, October 21, 2020, 15:30: TGHT / TBHT PS on. Slope Set.

Wednesday, October 21, 2020, 19:06: Auto-ramping TGHT / TBHT to 300 / 100 @ 1 A per min. Vacuum @ 1.85e-06T.

Thursday, October 22, 2020, 07:26: Auto-ramping TGHT / TBHT to 500 / 200 @ 2 A per min. Vacuum @ 7.61e-07T.

Thursday, October 22, 2020, 11:28: Auto-ramping TGHT / TBHT to 580 / 230 @ 2 A per min. Vacuum @ 1.53e-06T. The Omega IR2C is back. Temp @ 1576 deg C.

Thursday, October 22, 2020, 12:22: Auto-ramping TGHT to 625 A @ 2 A per min. Vacuum @ 2.47e-06T. Temp @ 1734 C.  

Thursday, October 22, 2020, 12:48: Auto-ramping TGHT to 645 A @ 2 A per min. Vacuum @ 3.11e-06T. Temp @ 1815 C.   

Thursday, October 22, 2020, 13:10: Auto-ramping TGHT to 660 A @ 2 A per min. Vacuum @ 3.39e-06T. Temp @ 1851 C.  

Thursday, October 22, 2020, 13:25: Manually tap up TGHT until 1900 C. Vacuum @ 3.53e-06T.

Thursday, October 22, 2020, 13:30: TGHT @ 673 A. Temp @ 1903 C. Vacuum @  3.79e-06T.

Thursday, October 22, 2020, 14:00: Auto-cooling @ 1 A per min. 

Friday, October 23, 2020, 07:50: PS off. Turbo pump off. Purge waterline. 

Friday, October 23, 2020, 09:02: Venting. 

Ta#61 LP-SIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm

Target density =  12.76 g/cm3

Target length = 3.4 cm

Total Mass = 43.388 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  464 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 100 singles / 1pack / 75 singles / 2packs / 75 singles / 1pack / 100 singles / 1pack

End caps installed (not yet expanded). No Ta foil heat shield added 

TBHT will be ramped up to 230A at 1.0A/min.

TGHT will be ramped up to 600A + at 2.0A/min.

Final desired temperature = 1900C.

OMEGA slope = 0.98.

Tuesday, October 06, 2020, 14:17: Roughing.

Tuesday, October 06, 2020, 14:36: Turbo pump on.

Tuesday, October 06, 2020, 14:43: Turbo pump not spinning up. Holding at 4 krpm. Will need to vent and Troubleshoot in the am.  

Attempted to run the turbo pump again. Only runs to 4 krpm. Shut down to avoid trip. Vent & remove Flex-line HS. Change all the SS gaskets. Re-install Flex-line HS w/ Ta#61.

Wednesday, October 07, 2020, 09:16: Roughing. 

Wednesday, October 07, 2020, 09:32: Turbo pump on. 

Wednesday, October 07, 2020, 10:05: Multiple attempts made to spin up the turbo pump. TP1 holds at 4 krpm, occasionally to 5 krpm, times out & trips. 

Wednesday, October 07, 2020, 10:08: Shut off TP1 & backing pump. 

Replaced TP1. https://elog.triumf.ca/TIS/Evaporator_2/514

Wednesday, October 07, 2020, 13:45: TP1 off. Soft start function off. Remote start configuration initiated. TP1 on @ 38krpm. OK. 

Wednesday, October 07, 2020, 13:47: Vacuum @ 1.31e-05T.

Wednesday, October 07, 2020, 13:49: Waterlines opened. Vacuum ok @ 1.27e-05T.

Wednesday, October 07, 2020, 13:50: PS switched on. 

Wednesday, October 07, 2020, 15:24: Slope set @ 0.98. Vacuum @ 3.30e-06T.

Wednesday, October 07, 2020, 15:26: TGHT / TBHT on. Manually tap up to 10 / 10 A.

Wednesday, October 07, 2020, 15:28: Auto-ramping TGHT / TBHT to 300 / 150 A @ 2 / 1 A per min. 

Thursday, October 08, 2020, 05:23: Vacuum @ 7.00e-07T. 

Thursday, October 08, 2020, 05:25: Auto-ramping TGHT / TBHT to 450 / 200 A @ 2 / 1 A per min. Temp @ 996 C

Thursday, October 08, 2020, 06:44: Auto-ramping TGHT / TBHT to 550 / 230 A @ 2 / 1 A per min. Temp @ 1426 C

Thursday, October 08, 2020, 07:43: Vacuum @ 3.88e-06T. Temp @ 1685 C. 

Thursday, October 08, 2020, 07:45: Auto-ramping TGHT to 600 A @ 2 A per min.

Thursday, October 08, 2020, 08:42: Auto-ramping TGHT to 630 A @ 2 A per min. Vacuum @ 4.01e-06T. Temp @ 1800 C. 

Thursday, October 08, 2020, 09:07: Auto-ramping TGHT to 645 A @ 2 A per min. Vacuum @ 4.91e-06T. Temp @ 1851 C.  

Thursday, October 08, 2020, 09:19: Auto-ramping TGHT to 655 A @ 2 A per min. Vacuum @ 5.37e-06T. Temp @ 1879 C.   

Thursday, October 08, 2020, 09:28: TGHT @ 650-657 A. Vacuum @ 5.70e-06T. Temp @ 1901 C. Desired temperature reached*

Thursday, October 08, 2020, 09:59: TGHT @ 650-657 A. Vacuum @ 4.64e-06T. Temp @ 1903 C.

Thursday, October 08, 2020, 10:01:  Auto-cooling TGHT / TBHT @ -3 / -2 A per min. 

Thursday, October 08, 2020, 13:57: TP1 / PS off.

Thursday, October 08, 2020, 14:08: Venting. 

Thursday, October 08, 2020, 14:15: Flex-Line HS removed w/ Ta#61. 

 Short oven loaded with additional hardware are spacers into the flex-line HS.

A Ta short tube was wrapped with 3 tantalum foils,

a tantalum cap was inserted in both sides of the Ta tube, the caps weren't sealed.

The tube was set in the EVAP2 

Wednesday, August 12, 2020, 11:48: Electrical check in EVAP 2:

Target to HS @ 563V 

Leg to leg above bracket

TGHT A @ 10A: 1.332 mOhm

TGHT B @ 10A: 1.300 mOhm

Leg to leg w/ bracket

TGHT A @ 10A: 1.490 mOhm

TGHT B @ 10A: 1.491 mOhm

Wednesday, August 12, 2020, 12:08: Roughing.

Wednesday, August 12, 2020, 2:08: Turbo.

Thursday, August 13, 2020, 09:14

 IGP1 = 7.9e-7 Torr

A leak check was performed, no leak detected.

 TGHT power supply on.

Thursday, August 13, 2020, 10:03

IGP1 = 7.7e-7 Torr.

The current was tapped to 50 A 

Autoramp set to 1 A each 10 s to 200 A

Good vaccum 3e-5 Torr

Bad vacuum 5e-5 torr

Thursday, August 13, 2020, 10:47

Autoramp reached 200 A

TGHT =  200.25 A, 2.38 V

IGP1 = 1.58e-6 Torr

 Thursday, August 13, 2020, 11:07

TGHT =  200.25 A, 2.38 V

IGP1 = 9.66e-7 Torr

Target is shinning dimly

Omega reads 1033 +-50 degC

ARIEL pyrometer is installed in the back of the EVA2 to measured the body temperature of the oven

Thursday, August 13, 2020, 15:30

The connection of the pyrometer with the software was not possible to establish and delay the ramp up of the oven

Friday, August 14, 2020, 10:47

Restarting experiment, 

IGP1 =  4.24e-7 Torr

TGHT = 0 A, ) V, (TGHT was ramped down)

Autoramp set to 1 A each 10 s to 200 A

Good vaccum 3e-5 Torr

Bad vacuum 5e-5 torr

Friday, August 14, 2020, 11:48

Target is shinning dimly

Omega reads 1033 +-50 degC

Autoramp set to 1 A each 10 s to 250 A

Autoramp set to 5 A each 60 s to 450 A

Friday, August 14, 2020, 13:51

TGHT = 6.46 V, 450.13 A

IGP1 = 2.32e-6 Torr

Omega = 1931 °C (slope 0.99)

ARIEL pyrometer = 1504.5 °C (slope 0.929)

Friday, August 14, 2020, 14:06

Autoramp = 5A each 2 min until 500 

Autoranp stopped at 475 A (EPICS TGHT = 6.87V, 476.663A)

Omega = 2013 °C

ARIEL pyrometer = 1547 °C

Friday, August 14, 2020, 17:34

Autoramp is set to  5A each 2 min until 500 

TGHT = 7.403 V, 500.006 A, 

omega = 2104 C

AP= 1586 C

Friday, August 14, 2020, 17:49

Autoramp  is set to  5A each 2 min until 550 

Autoramp stopped by itself at 545 A instead of 550 A

TGHT = 8.11V, 547.65A, 

omega = 2214C

AP= 1656.8 C

IGP1=6.8e-6 Torr

Friday, August 14, 2020, 18:13

 Autoramp  is set to  10A each 2 min until 600

Friday, August 14, 2020, 21:42

TGHT = 9.213 V, 597.8 A,

IGP1 3.27e-6 Torr

Omega =  2380 °C

Ramping down at 5 A per min to 475 A

Monday, August 17, 2020, 09:02

TGHT =  6.741 V, 471.6 A,

IGP1 = 3.46e-7 Torr

Omega = 2052 6°C 

Proceeded to ramp down at  5 A per min to 0 A 

 Wednesday, August 26, 2020, 10:26

A Ta short tube was loaded with a C-cartridge

Currently, the tube is under vacuum and it will be heated to 2000 °C during 3 days.

IGP1 = 3.2e-7 Torr

 Wednesday, August 26, 2020, 16:15

IGP1 = 2.5e-7 Torr

Good vacuum = 3e-2 Torr

Bad vacuum = 5e-2Torr

Autoram set to 200A at 10A/30 s

Wednesday, August 26, 2020, 17:05

TGHT = 3.9 V, 301.3 A

IGP1 = 5.4e-7 torr 

Omega = 1378 °C

AP (slope 0.9) = 1441.8 °C

Wednesday, August 26, 2020, 17:20 

Autoramp set to 550 A at 5A/30s

Wednesday, August 26, 2020, 23:43 

TGHT = 7.561 V, 504.9 A

Omega = 2124 °C

AP = 2010.5 °C

Thursday, August 27, 2020, 07:15

TGHT =  7.461 V, 510.2 A

Omega = 2103 °C

 Thursday, August 27, 2020, 13:41

TGHT = 7.5 V, 510.8 A

Omega = 2099 °C

Friday, August 28, 2020, 09:24

TGHT = 7.4 V, 513.9 A 

Omega = 2103 °C

Friday, August 28, 2020, 13:12

TGHT = 7.46 V, 505.6 A

IGP1 = 2.7e-7 Torr

Omega = 2103 °C

Saturday, August 29, 2020, 14:18

IGP1 = 2.5e-7 Torr

TGHT = 7.5 V, 510.8 A

Omega = 2109 °C 

Saturday, August 29, 2020, 17:44

IGP1 = 2.4e-7 Torr

TGHT = 7.5 V, 505.2 A

Omega = 2119 °C 

Saturday, August 29, 2020, 17:51 

Starting ramp down to 0 A at 5 A/min

Objective: Coating the inner surface of a tantalum tube to make a destructive test and use a reference for the tantalum boats coatings

Results: 

Sunday, March 27, 2021, 11:23

No water leak

IGP1 = 3.7e-7 torr

Sunday, March 27, 2021, 16:10

The wire was heated in the same manner as the last three runs

From 0A to 7A the autoramp was set to 0.5A/min

At 8A the wire started the glow dimmly 

Above 8A, the wire was heated manually at 0.5A until 16A where the step was changed to 1A, 

the temperature was measured with the filament pyrometer every 2 A starting at 10A

At 42 A the step was changed to 0.6A until 42.6A, 4.38V (2020 °C), the wire was kept at that temperature for 90 min

After that time, the current was ramped down at 0.5A/min until ~20A when the current rampping was changed too 1A/min

Objective: Coating the inner surface of a short tantalum boat with rhenium.

Result:

• The wire snnaped around 376 W (53 A, and 7.09 V) and 2170 °C (measured with filament pyrometer)
• The tube does not have indications of coating

Thursday, March 25, 2021, 11:23

Yesterday a heat shield was installed in the EVAP2.

The desired temperature of the Re wire is 2500 degC

A water leak was performed (elog 539 describes it), no leak was detected.

Tuesday, March 23, 2021, 11:01

Pressure 3.8e-7 Torr, current rate set to 6 A @ 0.5 A/min

The wire started glowing at TGHT =  4W, 7A, 0.56V

When reaching 7A the current was increased 0.5 A manually 

When reaching 16 A,  the current was increased 1 A manually until reaching 54 A when the wire snapped

Friday, March 26, 2021, 13:55

Yesterday a heat shield was installed in the EVAP2.

A 1mm thick rhenium wire was held within two copper brackets to pass through a Cu tube with the intention of coating its inside face.

The desired temperature of the Re wire is 2500 degC

A water leak was performed and no leak was detected

 Monday, August 31, 2020, 12:23

A short naked Ta tube (no heat shielding), previously coated with TaC was set under vacuum, 

and it will be kept at 2000 °C for 3 days to later identify the TaC's carbon penetration.

Currently pumping down.

 Tuesday, September 01, 2020, 12:25

IGP1 = 2.0-7 Torr

Good vacuum = 3e-2 Torr

Bad vacuum = 5e-2Torr

Autoram set to 200A at 10A/30 s

Tuesday, September 01, 2020, 12:36

IGP1 = 5.2e-7 Torr

Autoramp set to 300 A at 5 A/30 s 

Tuesday, September 01, 2020, 14:11

IGP1 = 3.4e-7 Torr 

TGHT = 330.2 A, 4.2 V

Omega = 1234 °C

Tuesday, September 01, 2020, 14:31

IGP1 = 1.76e-6 torr

TGHT = 6.94 V, 510 A

Oemga = 1564 C, 

AP = 1390.2 C

Autoramp set to 600 A at 5 A/30s 

Tuesday, September 01, 2020, 15:33

TGHT power supply = 600 A, 8.74 V

Omega = 1807 C

Autoramp set to 700 A at same rate

 Tuesday, September 01, 2020, 15:33

TGHT power supply = 11.94 V, 765 A

Omega = 2157 °C

Wednesday, September 02, 2020, 10:15 

IGP1 = 1.0e-6 Torr

TGHT = 12.0 V, 772 A

Omega = 2167 °C

Wednesday, September 02, 2020, 13:26

IGP1  = 9.1e-7 Torr

TGHT = 12 V, 769.5 A

Omega = 2166 °C 

Wednesday, September 02, 2020, 16:06

IGP1 = 8e-7 Torr

TGHT = 12 V, 773.3 A

Omega = 2167 °C 

Wednesday, September 02, 2020, 20:53

IGP1 =7.4e-7 Torr

TGHT = 11.8 V, 760.95 A

Omega = 2164 °C 

Thursday, September 03, 2020, 09:54

IGP1 = 5.5e-7 Torr

TGHT = 11.9 V, 774 A

Omega = 2162 °C 

Thursday, September 03, 2020, 11:06

IGP1 = 5.3e-7 Torr

TGHT  = 11.9 V, 758.7A

Omega = 2161 °C

Thursday, September 03, 2020, 14:39

IGP1 = 4.8e-7 Torr 

TGHT = 11.9 V, 771.8 A

Omega = 2164 °C

Friday, September 04, 2020, 09:34

IGP1 = 3.9e-7 Torr

TGHT = 11.9 V, 760.1 A

Omega = 2168 °C 

Friday, September 04, 2020, 13:39

 IGP1 = 3.5e-7 Torr

TGHT = 11.9 V, 758.6 A

Omega = 2170 °C

 Friday, September 04, 2020, 15:55

IGP1 = 3.5e-7 Torr

TGHT = 12 v, 760.6 a

Omega = 2171 °C