Logbooks Lab Maintenance Evaporator_1 Evaporator_2 Laser cutter Target Production Test-Stand RH-ISAC RH-Cyclotron RH-Meson Hall RH-Beamlines RH-ARIEL
  Evaporator_2, Page 32 of 35  Not logged in ELOG logo
  ID Date Author Target Material Target Oven W.O# Source Status Subjectdown
  140   Friday, June 20, 2014, 16:22 John WongSiC39530-8HP-FEBIADIn progressConditioning SiC#31 target

Laura Lambert wrote:

 Friday, June 20, 2014, 11:14

Total number of foils: 515 discs

Total mass of materials [incl graphite foils]: 64.7224g

Total length packed: 17.8cm

Container is wrapped with 3x Ta-heat shields.

Currently being pumped down.


 Friday, June 20, 2014, 14:56

HS cooling water valves opened, no leaks detected.

IGP1 = 6.2e-6 Torr

TGHT max = 820A/ 17V

TBHT max = 300A/ 5V

Stepping up manually to 40A


 Friday, June 20, 2014, 16:04

IGP1 = 8e-6 Torr

Slowly stepped up to 35A manually.

Vacuum has stabilized.

Initiating auto-ramp at 0.1A/min


 

 Friday, June 20, 2014, 16:16

Changing the heating current... 

From the previous SiC targets, TGHT was ramped up to 800A and yellow crystals were found; the end caps and target legs were also found broken (see my iPad).  This might be too hot for the Ta-boat to handle the sintering process. 

For this process,

TGHT will ramp up to 600A and TBHT to 230A over the weekend. 

Then, the temperature will be measured.  The sintering temperature of SiC is ~1800 - 2000C. 


 

  141   Monday, June 23, 2014, 09:47 Laura LambertSiC39530-8HP-FEBIADIn progressConditioning SiC#31 target

John Wong wrote:

Laura Lambert wrote:

 Friday, June 20, 2014, 11:14

Total number of foils: 515 discs

Total mass of materials [incl graphite foils]: 64.7224g

Total length packed: 17.8cm

Container is wrapped with 3x Ta-heat shields.

Currently being pumped down.


 Friday, June 20, 2014, 14:56

HS cooling water valves opened, no leaks detected.

IGP1 = 6.2e-6 Torr

TGHT max = 820A/ 17V

TBHT max = 300A/ 5V

Stepping up manually to 40A


 Friday, June 20, 2014, 16:04

IGP1 = 8e-6 Torr

Slowly stepped up to 35A manually.

Vacuum has stabilized.

Initiating auto-ramp at 0.1A/min


 

 Friday, June 20, 2014, 16:16

Changing the heating current... 

From the previous SiC targets, TGHT was ramped up to 800A and yellow crystals were found; the end caps and target legs were also found broken (see my iPad).  This might be too hot for the Ta-boat to handle the sintering process. 

For this process,

TGHT will ramp up to 600A and TBHT to 230A over the weekend. 

Then, the temperature will be measured.  The sintering temperature of SiC is ~1800 - 2000C. 


 

 Monday, June 23, 2014, 09:45

IGP1 = 5e-6 Torr

TGHT and TBHT are at ~200A

Increasing ramping rate to 0.2A/min


 Monday, June 23, 2014, 11:19

IGP1 = 6.9e-6 Torr

Increasing ramping rate to 2.0A/min


Monday, June 23, 2014, 12:09

JW:  Pressure went up too fast... lower the TGHT ramping up rate to 1A/min.


 Tuesday, June 24, 2014, 16:06

Increasing current with respect to temperature: See attached table


 

Attachment 1: current_vs_temp.jpeg
current_vs_temp.jpeg
  142   Tuesday, June 24, 2014, 23:57 John WongSiC39530-8HP-FEBIADIn progressConditioning SiC#31 target

Laura Lambert wrote:

John Wong wrote:

Laura Lambert wrote:

 Friday, June 20, 2014, 11:14

Total number of foils: 515 discs

Total mass of materials [incl graphite foils]: 64.7224g

Total length packed: 17.8cm

Container is wrapped with 3x Ta-heat shields.

Currently being pumped down.


 Friday, June 20, 2014, 14:56

HS cooling water valves opened, no leaks detected.

IGP1 = 6.2e-6 Torr

TGHT max = 820A/ 17V

TBHT max = 300A/ 5V

Stepping up manually to 40A


 Friday, June 20, 2014, 16:04

IGP1 = 8e-6 Torr

Slowly stepped up to 35A manually.

Vacuum has stabilized.

Initiating auto-ramp at 0.1A/min


 

 Friday, June 20, 2014, 16:16

Changing the heating current... 

From the previous SiC targets, TGHT was ramped up to 800A and yellow crystals were found; the end caps and target legs were also found broken (see my iPad).  This might be too hot for the Ta-boat to handle the sintering process. 

For this process,

TGHT will ramp up to 600A and TBHT to 230A over the weekend. 

Then, the temperature will be measured.  The sintering temperature of SiC is ~1800 - 2000C. 


 

 Monday, June 23, 2014, 09:45

IGP1 = 5e-6 Torr

TGHT and TBHT are at ~200A

Increasing ramping rate to 0.2A/min


 Monday, June 23, 2014, 11:19

IGP1 = 6.9e-6 Torr

Increasing ramping rate to 2.0A/min


Monday, June 23, 2014, 12:09

JW:  Pressure went up too fast... lower the TGHT ramping up rate to 1A/min.


 Tuesday, June 24, 2014, 16:06

Increasing current with respect to temperature: See attached table


 

 Tuesday, June 24, 2014, 23:44

Target has been heated at 600A.  Local temperature measured on the right leg = 1814C. 

RGA/ striptool/temperature data can be found on this link: 

https://www.dropbox.com/sh/69memvh6fthodoz/AABZiSKAR9njhbqO4sBATVbla

Something interesting was observed about the out gassing of this target - the right window was coated when the temperature rose above 1500C (on the right end, could be hotter inside?) - see attachment.

I suspect this is Si vapour deposited on the window when the target heater got closed to the sintering temperature for SiC (1800 - 2000C).  

Once the chamber is vented, the coated window will be inspected and analyzed.  More details later...  

Initiate auto-cooling (slow cool down)  TGHT 1A/min; TBHT 0.5/min.  Chamber should be able for venting tomorrow afternoon.  


 

 

Attachment 1: 2014-06-24_16.57.17.jpg
2014-06-24_16.57.17.jpg
  270   Monday, January 11, 2016, 15:47 Laura LambertSiC41077-3LP-SISDoneConditioning SiC test target for test stand measurements

Monday, January 11, 2016, 15:25

Small center block LP-SIS container previously sintered with TaC coating

3x Ta heat shields

Container is loaded with 260 discs of SiC with a total length of 8.5cm

Loaded into evap2 and pumped down this morning

HS water valves opened up, no leaks detected

Tapped up manually to 30A

Vacuum stable

IGP1 = 1e-6 Torr

Initiating auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively

Final setpoints: 400A for the TGHT and 230A for the TBHT

Final desired temperature: 1700C


 Tuesday, January 12, 2016, 12:55

TGHT = 138A, TBHT = 80A

IGP1 =  7.7e-6 Torr.


Vacuum stable and coming down.

Increasing ramping rate to 0.5A/min and 0.2A/min for the TGHT and TBHT respectively.


 Wednesday, January 13, 2016, 09:32

TGHT reached 400A ~11.5hrs ago

TBHT reached 230A ~8hrs ago

OMEGA = 1400C

IGP1 = 1.75e-7 Torr

Tapping up manually to 1700C...


 Wednesday, January 13, 2016, 10:14

Previous temperature measurement of OMEGA = 1400C is wrong due to window port being coated with SiC [see attached photos]

Will remain at TGHT = 420A for 4hrs then cool down this afternoon


Wednesday, January 13, 2016, 14:29

Remained at max setpoints for 4.5hrs.

Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


 Thursday, January 14, 2016, 09:47

Vented in air and opened up this morning

Target looks good

Will insert and expand endcaps this afternoon


 

Attachment 1: Photo_2016-0-13.jpg
Photo_2016-0-13.jpg
Attachment 2: Photo_2016-01-13_#2.jpg
Photo_2016-01-13_#2.jpg
Attachment 3: Photo_2016-01-13_#3.jpg
Photo_2016-01-13_#3.jpg
Attachment 4: Photo_2016-01-13_#4.jpg
Photo_2016-01-13_#4.jpg
  519   Wednesday, October 21, 2020, 14:39 Aaron SchmidtNb44508-2LP-SISIn progressConditioning Nb#9

 Nb#9 LP-SIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm

Target density =  7.24 g/cm3

Target length = 3.5 cm

Total Mass = 25.343 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  425 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

End caps installed (not yet expanded). No Ta foil heat shield added.


Final desired temperature = 1900C.

OMEGA slope = 0.98.

Wednesday, October 21, 2020, 14:09: Roughing. 

Wednesday, October 21, 2020, 14:32: Turbo pump on. 

Wednesday, October 21, 2020, 15:29: Waterlines opened. Vacuum ok @ 1.05E-05T. 

Wednesday, October 21, 2020, 15:30: TGHT / TBHT PS on. Slope Set.

Wednesday, October 21, 2020, 19:06: Auto-ramping TGHT / TBHT to 300 / 100 @ 1 A per min. Vacuum @ 1.85e-06T.


Thursday, October 22, 2020, 07:26: Auto-ramping TGHT / TBHT to 500 / 200 @ 2 A per min. Vacuum @ 7.61e-07T.

Thursday, October 22, 2020, 11:28: Auto-ramping TGHT / TBHT to 580 / 230 @ 2 A per min. Vacuum @ 1.53e-06T. The Omega IR2C is back. Temp @ 1576 deg C.

Thursday, October 22, 2020, 12:22: Auto-ramping TGHT to 625 A @ 2 A per min. Vacuum @ 2.47e-06T. Temp @ 1734 C.  

Thursday, October 22, 2020, 12:48: Auto-ramping TGHT to 645 A @ 2 A per min. Vacuum @ 3.11e-06T. Temp @ 1815 C.   

Thursday, October 22, 2020, 13:10: Auto-ramping TGHT to 660 A @ 2 A per min. Vacuum @ 3.39e-06T. Temp @ 1851 C.  

Thursday, October 22, 2020, 13:25: Manually tap up TGHT until 1900 C. Vacuum @ 3.53e-06T.

Thursday, October 22, 2020, 13:30: TGHT @ 673 A. Temp @ 1903 C. Vacuum @  3.79e-06T.

Thursday, October 22, 2020, 14:00: Auto-cooling @ 1 A per min. 


Friday, October 23, 2020, 07:50: PS off. Turbo pump off. Purge waterline. 

Friday, October 23, 2020, 09:02: Venting. 

  641   Thursday, August 24, 2023, 14:18 Aaron SchmidtNb45447-9LP-IG-LISIn progressConditioning Nb#11

 Nb#11 LP-IG-LIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm (0.001")

Target density =  7.13 g/cm3

Target length = 3.53 cm

Total Mass = 25.165 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  434 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added

Final desired temperature = 1900C.

Replacement for Nb#10


Thursday, August 24, 2023, 14:16: Roughing.

OMEGA slope = 0.98.

Thursday, August 24, 2023, 14:31: Turbo pump started. 

Thursday, August 24, 2023, 14:41: TGHT / TBHT PS on. Manually test @ 5 / 5 A. ok. Tap back to 0 A. 

Thursday, August 24, 2023, 18:26: Vacuum @ 4.35e-06T. Auto-ramping TGHT / TBHT to 580 / 230 A @ 2 A per minute. 

Thursday, August 24, 2023, 22:00: TGHT / TBHT @ 414 / 230 A (406 / 233 A - Offset). Auto-ramping TGHT to 580 A @ 2 A per min continued. Temperature @ 1353 C. Vacuum @ 4.03e-06T. 

Thursday, August 24, 2023, 23:29: TGHT / TBHT @ 580 / 230 A (569 / 233 A). Auto-ramping TGHT to 610 A @ 2 A per min (approx 600 A w/ offset). Temperature @ 1708 C. Vacuum @ 6.61e-06T. 

Thursday, August 24, 2023, 23:49: TGHT / TBHT @ 610 / 230 A (598 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (620 A w/ offset). Temperature @ 1765 C. Vacuum @ 7.22e-06T. 


Friday, August 25, 2023, 00:04: TGHT / TBHT @ 630 / 230 A (618 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1808 C. Vacuum @ 7.54e-06T. 

Friday, August 25, 2023, 00:16: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 670 A @ 2 A per min (660 A w/ offset). Temperature @ 1845 C. Vacuum @ 7.72e-06T. 

Friday, August 25, 2023, 00:27: TGHT / TBHT @ 670 / 230 A (657 / 233 A). Auto-ramping TGHT to 680 A @ 2 A per min (668 A w/ offset). Temperature @ 1880 C. Vacuum @ 8.46e-06T. 

Manually tap up to temperature.

Friday, August 25, 2023, 00:34: TGHT / TBHT @ 682 / 230 A (669 / 233 A). Temperature @ 1900-1901 C. Vacuum @ 8.59e-06T. Desired Temperature Reached.

Friday, August 25, 2023, 00:37: Auto-cooling @ 2 A per min. 

Friday, August 25, 2023, 06:15: 

 

Friday, August 25, 2023, 07:40: PS & TP off.

 

  638   Wednesday, June 21, 2023, 10:37 Aaron SchmidtNb45447-7LP-IG-LISIn progressConditioning Nb#10

Nb#10 LP-IG-LIS target description:

Total Ta foils = 470 [6x20 packs + 350 single discs]

Foil Thickness = 0.025mm (0.001")

Target density =  7.36 g/cm3

Target length = 3.5 cm

Total Mass = 25.7576 g [Incl foils + Ta wire on 6 packs]

Total mass w/ Target oven=  438 g (w/ end caps)

Discs in target are arranged as follows: 1pack / 75 singles / 1pack / 100 singles / 2packs / 100 singles / 1pack / 75 singles / 1pack

Dimpling direction on foils/ Packs.                                                               --> Center <--

End caps installed (Not expanded). No Ta foil heat shield added


Wednesday, June 21, 2023, 10:37: Roughing.

Wednesday, June 21, 2023, 13:39: TP1 on. 

Wednesday, June 21, 2023, 13:55: TGHT / TBHT PS on. Vacuum @ 3.35e-05T


Thursday, June 22, 2023, 13:16: TGHT / TBHT Manually set to 5 / 5 A. Vacuum @ 8.17e-07T.

Final desired temperature = 1900C.

Thursday, June 22, 2023, 13:49: OMEGA slope = 0.98.


Friday, June 23, 2023, 06:24: Auto-ramping TGHT / TBHT to 580 / 230 @ 2 A per min. 

Friday, June 23, 2023, 12:11: TGHT / TBHT @ 580 / 230 A (568 / 233 A). Auto-ramping TGHT to 610 A @ 2 A per min (600 A w/ offset). Temperature @ 1697 C. Vacuum @ 3.38e-06T.

Friday, June 23, 2023, 12:32: TGHT / TBHT @ 610 / 230 A (600 / 233 A). Auto-ramping TGHT to 630 A @ 2 A per min (620 A w/ offset). Temperature @ 1748 C. Vacuum @ 4.61e-06T.

Friday, June 23, 2023, 12:44: TGHT / TBHT @ 630 / 230 A (617 / 233 A). Auto-ramping TGHT to 650 A @ 2 A per min (640 A w/ offset). Temperature @ 1790 C. Vacuum @ 5.74e-06T.

Friday, June 23, 2023, 13:07: TGHT / TBHT @ 650 / 230 A (638 / 233 A). Auto-ramping TGHT to 670 A @ 2 A per min (660 A w/ offset). Temperature @ 1825 C. Vacuum @ 5.90e-06T.

Friday, June 23, 2023, 13:22: TGHT / TBHT @ 670 / 230 A (658 / 233 A). Auto-ramping TGHT to 680 A @ 2 A per min (668 A w/ offset). Temperature @ 1858 C. Vacuum @ 6.75e-06T. 

Friday, June 23, 2023, 13:29: TGHT / TBHT @ 680 / 230 A (667 / 233 A). Auto-ramping TGHT to 690 A @ 2 A per min (677 A w/ offset). Temperature @ 1877 C. Vacuum @ 6.99e-06T. 

Friday, June 23, 2023, 13:37: Manually tap up to temperature. 

Friday, June 23, 2023, 13:38: Vacuum @ 7.54e-06T. TGHT /  TBHT @ 694 / 230 A (680.5 / 233 A direct w/ offset). Temperature @ 1901-1902 C. Desired Temperature Reached.

 

Friday, June 23, 2023, 13:42: Auto-cooling @ 2 A per min. 

  166   Thursday, October 09, 2014, 17:41 John WongNb TARGET BOATDoneConditioning Nb targets (for Bob)

Thursday, October 09, 2014, 17:36

Target boat consists of 5 Nb discs.  Each disc is wrapped with Nb foil, and to be heated to 1400C for 4 hours.

Chamber has been pumped down to 6.5e-7 Torr.  HS valves open - no leaks detected.

TGHT has ramped to 330A to maintain the 1400C temperature. 

At 21:30, the target will be cooled down.

Temperature can be monitored from this link:

https://www.dropbox.com/sh/kor6gnutnlimqxw/AAAee2yb-Hj3JEbBysrAW2oYa?dl=0


 Thursday, October 09, 2014, 22:48

Samples have been heated at 1420C for over 4 hours.  

Pressure at 6.6 e-7 Torr. 

Cooling process initiated, ramping down at 2A/min. 


 Friday, October 10, 2014, 13:50

Samples were successfully conditions; no signs of any damage.


 

Attachment 1: samples@1400C.png
samples@1400C.png
  164   Thursday, October 09, 2014, 15:59 John WongNb TARGET BOATIn progressConditioning Nb target (for Bob)

Thursday, October 09, 2014, 15:56

The target boat contains 5 samples of Nb discs.  Each disc is wrapped with Nb foil and labelled. 

Samples will be heated up to 1400C for 4 hours. 

chamber has been pumped down to 3.9e-6 Torr. HS valves open - no leaks detected.

Ramping up TGHT...


 

  293   Wednesday, May 04, 2016, 13:45 Laura Lambert 40282-3TARGET BOATIn progressConditioning Nb samples for Tobias

 Wednesday, May 04, 2016, 13:28

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.

Smaller sample closest to OMEGA IR reading [right side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 yesterday.

Vacuum pump bearings gone - pump replaced this morning by vacuum group.

Pumping down now...


 Friday, May 06, 2016, 13:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 2.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to 250A over the weekend.

Will tap up manually monday to final desired temperature of 1400C.


 Monday, May 09, 2016, 09:38

OMEGA = 1128C

IGP1 = 1.3e-7 Torr

TGHT = 250A, 3.7V

Tapping up manually to 1400C...


 Monday, May 09, 2016, 14:05

Evap2 has reached ~1405C

TGHT = 341A, 5.34V

IGP1 = 1.9e-7 Torr

Will remain at max setpoints for min 4hrs then initiate cool down.


 

Attachment 1: Nb_samples_in_boat_(2).jpg
Nb_samples_in_boat_(2).jpg
  294   Monday, May 09, 2016, 18:19 John Wong 40282-3TARGET BOATIn progressConditioning Nb samples for Tobias

Laura Lambert wrote:

 Wednesday, May 04, 2016, 13:28

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.

Smaller sample closest to OMEGA IR reading [right side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 yesterday.

Vacuum pump bearings gone - pump replaced this morning by vacuum group.

Pumping down now...


 Friday, May 06, 2016, 13:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 2.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to 250A over the weekend.

Will tap up manually monday to final desired temperature of 1400C.


 Monday, May 09, 2016, 09:38

OMEGA = 1128C

IGP1 = 1.3e-7 Torr

TGHT = 250A, 3.7V

Tapping up manually to 1400C...


 Monday, May 09, 2016, 14:05

Evap2 has reached ~1405C

TGHT = 341A, 5.34V

IGP1 = 1.9e-7 Torr

Will remain at max setpoints for min 4hrs then initiate cool down.


 

 Monday, May 09, 2016, 18:18

TGHT at 341A/5.34V for over 4 hours.  Vac stables at 1.78e-7 Torr.

Cooling down at 2A/min


 

  295   Tuesday, May 10, 2016, 11:57 Laura Lambert 40282-3TARGET BOATDoneConditioning Nb samples for Tobias

John Wong wrote:

Laura Lambert wrote:

 Wednesday, May 04, 2016, 13:28

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Larger niobium samples are placed in the slots, holding in place, to avoid warping; smaller niobium sample sitting inside the boat by itself.

Smaller sample closest to OMEGA IR reading [right side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 yesterday.

Vacuum pump bearings gone - pump replaced this morning by vacuum group.

Pumping down now...


 Friday, May 06, 2016, 13:36

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 2.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to 250A over the weekend.

Will tap up manually monday to final desired temperature of 1400C.


 Monday, May 09, 2016, 09:38

OMEGA = 1128C

IGP1 = 1.3e-7 Torr

TGHT = 250A, 3.7V

Tapping up manually to 1400C...


 Monday, May 09, 2016, 14:05

Evap2 has reached ~1405C

TGHT = 341A, 5.34V

IGP1 = 1.9e-7 Torr

Will remain at max setpoints for min 4hrs then initiate cool down.


 

 Monday, May 09, 2016, 18:18

TGHT at 341A/5.34V for over 4 hours.  Vac stables at 1.78e-7 Torr.

Cooling down at 2A/min


 

 Tuesday, May 10, 2016, 08:45

Vented in air and opened up this morning.

Samples look good!


 

  339   Tuesday, November 22, 2016, 15:58 Laura LambertNb40282-3TARGET BOATDoneConditioning Nb samples for Doug

Tuesday, November 22, 2016, 15:53

Target boat has a layer of niobium foil on the bottom of the boat.

A niobium foil has been made with slots to hold samples [similar to when sintering endcaps] *See attached photos

Niobium samples are placed in slots, holding in place, to avoid warping.

Smaller samples closest to MIKRON IR reading [left side]

Boat is wrapped with 1 large layer of Ta foil, wrapped around the boat 3x, careful to avoid touching samples.

Loaded into evap2 today.

Pumping down now...


 Wednesday, November 23, 2016, 11:45

HS water valves opened, no leaks detected.

Tapped up manually to 35A.

IGP1 = 6.4e-7 Torr

Setting auto-ramp rate at 0.2A/min to max setpoint of 250A.

Will tap up manually to final desired temperature of 1400C.


 Wednesday, November 23, 2016, 13:17

IGP1 = 5.9e-7

TGHT = 66A, 0.51V

Vacuum stable.

Increasing ramping rate to 1.0A/min


 Thursday, November 24, 2016, 08:46

IGP1 = 3.9e-7 Torr

TGHT = 250A, 3.41V      *NOTE: the current set reads 243.8A but the readout is 250A

OMEGA = 1013C

MIKRON has no reading yet

Tapping up manually to 1400C


 Thursday, November 24, 2016, 15:42

Samples have remained at ~1400C for 5hrs.

IGP1 = 5.8e-7 Torr

TGHT = 420A, 6.5V

OMEGA = 1410C

MIKRON = 1420C

Initiating auto-cool at 2.0A/min


 Friday, November 25, 2016, 11:39

Vented in air and opened up this morning.

Samples look good!


 

Attachment 1: samples.jpg
samples.jpg
Attachment 2: evap2.jpg
evap2.jpg
Attachment 3: heating_up.xlsx
Attachment 4: visual_of_MIKRON_pointing_at_samples.JPG
visual_of_MIKRON_pointing_at_samples.JPG
  460   Friday, September 27, 2019, 18:18 Marla CervantesNb TARGET BOATDoneConditioning NB samples for Edward

Wednesday, September 25, 2019, 18:06

Target boat with a layer of niobium foil on the bottom is used to heat up Nb samples to 1400 C for 4 hrs.

The niobium samples are wrapped in a Nb foil.

Boat is wrapped with 2 layers of Ta foil, careful to avoid touching samples.


Thursday, September 26, 2019, 18:10 

The target assembly was exchange to a clean one e-log 459 and the Nb arrangement was loaded into evap2.


Friday, September 27, 2019, 18:13

HS water valves opened, no leaks detected.

Tapped up manually to 40 A.

IGP1 = 9.54e-7 Torr

Setting auto-ramp rate at 0.2 A/min to max setpoint of 100 A.

Vacuum stable.

Setting auto-ramp at 1 A/min to 300 A lead to ~1200 C.

Autoramping at 1 A/min to 400 A will stop at 1400 C.

Temperature reading is 1400 C at:

TGHT = 5.61 V, 345.656 A

The temperature reading went to 1408 C on Omega and 1417 C on Micron so the current was dropped to 342.537 A and 5.56 V

The temperature went to 1418 C on Omega and the current was dropped to 339.281 A


After 4 hours at 1400 C, the Nb was cooled down

The final pressure was 3.07e-7 Torr 

The EVAP2 was vented with air and the Nb was removed. 

Attachment 1: Nb-finalTemp.JPG
Nb-finalTemp.JPG
Attachment 2: Nb-arrangement.jpg
Nb-arrangement.jpg
  365   Wednesday, May 10, 2017, 16:07 Laura LambertEmpty TARGET BOATIn progressConditioning Heat Shield for IGLIS UCx#20 - test stand is down

 Wednesday, May 10, 2017, 16:05

Loaded.

HS water valves opened, no leaks detected.

Started auto-ramp at a rate of 1A/30sec to a final setpoint of 580A


 

  366   Wednesday, May 10, 2017, 21:33 Anders MjosEmpty TARGET BOATIn progressConditioning Heat Shield for IGLIS UCx#20 - test stand is down

Laura Lambert wrote:

 Wednesday, May 10, 2017, 16:05

Loaded.

HS water valves opened, no leaks detected.

Started auto-ramp at a rate of 1A/30sec to a final setpoint of 580A


 

 Wednesday, May 10, 2017, 21:31: TGHT at 580 A for 1 h. Vacuum came down to 1.4E-6 Torr. TGHT voltage stable. Ramping down.

  367   Thursday, May 11, 2017, 10:51 Laura LambertEmpty TARGET BOATDoneConditioning Heat Shield for IGLIS UCx#20 - test stand is down

Anders Mjos wrote:

Laura Lambert wrote:

 Wednesday, May 10, 2017, 16:05

Loaded.

HS water valves opened, no leaks detected.

Started auto-ramp at a rate of 1A/30sec to a final setpoint of 580A


 

 Wednesday, May 10, 2017, 21:31: TGHT at 580 A for 1 h. Vacuum came down to 1.4E-6 Torr. TGHT voltage stable. Ramping down.

 Thursday, May 11, 2017, 10:51

vented in air and opened it up this morning.

Heat shield looks good!


 

  176   Monday, February 02, 2015, 16:33 John WongEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

  177   Tuesday, February 03, 2015, 10:31 Laura LambertEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

John Wong wrote:

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

 Tuesday, February 03, 2015, 10:28

HS water valves opened; no leaks detected.

IGP1 = 5.9e-7 Torr


 Wednesday, February 04, 2015, 11:10

attempted to initiate manual ramp up of TGHT and TBHT yesterday, but not responding to EPICS

currently sitting under vacuum, waiting on fix...


 Wednesday, February 04, 2015, 14:16

controls fixed.

initiated auto-ramp.


 Thursday, February 05, 2015, 08:56

IGP1 = 4.1e-7 Torr

TGHT = 290A

TBHT = 225A

Increasing auto-ramp to 1.0A/min


 Thursday, February 05, 2015, 13:49

IGP1 = 1.4e-6 Torr

TGHT = 569A

TBHT = 232A

Increasing auto-ramp to 2.0A/min


 

  178   Thursday, February 05, 2015, 18:03 John WongEmpty41077-2LP-SISIn progressCoating/Sintering TaC on target container - For Graphite Insert

Laura Lambert wrote:

John Wong wrote:

Monday, February 02, 2015, 16:28

Container is coated with TaC.  No Ta foil wrapped around. 

Chamber is being pumped down.

TGHT/TBHT will be ramped up to 580A/230A at 0.2A/min.


 

 

 Tuesday, February 03, 2015, 10:28

HS water valves opened; no leaks detected.

IGP1 = 5.9e-7 Torr


 Wednesday, February 04, 2015, 11:10

attempted to initiate manual ramp up of TGHT and TBHT yesterday, but not responding to EPICS

currently sitting under vacuum, waiting on fix...


 Wednesday, February 04, 2015, 14:16

controls fixed.

initiated auto-ramp.


 Thursday, February 05, 2015, 08:56

IGP1 = 4.1e-7 Torr

TGHT = 290A

TBHT = 225A

Increasing auto-ramp to 1.0A/min


 Thursday, February 05, 2015, 13:49

IGP1 = 1.4e-6 Torr

TGHT = 569A

TBHT = 232A

Increasing auto-ramp to 2.0A/min


 

 Thursday, February 05, 2015, 18:02

Auto-cooling TGHT to 400A at 1A/min.  Need to take voltage reading tomorrow. 


 

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